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[求助]
求助微谱数据，谢谢大家 已有1人参与
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0.53,56.0,94.0,98.9,103.5,104.1,121.3,139.1,147.6,157.6,161.2,163.9,164.2,182.1 溶剂 CDCL3 我也不清楚0.53的碳信号是不是化合物的信号，但这个信号又比较强，大家要是不怕麻烦帮我把0.53的信号去掉也查查看，谢谢大家哦 新手金币少 给的不多，希望谅解 谢谢大家 |
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周玲4340
铜虫 (小有名气)
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【答案】应助回帖
★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
辣笔v小新: 金币+1, 鼓励应助交流 2014-03-25 06:44:22
twzdd2014: 金币+5, ★★★很有帮助, 非常感谢你的帮助 可是结果好像对不上 2014-03-27 18:22:37
感谢参与，应助指数 +1
辣笔v小新: 金币+1, 鼓励应助交流 2014-03-25 06:44:22
twzdd2014: 金币+5, ★★★很有帮助, 非常感谢你的帮助 可是结果好像对不上 2014-03-27 18:22:37
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查询结果：共查到20个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . 1-allyl-6-aminopyrimidine-2,4(1H,3H)-dione C7H9N3O2 相似度:57.1% Journal of Heterocyclic Chemistry 2009 46 79-83 Synthetic strategy toward 1,9-functionalized pyrido[2,3-d:6,5-d']dipyrimidine-2,4,6,8-tetrones Gabor Borzsonyi,Rachel L. Beingessner and Hicham Fenniri Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 2,4-dimethyl-cis-3,5-diphenyl-[1,4]-oxazepan-7-one C19H21NO2 相似度:57.1% Indian Journal of Chemistry Section B 2005 44B 2527-2531 A study on the reactivity of 1,3-dimethyl-2,6-diphenyl-4-piperidone : Synthesis of some novel heterocycles Padmavathi,V; Reddy,T V Ramana; Reddy,K Audisesha; Padmaja,A; Reddy,D Bhaskar Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 4-ethylidene-1-pyrazoline 相似度:57.1% Canadian Journal of Chemistry 1978 56 992-997 Synthesis and 1H and 13C nuclear magnetic resonance spectra of some 4-alkylidene-1-pyrazolines and alkylidenecyclopropanes Robert J. Crawford, Hirokazu Tokunaga, Louis M. H. C. Schrijver, Jacky C. Godard, Thomas Nakashima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . E-3,3-dideuterio-4-ethylidene-1-pyrazoline 相似度:57.1% Canadian Journal of Chemistry 1978 56 992-997 Synthesis and 1H and 13C nuclear magnetic resonance spectra of some 4-alkylidene-1-pyrazolines and alkylidenecyclopropanes Robert J. Crawford, Hirokazu Tokunaga, Louis M. H. C. Schrijver, Jacky C. Godard, Thomas Nakashima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . E-4-ethylidene-3-methyl-1-pyrazoline C6H10N2 相似度:57.1% Canadian Journal of Chemistry 1978 56 992-997 Synthesis and 1H and 13C nuclear magnetic resonance spectra of some 4-alkylidene-1-pyrazolines and alkylidenecyclopropanes Robert J. Crawford, Hirokazu Tokunaga, Louis M. H. C. Schrijver, Jacky C. Godard, Thomas Nakashima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . (2S,3R,5R,6S)-2,3,5,6-tetrahydroxy-4-[2-[4-hydroxyphenyl)acetyl]oxycyclohexyl-2-(4-hydroxy-phenyl)-acetate C22H24O10 相似度:55.5% Phytochemistry 1999 51 991-994 Eudesmanolides and inositol derivatives from Taraxacum linearisquameum C. Zidorn, E.P. Ellmerer-Muller, H. Stuppner Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 4α-hydroxymenthol C10H20O2 相似度:50% Journal of Natural Products 1998 61 1340-1342 Fungal Transformation of (1R, 2S, 5R)-(-)-Menthol by Cephalosporium aphidicola Atta-ur-Rahman, Muhammad Yaqoob, Afgan Farooq, Shazia Anjum, Fahim Asif, and M. Iqbal Choudhary Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . (-)-(1S,3R,4S,6S)-6-hydroxymenthol C10H20O2 相似度:50% Natural Product Research 2003 17 307-311 Biopreparation of (-)-(1S,3R,4S,6S)- 6-Hydroxymenthol and (-)-(1S,3R,4S)-1-Hydroxymenthol from l-Menthol by Rhizoctonia Solani AG-1-IA and IB Mitsuo Miyazawa; Hideki Kawazoe; Mitsuro Hyakumachi Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 4-(3,4-dihydroxy-(E)-1-pentenyl)-oxazole C8H11NO3 相似度:50% Journal of Natural Products 1995 Vol 58 1605-1607 MR-93A, a New Oxazole from Trichoderma harzianum KCTC 0114BP Choonghwan Lee, Myungchul Chung, Hojae Lee, Yunghee Kho, Hiroyuki Koshino Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . (3R)-3-{[(tert-Butyl)(dimethyl)silyl]oxy}hex-5-en-1-ol C12H26NaO2Si 相似度:50% Helvetica Chimica Acta 2011 94 1102-1107 Total Synthesis of Leiocarpin C and (+)-Goniodiol via an Olefin Cross-Metathesis Protocol Palakodety Radha Krishna and Munagala Alivelu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . evodiamine 相似度:50% Journal of Shenyang Pharmaceutical University 2005 22 12-14 Chemical constituents of Evodia rutaecarpa (Juss.) Benth. ZHANG Qi-hui, GAO Hui-yuan, WU Li-jun, ZHANG Lei Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . (E)-5-(3S,4R,5-Trihydroxy-1-pentylidene)imidazolidine-2,4-dione C8H12N2O5 相似度:50% Bioorganic & Medicinal Chemistry 1998 6 911-923 Inhibitors of glycogen phosphorylase b: synthesis, biochemical screening, and molecular modeling studies of novel analogues of hydantocidin Yankanagouda S. Agasimundin, Mary W. Mumper, Ramachandra S. Hosmane Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . (1'E)-erythro-4-(3',4'-dihydroxypentenyl)oxazole C8H11O3N 相似度:50% Bioscience, Biotechnology, and Biochemistry 1997 61 1428-1433 Two Oxazolyl Compounds and a Monosubstituted α-Pyrone as Free-radical Scavengers Isolated from a Fungus Yasujiro MORIMITSU, Akira HIROTA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . ethyl 2-diazo-3-oxohexanoate 相似度:50% Russian Journal of Organic Chemistry 2007 43 607-614 Chemistry of diazocarbonyl compounds: XXX. Development of a synthetic approach to pyridazine structure via wittig reaction of fluoroalkyl-containing diazo keto esters S. V. Galiullina, V. M. Zakharova, G. P. Kantin and V. A. Nikolaev Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . methyl 2,6-dideoxy-3-C-methyl-α-D-ribo-hexopyranoside(methyl α-D-mycaroside) C8H16O4 相似度:50% The Journal of Antibiotics 2001 54 211-219 Isolation and Structure Elucidation of Vicenistatin M, and Importance of the Vicenisamine Aminosugar for Exerting Cytotoxicity of Vicenistatin YOSHITAKA MATSUSHIMA,TAKUYA NAKAYAMA,MASAKI FUJITA,RENUKA BHANDARI,TADASHI EGUCHI,KAZUTOSHI SHINDO and KATSUMI KAKINUMA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . methyl β-decilonitroside 相似度:50% The Journal of Antibiotics 1990 43 54-61 THE ABSOLUTE CONFIGURATION OF DECILONITROSE, A SUGAR COMPONENT OF DECILORUBICIN, IS UNDOUBTEDLY 2, 3, 6-TRIDEOXY-3-C-METHYL-3-NITRO-L-RIBO-HEXOPYRANOSE YOSHIO NISHIMURA, KIYOTO ISHII, SHINICHI KONDO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . melanoxadin C8H11NO3 相似度:50% The Journal of Antibiotics 1995 48 1052-1054 A New Melanin Biosynthesis Inhibitor, Melanoxadin from Fungal Metabolite by Using the Larval Haemolymph of the Silkworm, Bombyx mori RYUJU HASHIMOTO, SENJI TAKAHASHI, KUNIKATSU HAMANO, AKIRA NAKAGAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . methyl 2,3,6-trideoxy-3-C-methyl-3-nitro-β-L-ribo-hexopyranoside 相似度:50% The Journal of Antibiotics 1983 36 454-456 DECILONITROSE AND 4-O-SUCCINYL-L-DIGINOSE, SUGAR COMPONENTS OF DECILORUBICIN KIYOTO ISHII, YOSHIO NISHIMURA, SHINICHI KONDO, HAMAO UMEZAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . (2S,3S)-2-allyloxypent-4-en-3-ol 相似度:50% European Journal of Organic Chemistry 2002 2002 2649-2655 Stereoselective Synthesis of the Naturally Occurring Lactones (−  -Osmundalactone and (−-Muricatacine Using Ring-Closing MetathesisMiguel Carda, Santiago Rodríguez, Florenci González, Encarnación Castillo, Alicia Villanueva and J. Alberto Marco Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . (-)-(1S,3R,4S,6S)-6-Hydroxymenthol 相似度:50% Journal of Agricultural and Food Chemistry 2003 51 1880-1883 Lytic Activity of l-Menthol Derivatives against the Snow Blight Disease Fungus, Micronectriella nivalis Mitsuo Miyazawa, Hideki Kawazoe, Yuji Sumi, and Mitsuro Hyakumachi Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
2楼2014-03-24 19:55:36