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Nb2O5xrd的表征问题
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一个审稿意见：In the XRD section, could the authors comment on the board peak at ~30 degrees? It appears to the reviewer that the crystallnity of the hierarchical structure is somehow low without proper post-annealing process. A significant part of the structure might be still amorphous or hydrated. In addition, the dominant crystal structure appears to be more like pseudo-hexagonal rather than orthorhombic although both structures have very similar XRD diffraction patterns. The authors should do more detail analysis and clarify the difference from pseudo-hexagonal structure. 我想问一下，对于较宽的峰，除了归结于晶体粒径小以外，是否有别的解释；另外，这个pseudo-hexagonal（伪六角）该怎么解释，我在jade中只能找到hexagonal，pseudo-hexagonal和hexagonal是一回事吗，差别是什么？谢谢 |
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