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In contrast, the diffractograms of the ground samples display broad and featureless reections along with a series of overlapped peaks, reflecting notable amorphous features. The formation of amorphous states upon grinding was further confirmed by DSC experiment. As shown in Fig. 5b, there are no thermal transitions for the pristine solids before isotropic melt transition (Tm); however, each ground solid shows the respective cold-crystallization transition. |
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