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¹§Ï²±»ÊÕ¼ÁË: Accession number: 20140117165847 Title: Synthesis of C5 petroleum resin with light color and high softening point Authors: Wang, Guoqiang1; Zhang, Wanxi1; Liang, Jicai1; Chen, Guangyi1; Wei, Zhiyong1; Zhang, Long2 Email author zhanglongzhl@163.com Author affiliation: 1 School of Automotive Engineering, Dalian University of Technology, Dalian 116024, China 2 Jilin Provincial Engineering Laboratory for the Complex Utilization of Biomass and Petroresources, Changchun University of Technology, Changchun 130012, China Corresponding author: Zhang, L. (zhanglongzhl@163.com) Source title: Gaofenzi Cailiao Kexue Yu Gongcheng/Polymeric Materials Science and Engineering Abbreviated source title: Gaofenzi Cailiao Kexue Yu Gongcheng Volume: 29 Issue: 10 Issue date: October 2013 Publication year: 2013 Pages: 1-4 Language: Chinese ISSN: 10007555 CODEN: GCKGEI Document type: Journal article (JA) Publisher: Chengdu University of Science and Technology, 24 South Section 1, Yihuan Rd., Chengdu, 610065, China Abstract: The high softening point resin was preparation by cationic polymerization. The influences of the solvent, solvent concentration, reaction temperature, and the catalyst concentration on the polymerization were investigated. Bitumen softening point tester, gel permeation chromatographer, NMR spectrometer, colorimeter and FT-IR spectrometer were used to measure the softening point, molecular weight, cyclization degree and structure of resins. The softening point of resin is about 50¡ãC higher using dichloromethane as solvent than using toluene. The highest softening point of the 1, 3-pentadiene resin produced is 139¡ãC, which is the highest among current reports. The softening point of the resin increases with the increase of reaction temperature. Effect of amount of catalyst on the softening point is very small. Number of references: 6 Main heading: Resins Controlled terms: Catalysts - Cationic polymerization - Color - Dichloromethane - Organic solvents - Solvents - Spectrometers Uncontrolled terms: 1 ,3-pentadiene - Catalyst concentration - Light color - NMR spectrometer - Petroleum resins - Reaction temperature - Softening points - Solvent concentration Classification code: 815.2 Polymerization - 815.1.1 Organic Polymers - 804.1 Organic Compounds - 804 Chemical Products Generally - 803 Chemical Agents and Basic Industrial Chemicals - 801 Chemistry - 741.1 Light/Optics Database: Compendex Compilation and indexing terms, © |
2Â¥2014-02-23 18:38:19
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3Â¥2014-02-23 18:38:27













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