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银狐傲雪

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[求助] SiO2@TiO2问题已有1人参与

Fe3O4@SiO2obtained in the previous step was redispersed in ethyl alcohol (10 mL) under sonication for 10 min. Tetrabutyl titanate (160 mL) and ethyl alcohol (1 mL) were added to a dried beaker (10 mL capacity) and stirred evenly, followed bythe addition of the suspension of Fe3O4@SiO2(5 mL). Then, ultra-pure water (3 mL) was put in a teon-lined stainlesssteel autoclave (60 mL capacity) and the beaker containing the mixture solution was transferred to it. The autoclave was heated to and maintained at 150 C for 750 min.
请教一下大家,为什么要把烧杯和混合溶液都放入含3mL纯水的反应釜里(the beaker containing the mixture solution )?
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yoesyte

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【答案】应助回帖

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银狐傲雪: 金币+5, 有帮助 2014-10-30 18:51:42
应该是作者写的不够清楚,应该是把烧杯里含有的溶液转移到反应釜里。
2楼2014-10-29 14:06:52
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