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huaxiashizhe

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[求助] 求Y4O5Cl2的XRD图谱已有1人参与

有哪位大神知道Y4O5Cl2的XRD图谱，请问需要怎么才能合成。

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XRD&SEM qq2978260443

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【答案】应助回帖

Name and formula

Reference code: 00-023-0731

Compound name: Yttrium Oxide Chloride

Empirical formula: Cl2O5Y4
Chemical formula: Y4O5Cl2

Crystallographic parameters

Crystal system: Unknown

RIR: -

Subfiles and quality

Subfiles: Inorganic
Quality: Low precision (O)

Comments

Creation Date: 1970/1/1
Modification Date: 1970/1/1
Sample Preparation: Sample obtained by direct synthesis of YOCl and Y2O3  at 800? to 1000 C with traces of moisture.

References

Primary reference: Markovskii et al., Russ. J. Inorg. Chem. (Engl. Transl.), 14, 7, (1969)

Peak list

No. h k l    d [A]    2Theta[deg] I [%]
  1                   5.78000 15.317    85.0
  2                   3.81000 23.329    25.0
  3                   3.61000 24.641    4.0
  4                   3.21000 27.769    70.0
  5                   3.18000 28.037    20.0
  6                   2.89000 30.917    4.0
  7                   2.79000 32.054    100.0
  8                   2.71000 33.027    60.0
  9                   2.59000 34.605    40.0
10                   2.51000 35.744    5.0
11                   2.31000 38.958    25.0
12                   2.25000 40.041    2.0
13                   2.14000 42.195    6.0
14                   2.13000 42.402    4.0
15                   2.12000 42.612    4.0
16                   2.10000 43.038    2.0
17                   2.01000 45.068    30.0
18                   1.97400 45.937    4.0
19                   1.92700 47.124    20.0
20                   1.90000 47.835    20.0
21                   1.85200 49.156    2.0
22                   1.82800 49.845    10.0
23                   1.78000 51.285    20.0
24                   1.71900 53.245    10.0
25                   1.70400 53.751    10.0
26                   1.64700 55.770    25.0
27                   1.60400 57.402    4.0
28                   1.58600 58.115    15.0
29                   1.51700 61.032    25.0
30                   1.47500 62.965    4.0
31                   1.46800 63.300    2.0
32                   1.44500 64.428    2.0
33                   1.43400 64.982    2.0
34                   1.42100 65.651    4.0
35                   1.39200 67.198    8.0
36                   1.38100 67.805    4.0
37                   1.35300 69.407    4.0
38                   1.29500 73.000    4.0
39                   1.28300 73.796    2.0
40                   1.26700 74.886    2.0
41                   1.26000 75.374    2.0
42                   1.25600 75.656    6.0

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