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zhangwei章薇

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In contrast, the diffractograms of the ground samples display broad and featureless reections along with a series of overlapped peaks, reflecting notable amorphous features. The formation of amorphous states upon grinding was further confirmed by DSC experiment. As shown in Fig. 5b, there are no thermal transitions for the pristine
solids before isotropic melt transition (Tm); however, each ground solid shows the respective cold-crystallization transition.
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RXMCDM: 金币+1, 多谢应助! 2014-10-12 08:29:35
zhangwei章薇: 金币+5, 翻译EPI+1 2014-10-12 16:32:16
与此相反,研磨样品的衍射图显示随着一系列重叠的宽峰和特征性反射,表现出显著的非晶态特征。用DSC实验进一步证实了研磨时的非晶状态。如图5b所示,在等向性熔体转变(Tm)之前,原始固体没有热转变;然而,每个研磨固体均示出了各冷结晶的转变。
2楼2014-10-12 01:35:52
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