| 查看: 2113 | 回复: 2 | ||
[求助]
投稿ACTAE，检测没有AB错误，上传FCF出现了错误！急急急求指导修改！！ 已有2人参与
|
|
投稿之前检测过，没有AB类错误。上传FCF文件之后，出现以下错误，求指导修改！ Alert level B Crystal system given = triclinic PLAT921_ALERT_1_B R1 in the CIF and FCF Differ by ............... -0.0136 Check PLAT922_ALERT_1_B wR2 in the CIF and FCF Differ by ............... -0.0346 Check PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 3 Check Alert level C PLAT761_ALERT_1_C CIF Contains no X-H Bonds ...................... Please Check PLAT762_ALERT_1_C CIF Contains no X-Y-H or H-Y-H Angles .......... Please Check PLAT910_ALERT_3_C Missing # of FCF Reflections Below Th(Min) ..... 6 Why ? PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 Why ? PLAT923_ALERT_1_C S values in the CIF and FCF Differ by ....... -0.375 Check PLAT926_ALERT_1_C Reported and Calculated R1 Differ by ......... -0.0022 Check PLAT927_ALERT_1_C Reported and Calculated wR2 Differ by ......... -0.0033 Check Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT164_ALERT_4_G Nr. of Refined C-H H-Atoms in Heavy-Atom Struct. 14 Note PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 985 Note PLAT982_ALERT_1_G The Zn-f'= 0.312 Deviates from the IT-value 0.284 PLAT983_ALERT_1_G The Zn-f"= 1.467 Deviates from the IT-Value 1.430 |
回复此楼» 猜你喜欢
武汉纺织大学技术研究院招收化学、生物、材料、纺织、机械等专业调剂生
已经有0人回复
-
台州学院有序多孔材料团队化学、材料与化工硕士招生，请速联系！
已经有0人回复
-
无机化学论文润色/翻译怎么收费?
已经有59人回复
-
首都师范大学化学系田洋课题组专硕招调剂生
已经有10人回复
-
广州大学大湾区环境研究院环境大分子材料研究所王平山教授团队 2026年研究生招生简章
已经有0人回复
-
天津理工大学
已经有0人回复
-
台州学院有序多孔材料团队最后冲刺，同学们别错过哦，请速联系！
已经有0人回复
-
江西科技师范大学物理化学课题组接收调剂生，名额还有，速来
已经有0人回复
2楼2014-03-17 22:24:32
sunzan
至尊木虫 (知名作家)
- 应助: 210 (大学生)
- 金币: 41157.5
- 散金: 252
- 红花: 69
- 帖子: 5718
- 在线: 932.5小时
- 虫号: 1125699
- 注册: 2010-10-18
- 性别: GG
- 专业: 配位化学
3楼2014-03-18 08:24:54
