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Nb2O5xrd的表征问题
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一个审稿意见:In the XRD section, could the authors comment on the board peak at ~30 degrees? It appears to the reviewer that the crystallnity of the hierarchical structure is somehow low without proper post-annealing process. A significant part of the structure might be still amorphous or hydrated. In addition, the dominant crystal structure appears to be more like pseudo-hexagonal rather than orthorhombic although both structures have very similar XRD diffraction patterns. The authors should do more detail analysis and clarify the difference from pseudo-hexagonal structure. 我想问一下,对于较宽的峰,除了归结于晶体粒径小以外,是否有别的解释;另外,这个pseudo-hexagonal(伪六角)该怎么解释,我在jade中只能找到hexagonal,pseudo-hexagonal和hexagonal是一回事吗,差别是什么?谢谢 |
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2014-03-02 23:28
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