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虫号: 2350259
注册: 2013-03-15
专业: 分析仪器与试剂

[求助] 急急急求大神帮忙配制电解液：酒石酸钾钠，cdso4,seo2！！！

做量子敏化太阳电池求大神帮忙配制电解液：含酒石酸钾钠，cdso4,seo2！！！感觉读不出配制的顺序和注意事项啊，求指导！！
2.2. Deposition of CdSe nanoparticles into TiO2 NTAs
The CdSe nanoparticles were deposited into TiO2 NTAs by cyclic
voltammetry electrochemical deposition with 2 cyclic voltammetry
cycles. The deposition potential was chosen in the range
of
−0.4 V and
−1.0 V (vs. SCE). The electrodeposition of CdSe was
performed in a conventional three-electrode system with a TiO2
NTAs as the working electrode, a Pt foil as the counter electrode,
and a saturated calomel electrode (SCE) as the reference
electrode. The electrolyte solution was prepared by mixing 0.1 M
CdCl2·5H2O, 0.01 M C4O6H4KNa (potassium sodium tartrate) and
different concentration of SeO2 in 100 ml of deionized water, followed
by adjusting the pH value to 3 by dropwise addition of 1 M
solution of HCl. After electrochemical deposition, the samples were
thoroughly rinsed by distilled water and then annealed at 350 ◦C in
vacuum atmosphere for 60 min. The samples were noted as S0, S2,
S4, S6, S8, S10 according to the concentration of SeO2 (0, 2, 4, 6, 8,
10 mM).

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