| 查看: 4972 | 回复: 4 | ||
sunshineyulu金虫 (小有名气)
|
[求助]
求助碳酸钠和碳酸氢钠的标准XRD图谱已有1人参与
|
| 请问哪位有碳酸钠和碳酸氢钠的XRD标准卡片的数据，就需要2θ和intensity的数据，想在origin里面作个图放文章里作为标准，非常感谢！ |
回复此楼» 猜你喜欢
MOF合成
已经有0人回复
-
请问各位大佬ACS投稿状态这样是成功了吗？
已经有6人回复
-
无机化学论文润色/翻译怎么收费?
已经有298人回复
» 本主题相关价值贴推荐，对您同样有帮助:
碳酸氢钠为什么也叫终碳酸钠
已经有5人回复- 求助Ag2CO3标准XRD图谱
已经有4人回复
- XRD标准衍射图谱的绘制
已经有4人回复
- 碳酸钠、碳酸氢钠、硫化钠、硫氢化钠
已经有4人回复
- 哪位大侠有Zn(OH)2 的XRD标准图谱，谢谢。
已经有6人回复
- 导出XRD的标准图谱
已经有12人回复
- 求助：解析N掺杂TiO2的XRD图谱 及TiN的标准图谱
已经有5人回复
- 如何在线分析碳酸钠和碳酸氢纳的混合溶液
已经有3人回复
- 三元材料的XRD图谱精修时如何选择标准图谱
已经有7人回复
- 【求助】氧化铝各个相的XRD标准图谱
已经有9人回复
- 【求助】单斜晶体的XRD图谱分析
已经有9人回复
- 【求助】XRD分析中，pdf卡片里的数据，用什么软件转化成标准的衍射图谱？
已经有12人回复
- 【求助】二氧化硅和碳酸钙的XRD的标准谱图
已经有9人回复
- 【求助】碳酸钙的标准XRD
已经有11人回复
- 【求助】大家有没有XRD标准图谱的下载地址或数据库呢
已经有6人回复
- 【求助】由XRD图谱如何找含量较少的物质？
已经有4人回复
- 【求助】XRD图谱中峰值最大的物质能不能说其含量最高？
已经有11人回复
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
★ ★ ★ ★ ★
感谢参与，应助指数 +1
sunshineyulu: 金币+5, ★★★很有帮助 2014-08-09 14:23:53
感谢参与，应助指数 +1
sunshineyulu: 金币+5, ★★★很有帮助 2014-08-09 14:23:53
|
Card Information Names: alpha-Sodium Carbonate Gregoryite, syn Formula: Na2 C O3 PDF Number: 000-25-0815 Quality: indexed Subfiles: inorganic mineral PHR Cell and Symmetry Information System: hexagonal Space Group: P63mc (no. 186) a: 5.215 c: 6.584 Density (Dx): 2.269 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): Guinier Cut Off: 50.0 Instrument(I): densitometer I type: unknown Comments and Additional Information General: This phase is stable above 490 C. General: Pattern obtained at 565 C. Literature References General: Technisch Physische Dienst, Delft, TheNetherlands. ICDD Grant-in-Aid ( ) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 1 0 0 4.5200 19.6240 1 1 0 1 3.7200 23.9008 27 0 0 2 3.2900 27.0804 40 1 0 2 2.6600 33.6655 100 1 1 0 2.6100 34.3302 75 2 0 0 2.2590 39.8735 1 2 0 1 2.1370 42.2556 40 2 0 2 1.8630 48.8450 30 2 1 0 1.7070 53.6475 8 2 1 1 1.6530 55.5485 4 0 0 4 1.6450 55.8422 4 2 0 3 1.5740 58.5993 2 1 0 4 1.5460 59.7673 1 2 1 2 1.5150 61.1194 4 3 0 0 1.5060 61.5241 6 3 0 1 1.4680 63.2980 2 1 1 4 1.3920 67.1959 1 2 2 0 1.3030 72.4786 8 2 2 2 1.2110 78.9987 1 3 1 2 1.1680 82.5214 1 |
2楼2014-08-08 20:29:17
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
★ ★
sunshineyulu: 金币+2, ★有帮助 2014-08-09 14:23:38
sunshineyulu: 金币+2, ★有帮助 2014-08-09 14:23:38
|
Card Information Names: gamma-Sodium Carbonate Natrite Sodium carbonate - $-gamma Formula: Na2 C O3 PDF Number: 000-77-2082 Quality: calculated Subfiles: inorganic mineral COR FIZ PHR Cell and Symmetry Information System: monoclinic Space Group: C2/m (no. 12) a: 8.90400 b: 5.23900 c: 6.04200 b: 101.350 Density (Dx): 2.547 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54060 Instrument(d): calculated Cut Off: 17.7 Instrument(I): calculated I type: peak heights I/Icor: 0.57 Comments and Additional Information ICSD Number: 060311 Temperature factor: ATF Structure: Modulated structure Pattern: See PDF 00-037-0451. TT Calc. density unusual but tolerable. TI The modulated structure of gamma Na2 C O3 in a harmonic approximation WY j i3 c a (C12/M1) AF AB2X3 Literature References General: Calculated from ICSD using POWD-12++ (1997) Structure: van Aalst, W., den Hollander, J., Peterse,W.J.A.M., de Wolff, P.M. Acta Crystallogr., Sec. B 32 47 (1976) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 0 0 1 5.9238 14.9427 1 1 1 0 4.4922 19.7468 29 2 0 0 4.3649 20.3284 2 -2 0 1 3.8996 22.7851 29 -1 1 1 3.7678 23.5932 56 1 1 1 3.4167 26.0584 172 2 0 1 3.2241 27.6452 219 0 0 2 2.9619 30.1474 816 -2 0 2 2.7113 33.0095 181 0 2 0 2.6195 34.2019 476 -1 1 2 2.5966 34.5134 511 3 1 0 2.5439 35.2514 999 -3 1 1 2.4985 35.9131 38 0 2 1 2.3957 37.5102 55 1 1 2 2.3652 38.0133 862 2 0 2 2.2535 39.9750 455 2 2 0 2.2461 40.1127 296 -4 0 1 2.1927 41.1336 307 -2 2 1 2.1744 41.4939 503 -3 1 2 2.1183 42.6459 27 2 2 1 2.0330 44.5288 250 0 0 3 1.9746 45.9205 3 0 2 2 1.9622 46.2274 10 -4 0 2 1.9498 46.5392 283 -2 0 3 1.9498 46.5392 283 4 0 1 1.9285 47.0843 69 -2 2 2 1.8839 48.2684 561 -1 1 3 1.8791 48.3985 335 3 1 2 1.7841 51.1582 35 1 3 0 1.7124 53.4646 95 -3 1 3 1.7083 53.6021 263 2 2 2 1.7083 53.6021 263 4 2 0 1.6768 54.6950 143 -1 3 1 1.6623 55.2126 12 5 1 0 1.6564 55.4243 47 -4 0 3 1.6328 56.2957 125 1 3 1 1.6284 56.4633 84 4 0 2 1.6120 57.0882 69 0 2 3 1.5765 58.4966 110 -5 1 2 1.5765 58.4966 110 -4 2 2 1.5641 59.0080 123 -2 2 3 1.5641 59.0080 123 4 2 1 1.5530 59.4703 9 5 1 1 1.5232 60.7568 16 -1 3 2 1.5079 61.4373 4 3 3 0 1.4974 61.9167 81 -2 0 4 1.4948 62.0359 70 -3 3 1 1.4880 62.3524 20 -6 0 1 1.4810 62.6809 116 0 0 4 1.4810 62.6809 116 1 3 2 1.4583 63.7689 59 6 0 0 1.4550 63.9311 54 -1 1 4 1.4509 64.1338 27 3 1 3 1.4441 64.4692 3 -6 0 2 1.4213 65.6336 6 3 3 1 1.4180 65.8051 23 2 2 3 1.4137 66.0308 19 -5 1 3 1.4047 66.5074 6 -3 3 2 1.3944 67.0655 4 -3 1 4 1.3879 67.4210 92 -4 2 3 1.3857 67.5446 50 4 2 2 1.3729 68.2589 1 1 1 4 1.3660 68.6528 1 -4 0 4 1.3557 69.2484 3 6 0 1 1.3527 69.4246 26 5 1 2 1.3428 70.0067 24 4 0 3 1.3390 70.2364 14 2 0 4 1.3253 71.0704 2 -1 3 3 1.3191 71.4537 6 0 4 0 1.3097 72.0463 78 -6 2 1 1.2892 73.3809 36 0 2 4 1.2892 73.3809 36 6 2 0 1.2719 74.5433 103 1 3 3 1.2697 74.6993 59 -3 3 3 1.2559 75.6591 4 -6 2 2 1.2493 76.1349 16 -5 3 1 1.2438 76.5287 2 -2 4 1 1.2416 76.6904 3 -7 1 1 1.2360 77.1032 2 -5 1 4 1.2233 78.0491 12 6 0 2 1.2147 78.7082 1 2 4 1 1.2132 78.8259 1 7 1 0 1.2132 78.8259 1 -7 1 2 1.2066 79.3404 33 -4 2 4 1.2040 79.5498 22 -5 3 2 1.2005 79.8242 57 0 4 2 1.1979 80.0388 38 3 1 4 1.1937 80.3753 65 0 0 5 1.1848 81.1061 2 2 2 4 1.1826 81.2878 4 -2 4 2 1.1794 81.5566 23 5 3 1 1.1765 81.7988 19 5 1 3 1.1663 82.6646 1 -6 0 4 1.1581 83.3872 30 -3 1 5 1.1526 83.8743 15 7 1 1 1.1462 84.4478 6 -1 3 4 1.1422 84.8143 22 -4 0 5 1.1389 85.1170 15 3 3 3 1.1389 85.1170 15 -7 1 3 1.1352 85.4623 8 2 4 2 1.1324 85.7234 33 4 0 4 1.1267 86.2559 2 -4 4 1 1.1244 86.4785 11 -5 3 3 1.1193 86.9763 8 -8 0 1 1.1129 87.5981 5 -3 3 4 1.1107 87.8180 46 6 2 2 1.1020 88.6900 1 1 3 4 1.0994 88.9603 1 -8 0 2 1.0963 89.2717 27 0 4 3 1.0915 89.7766 3 2 0 5 1.0904 89.8856 2 |
3楼2014-08-08 20:31:48
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
- 红花: 107
- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
★ ★ ★ ★ ★
sunshineyulu: 金币+5, ★★★很有帮助 2014-08-09 14:23:26
sunshineyulu: 金币+5, ★★★很有帮助 2014-08-09 14:23:26
|
Card Information Names: Sodium Hydrogen Carbonate Nahcolite, syn Formula: Na H C O3 PDF Number: 000-15-0700 Quality: star Subfiles: inorganic mineral CP EDU FOR PHR Cell and Symmetry Information System: monoclinic Space Group: P21/n (no. 14) a: 7.475 b: 9.686 c: 3.481 b: 93.38 Density (Dm): 2.238 Density (Dx): 2.217 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54056 Instrument(d): Guinier Cut Off: 50.0 Instrument(I): unknown I type: unknown I/Icor: 0.30 Comments and Additional Information Optical: A=1.378, B=1.500, Q=1.584, Sign=-, 2V=75 degrees Colour: Colorless, white, gray, light brown General: Other data 00-021-1119. Source: Optical data on specimen from Searles Lake, San Bernadino County, California, USA. Lines: Plus 11 additional reflections to 1.522. Pattern: To replace 00-021-1119. Pattern: See ICSD 18183 (PDF 01-072-1663); See ICSD 23868 (PDF 01-073-1390); See ICSD 26933 (PDF 01-074-1203). Literature References General: de Wolff, P., Technisch Physische Dienst,Delft, The Netherlands. ICDD Grant-in-Aid ( ) Optical: Dana's System of Mineralogy, 7th Ed. II 134 ( ) Peak Data Wavelength 1.5406 used to convert d to 2theta PeakList h k l d 2theta I 1 1 0 5.9100 14.9779 16 0 2 0 4.8400 18.3150 25 1 2 0 4.0600 21.8734 4 2 0 0 3.7310 23.8293 4 2 1 0 3.4820 25.5611 30 0 1 1 3.2710 27.2407 8 -1 0 1 3.2240 27.6457 8 1 0 1 3.0820 28.9466 25 -1 1 1 3.0590 29.1690 35 1 3 0 2.9630 30.1361 20 2 2 0 2.9560 30.2092 70 1 1 1 2.9360 30.4199 100 0 2 1 2.8240 31.6574 1 -1 2 1 2.6840 33.3556 30 1 2 1 2.6000 34.4664 100 -2 1 1 2.5300 35.4512 1 2 3 0 2.4420 36.7735 1 3 1 0 2.4090 37.2957 4 2 1 1 2.3940 37.5381 2 0 3 1 2.3650 38.0160 4 -2 2 1 2.3050 39.0451 30 3 2 0 2.2120 40.7579 40 -3 0 1 2.0800 43.4716 4 -3 1 1 2.0350 44.4836 35 2 4 0 2.0310 44.5759 4 0 4 1 1.9870 45.6179 8 3 0 1 1.9690 46.0588 18 -1 4 1 1.9360 46.8904 12 -3 2 1 1.9130 47.4886 6 1 4 1 1.9040 47.7270 20 1 5 0 1.8750 48.5122 6 4 0 0 1.8660 48.7614 8 4 1 0 1.8320 49.7271 1 3 2 1 1.8230 49.9894 1 -2 4 1 1.7790 51.3143 6 0 0 2 1.7370 52.6490 12 2 5 0 1.7190 53.2434 2 0 1 2 1.7100 53.5459 2 -1 1 2 1.6890 54.2659 10 |
4楼2014-08-08 20:33:31
sunshineyulu
金虫 (小有名气)
- 应助: 0 (幼儿园)
- 金币: 2385.3
- 帖子: 85
- 在线: 99.9小时
- 虫号: 2049812
- 注册: 2012-10-08
- 性别: MM
- 专业: 环境工程
5楼2014-08-09 14:23:12