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ai532521木虫 (小有名气)
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[求助]
微谱解析，万分感谢已有1人参与
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溶剂：氘代甲醇 化学位移：27.55,27.67,27.74,28.18,29.17,29.21,37.25,49.99,52.49,56.87,67.78,71.61,75.37,77.12,78.09,78.19,102.56,125.51,126.25,128.96,138.34,166.06,202.20 |
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ai532521: 金币+15, ★★★很有帮助, 溶剂影响不大，万分感谢 2014-01-10 21:27:49
感谢参与，应助指数 +1
ai532521: 金币+15, ★★★很有帮助, 溶剂影响不大，万分感谢 2014-01-10 21:27:49
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溶剂为CD3OD时查到以下结果 查询结果：共查到54个化合物(查询结果仅供参考) 1 . eriojaposide A C24H38O11 相似度:66.6% Journal of Natural Products 2001 64 737-740 Megastigmane Glycosides and an Acylated Triterpenoid from Eriobotrya japonica Hideyuki Ito,Eri Kobayashi, Shu-Hua Li, Tsutomu Hatano, Daigo Sugita, Naoki Kubo, Susumu Shimura, Yoshio Itoh, and Takashi Yoshida Structure 13C NMR 碳谱模拟图 2 . 9-hydroxy-4,7-megastigmadien-3-one 9-O-[α-L-rabinopyranosyl-(1→6)-β-D-glucopyranoside] 相似度:66.6% Phytochemistry 1997 45 777-779 Megastigmane glycosides from Lonicera gracilipes var. Glandulosa Noriko Matsuda, Kyouko Isawa, Masao Kikuchi Structure 13C NMR 碳谱模拟图 3 . 3-oxo-α-ionyl-9-O-β-D-apiofuranosyl-(1→6)-β-D-glucopyranoside C24H38O11 相似度:66.6% Journal of Natural Products 1992 Vol 55 1025 Plant Metabolites. New Sesquiterpene and Ionone Glycosides from Eriobotrya japonica Nunziatina De Tommasi, Rita Aquino, Francesco De Simone, Cosimo Pizza Structure 13C NMR 碳谱模拟图 4 . ficumegasoside C24H38O11 相似度:66.6% Bioorganic & Medicinal Chemistry Letters 2011 21 633-637 Antioxidant activity of a new C-glycosylflavone from the leaves of Ficus microcarpa Phan Van Kiem, Nguyen Xuan Cuong, Nguyen Xuan Nhiem, Vu Kim Thu, Ninh Khac Ban,Chau Van Minh, Bui Huu Tai, Truong Nam Hai, Sang Hyun Lee, Hae Dong Jang, Young Ho Kim Structure 13C NMR 碳谱模拟图 5 . (4Z,6R,7E,9R)-megastigma-4,7-dien-9-ol-3-one 9-O-α-L-arabinofuranosyl-(1''→ 6')-β-D-glucopyranoside C24H38O11 相似度:66.6% Journal of Natural Medicines 2012 66 664-670 Three new aliphatic glycosides from the leaves of Antidesma japonicum Sieb. et Zucc. Ayumi Iha, Katsuyoshi Matsunami, Hideaki Otsuka, Masatoshi Kawahata and Kentaro Yamaguchi, et al. Structure 13C NMR 碳谱模拟图 6 . (6R,7E,9R)-9-hydroxy-4,7-megastigmadien-3-one-9-O-[α-L-arabinopyranosyl-(1→ 6)-β-D-glucopyranoside 相似度:66.6% China Journal of Chinese Materia Medica 2011 36 1305-1310 Chemical constituents of aerial parts ofGelsemium elegans ZHANG, Qiuping, ZHANG, Binfeng, CHOU, Guixin, WANG, Zhengtao Structure 13C NMR 碳谱模拟图 7 . dearabinosyl pneumonanthoside 相似度:65.2% Phytochemistry 1999 50 1219-1223 Norterpenoid and sesquiterpenoid glucosides from Juniperus phoenicea and Galega officinalis Yves Champavier, Gilles Comte, Joseph Vercauteren, Daovy P. Allais,Albert J. Chulia Structure 13C NMR 碳谱模拟图 8 . (6R,7E,9R)-9-hydroxymegastigma-4,7-dien-3-one-9-O-β-D-glucopyranoside C19H30O7 相似度:65.2% Phytochemistry 1999 50 859-862 Megastigmane glycosides from seeds of Trifolium alexandrinum Khaled M. Mohamed, Mahmoud H. Mohamed, Kazuhiro Ohtani, Ryoji Kasai,Kazuo Yamasaki Structure 13C NMR 碳谱模拟图 9 . compound 3x C19H30O7 相似度:65.2% Phytochemistry 1994 36 1465-1467 A sterol with an unusual side chain from Anoectochilus koshunensis Aiko Ito, Keiko Yasumoto, Ryoji Kasai, Kazuo Yamasaki Structure 13C NMR 碳谱模拟图 10 . (6R,9R)-3-oxo-α-ionol β-D-glucopyranoside 相似度:65.2% Phytochemistry 1992 31 1649-1652 Two diastereomeric 3-oxo-α-ionol β-d-glucosides from raspberry fruit Anni Pabst, Denis Barron, Etienne Sémon, Peter Schreier Structure 13C NMR 碳谱模拟图 11 . (6S,9R)-3-oxo-α-ionol-9-O-β-D-glucopyranoside 相似度:65.2% Chinese Traditional and Herbal Drugs 2008 39 648-651 Chemical components from Dryopteris fragrans and their cytotoxicity ZHANG Yan-long; FU Hai-yan; ZHANG Ying-ying; SONG Qing-yu; XU Wen-hua; KUANG Hai-xue Structure 13C NMR 碳谱模拟图 12 . (6R,7E,9R)-9-hydroxy-megastigman-4,7-dien-3-one-9-O-β-D-glucopyranoside 相似度:65.2% Pharmazie 2003 58 363-364 Megastigmane and flavone glycosides from Acanthus ilicifolius Jun Wu - Si Zhang - Qiang Xiao - Qingxin Li - Jianshe Huang - Lijuan Long - Liangmin Huang Structure 13C NMR 碳谱模拟图 13 . (6R,9R)-3-oxo-α-ionol-9-O-β-D-glucopyranoside 相似度:65.2% Archives of Pharmacal Research 2008 31 1094-1097 Chemical constituents from the flower of Datura metel L. Hai-xue Kuang, Bing-you Yang, Yong-gang Xia and Wei-sheng Feng Structure 13C NMR 碳谱模拟图 14 . compound 11 相似度:65.2% Journal of Natural Medicines 2012 66 664-670 Three new aliphatic glycosides from the leaves of Antidesma japonicum Sieb. et Zucc. Ayumi Iha, Katsuyoshi Matsunami, Hideaki Otsuka, Masatoshi Kawahata and Kentaro Yamaguchi, et al. Structure 13C NMR 碳谱模拟图 15 . (6R,7E,9R)-9-Hydroxy-megastigma-4,7-dien-3-one 9-O-β-D-glucopyranoside C19H30O7 相似度:65.2% Chemistry of Natural Compounds 2012 48 346-349 Megastigmane O-glucopyranosides from Litsea glutinosa Yun-Song Wang, Zhen Liao, Hong-Kun Zhu, Xiao-Fei Feng and Kun-Ming-Jiang, et al. Structure 13C NMR 碳谱模拟图 16 . (+)-3-oxo-α-ionyl-O-β-D-glucopyranoside 相似度:65.2% Chinese Traditional and Herbal Drugs 2012 43 1699-1703 Studies on chemical constituents from roots of Pterospermum heterophyllum WANG Meng-meng; LI Shuai; LUO Guang-ming; CUI Bao-song; QIAO Yong-qi; LIU Jia-bao Structure 13C NMR 碳谱模拟图 17 . eriojaposide B C25H40O11 相似度:64% Journal of Natural Products 2001 64 737-740 Megastigmane Glycosides and an Acylated Triterpenoid from Eriobotrya japonica Hideyuki Ito,Eri Kobayashi, Shu-Hua Li, Tsutomu Hatano, Daigo Sugita, Naoki Kubo, Susumu Shimura, Yoshio Itoh, and Takashi Yoshida Structure 13C NMR 碳谱模拟图 18 . Cuneatoside C24H38O12 相似度:62.5% Journal of Asian Natural Products Research 2006 8 747-751 Cuneatoside, a new megastigmane diglycoside from Erythroxylum cuneatum Blume T. KANCHANAPOOM, A. SIRIKATITHAM, H. OTSUKAk and S. RUCHIRAWAT Structure 13C NMR 碳谱模拟图 19 . (6R,9S)-megastigman-3-one-4,7-ene-9-ol-9-O-α-L-arabinofuranosyl-(1→6)-β-D-glucopyranoside 相似度:62.5% Natural Product Research and Development 2010 22 731-735 Studies on the Chemical Constituents of Euphorbia helioscopia HE Jiang-bo;LIU Guang-ming; CHENG Yong-xian Structure 13C NMR 碳谱模拟图 20 . (6R,9R)-3-oxo-α-ionol-9-O-β-D-glucopyranosyl(1→2)-β-D-glucopyranoside C25H40O12 相似度:60% Natural Product Research 2011 Vol. 25, No. 13 1219-1223 Two new 3-oxo-α-ionol glucosides from Urtica laetevirens Maxim. Yuan Zhou, Bao-Min Feng, Li-Ying Shi, Hui-Guo Wang, Ling Tang and Yong-Qi Wang Structure 13C NMR 碳谱模拟图 21 . (6S,9R)-3-oxo-α-ionol-9-O-β-D-glucopyranosyl(1→2)-β-D-glucopyranoside C25H40O12 相似度:60% Natural Product Research 2011 Vol. 25, No. 13 1219-1223 Two new 3-oxo-α-ionol glucosides from Urtica laetevirens Maxim. Yuan Zhou, Bao-Min Feng, Li-Ying Shi, Hui-Guo Wang, Ling Tang and Yong-Qi Wang Structure 13C NMR 碳谱模拟图 22 . macarangioside E C26H34O11 相似度:58.3% Phytochemistry 2009 70 1277-1285 Absolute configuration of (+)-pinoresinol 4-O-[6''-O-galloyl]-β-D-glucopyranoside,macarangiosides E, and F isolated from the leaves of Macaranga tanarius Katsuyoshi Matsunami, Hideaki Otsuka, Kazunari Kondo, Takakazu Shinzato, Masatoshi Kawahata, Kentaro Yamaguchi, Yoshio Takeda Structure 13C NMR 碳谱模拟图 23 . trifostigmanoside II C24H38O11 相似度:58.3% Phytochemistry 1999 50 859-862 Megastigmane glycosides from seeds of Trifolium alexandrinum Khaled M. Mohamed, Mahmoud H. Mohamed, Kazuhiro Ohtani, Ryoji Kasai,Kazuo Yamasaki Structure 13C NMR 碳谱模拟图 24 . salvionoside A C24H38O11 相似度:58.3% Phytochemistry 1997 44 117-120 Megastigmane glycosides from Salvia nemorosa Yoshio Takeda, Hongjie Zhang, Takashi Matsumoto, Hideaki Otsuka, Yasushi Oosio, Gisho Honda, Mamoru Tabata, Tetsuro Fujita, Handong Sun, Ekrem Sezik, Erdem Yesilada Structure 13C NMR 碳谱模拟图 25 . foliasalacioside B2 C24H40O11 相似度:58.3% Heterocycles 2008 75 131-143 Megastigmane Glycosides from the Leaves of Salacia chinensis Seikou Nakamura, Yi Zhang, Yutana Pongpiriyadacha, Tao Wang, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 26 . leeaoside C24H40O11 相似度:58.3% Journal of Natural Medicines 2007 61 449-451 Leeaoside, a new megastigmane diglycoside from the leaves of Leea thorelii Gagnep Wiyada Kaewkrud, Hideaki Otsuka, Somsak Ruchirawat and Tripetch Kanchanapoom Structure 13C NMR 碳谱模拟图 27 . foliasalacioside B2 相似度:58.3% Journal of Natural Medicines 2012 66 664-670 Three new aliphatic glycosides from the leaves of Antidesma japonicum Sieb. et Zucc. Ayumi Iha, Katsuyoshi Matsunami, Hideaki Otsuka, Masatoshi Kawahata and Kentaro Yamaguchi, et al. Structure 13C NMR 碳谱模拟图 28 . (6R,7E,9R)-megastigma-4,7-dien-3-one 9,13-di-O-β-D-glucopyranoside C25H40O13 相似度:56.5% Chemical & Pharmaceutical Bulletin 2008 56(4) 610-611 Three New Glycosides from the Leaves of Hydrangea macrophylla subsp. serrata (THUNB.) MAKINO Masao KIKUCHI,Rie KAKUDA, Masafumi KIKUCHI, and Yasunori YAOITA Structure 13C NMR 碳谱模拟图 29 . (6R,9R)-bumenyl α-L-rhamnopyranosyl-(1→6)-β-D-gluco-pyranoside C25H42O11 相似度:56% Chinese Chemical Letters 2008 19 845-848 A new glycoside from the leaves of Neoalsomitra ntegrifoliola Dong Min Su, Jing Qu, You Cai Hu, Shi Shan Yu, Wen Zhao Tang, Yun Bao Liu, Shuang Gang Ma, De Quan Yu Structure 13C NMR 碳谱模拟图 30 . gusanlungionoside A C25H40O11 相似度:56% Journal of Natural Products 2011 74 1009-1014 Gusanlungionosides A-D, Potential Tyrosinase Inhibitors from Arcangelisia gusanlung Ling-Ling Yu, Wei-Cheng Hu, Gang Ding, Rong-Tao Li, Jian-He Wei, Zhong-Mei Zou, and Myeong-Hyeon Wang Structure 13C NMR 碳谱模拟图 31 . gusanlungionoside B C25H40O11 相似度:56% Journal of Natural Products 2011 74 1009-1014 Gusanlungionosides A-D, Potential Tyrosinase Inhibitors from Arcangelisia gusanlung Ling-Ling Yu, Wei-Cheng Hu, Gang Ding, Rong-Tao Li, Jian-He Wei, Zhong-Mei Zou, and Myeong-Hyeon Wang Structure 13C NMR 碳谱模拟图 32 . eleganoside A C24H40O11 相似度:54.1% Helvetica Chimica Acta 2011 94 1130-1138 Two New Megastigmane Glycosides and a New Iridoid Glycoside from Gelsemium elegans Qiu-Ping Zhang, Bin-Feng Zhang, Gui-Xin Chou, and Zheng-Tao Wang Structure 13C NMR 碳谱模拟图 33 . foliasalacioside B1 相似度:54.1% Helvetica Chimica Acta 2011 94 1130-1138 Two New Megastigmane Glycosides and a New Iridoid Glycoside from Gelsemium elegans Qiu-Ping Zhang, Bin-Feng Zhang, Gui-Xin Chou, and Zheng-Tao Wang Structure 13C NMR 碳谱模拟图 34 . guettardionoside C24H40O11 相似度:54.1% Journal of Natural Medicines 2011 65 364-369 A glycerol α-D-glucuronide and a megastigmane glycoside from the leaves of Guettarda speciosa L. Wen-Hu Cai ,Katsuyoshi Matsunami ,Hideaki Otsuka ,Takakazu Shinzato ,Yoshio Takeda Structure 13C NMR 碳谱模拟图 35 . 3β-hydroxy-α-ionol 9-O-β-D-apiofuranosyl-(1→6)-β-D-glucopyranoside C24H40O11 相似度:54.1% Journal of Agricultural and Food Chemistry 1996 44 1676-1681 Constituents of Cydonia vulgaris: Isolation and Structure Elucidation of Four New Flavonol Glycosides and Nine New α-Ionol-Derived Glycosides Nunziatina De Tommasi, Sonia Piacente, Francesco De Simone, and Cosimo Pizza Structure 13C NMR 碳谱模拟图 36 . debiloside A C19H30O8 相似度:52.1% Helvetica Chimica Acta 2006 Vol. 89 1422 Debilosides A–C: Three New Megastigmane Glucosides from Equisetum debile Xiao-Hong Xu, Chang-Heng Tan, Shan-Hao Jiang, and Da-Yuan Zhu Structure 13C NMR 碳谱模拟图 37 . jasminoside H C22H36O12 相似度:52.1% Journal of Natural Products 2008 71(6) 995-999 Pyronane Monoterpenoids from the Fruit of Gardenia jasminoides Quan Cheng Chen, UiJoung Youn, Byung-Sun Min, and KiHwan Bae Structure 13C NMR 碳谱模拟图 38 . 3-deoxy-MS-II C25H24O4 相似度:52.1% Journal of Natural Products 2004 67 454-456 Cytotoxic Compounds from Mundulea chapelieri from the Madagascar Rainforest Shugeng Cao, Jennifer K. Schilling, James S. Miller, Rabodo Andriantsiferana, Vincent E. Rasamison, and David G. I. Kingston Structure 13C NMR 碳谱模拟图 39 . byzantionoside B C19H32O7 相似度:52.1% Phytochemistry 1997 44 1335-1337 Megastigmane glucosides from Stachys byzantina Yoshio Takeda, Hongjie Zhang, Toshiya Masuda, Gisho Honda, Hideaki Otsuka, Ekrem Sezik, Erdem Yesilada, Handong Sun Structure 13C NMR 碳谱模拟图 40 . blumeol C glucoside 相似度:52.1% Phytochemistry 1997 44 1335-1337 Megastigmane glucosides from Stachys byzantina Yoshio Takeda, Hongjie Zhang, Toshiya Masuda, Gisho Honda, Hideaki Otsuka, Ekrem Sezik, Erdem Yesilada, Handong Sun Structure 13C NMR 碳谱模拟图 41 . blumenol C glucoside C19H32O7 相似度:52.1% Chemical & Pharmaceutical Bulletin 2010 58 438-441 Structural Revisions of Blumenol C Glucoside and Byzantionoside B Katsuyoshi Matsunami, Hideaki Otsuka and Yoshio Takeda Structure 13C NMR 碳谱模拟图 42 . byzantionoside B C19H32O7 相似度:52.1% Chemical & Pharmaceutical Bulletin 2010 58 438-441 Structural Revisions of Blumenol C Glucoside and Byzantionoside B Katsuyoshi Matsunami, Hideaki Otsuka and Yoshio Takeda Structure 13C NMR 碳谱模拟图 43 . (6S,9S)-3-Oxo-α-ionol-β-D-glucopyranoside 相似度:52.1% Archives of Pharmacal Research 2003 26 1018-1023 Constituents of the stems and fruits of Opuntia ficus-indica var. saboten Eun Ha Lee, Hyoung Ja Kim, Yun Seon Song, Changbae Jin and Kyung-Tae Lee, et al. Structure 13C NMR 碳谱模拟图 44 . jasminoside T C21H34O11 相似度:52.1% Bioorganic & Medicinal Chemistry Letters 2013 23 1127-1131 Chemical constituents from the fruit of Gardenia jasminoides and their inhibitory effects on nitric oxide production Kaifeng Peng, Liguo Yang, Shizhe Zhao, Lixia Chen, Feng Zhao, Feng Qiu Structure 13C NMR 碳谱模拟图 45 . blumenyl C β-D-glucopyranoside 相似度:52.1% European Journal of Organic Chemistry 2001 2001 3537-3543 Alkaloidal, Megastigmane and Lignan Glucosides from Antidesma membranaceum (Euphorbiaceae) Alexander Buske, Jürgen Schmidt, Andrea Porzel and Günter Adam Structure 13C NMR 碳谱模拟图 46 . 3-oxo-4-hydroxy-β-ionyl-9-O-β-D-glucopyranoside C19H30O8 相似度:52.1% Journal of Agricultural and Food Chemistry 1998 46 1797-1804 Studies on the Constituents of Amaranthus caudatus Leaves: Isolation and Structure Elucidation of New Triterpenoid Saponins and Ionol-Derived Glycosides Luca Rastrelli, Rita Aquino, Susana Abdo, Maria Proto, Francesco De Simone, and Nunziatina De Tommasi Structure 13C NMR 碳谱模拟图 47 . platanionoside G C24H40O11 相似度:50% Chemical & Pharmaceutical Bulletin 2002 50(3) 390-394 Platanionosides D—J: Megastigmane Glycosides from the Leaves of Alangium platanifolium (SIEB. et ZUCC.) HARMS var. platanifolium SIEB. et ZUCC. Hideaki OTSUKA and Akie TAMAKI Structure 13C NMR 碳谱模拟图 48 . 12β-hydroxy-desacetyl-scillirosidn 相似度:50% Natural Product Research 1993 3 139-143 Bufadienolides and a Steroidal Sapogenin from Urginea sanguinea (Hyacynthaceae) Liselotte Krenn; Brigitte Kopp; Maria Bamberger; Eva Brustmann; Wolfgang Kubelka Structure 13C NMR 碳谱模拟图 49 . trifostigmanoside III C24H40O11 相似度:50% Phytochemistry 1999 50 859-862 Megastigmane glycosides from seeds of Trifolium alexandrinum Khaled M. Mohamed, Mahmoud H. Mohamed, Kazuhiro Ohtani, Ryoji Kasai,Kazuo Yamasaki Structure 13C NMR 碳谱模拟图 50 . salvionoside B C24H38O11 相似度:50% Phytochemistry 1997 44 117-120 Megastigmane glycosides from Salvia nemorosa Yoshio Takeda, Hongjie Zhang, Takashi Matsumoto, Hideaki Otsuka, Yasushi Oosio, Gisho Honda, Mamoru Tabata, Tetsuro Fujita, Handong Sun, Ekrem Sezik, Erdem Yesilada Structure 13C NMR 碳谱模拟图 51 . salvionoside C C24H40O11 相似度:50% Phytochemistry 1997 44 117-120 Megastigmane glycosides from Salvia nemorosa Yoshio Takeda, Hongjie Zhang, Takashi Matsumoto, Hideaki Otsuka, Yasushi Oosio, Gisho Honda, Mamoru Tabata, Tetsuro Fujita, Handong Sun, Ekrem Sezik, Erdem Yesilada Structure 13C NMR 碳谱模拟图 52 . 16-O-β-D-Glucopyranosyl Coccoline C24H30NO9 相似度:50% Chemical & Pharmaceutical Bulletin 2011 59(5) 564-567 Erythrinan Alkaloids from Seeds of Erythrina velutina Masaaki OZAWA, Akio KISHIDA, and Ayumi OHSAKI Structure 13C NMR 碳谱模拟图 53 . foliasalacioside B1 C24H40O11 相似度:50% Heterocycles 2008 75 131-143 Megastigmane Glycosides from the Leaves of Salacia chinensis Seikou Nakamura, Yi Zhang, Yutana Pongpiriyadacha, Tao Wang, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 54 . foliasalacioside D C24H40O11 相似度:50% Heterocycles 2008 75 131-143 Megastigmane Glycosides from the Leaves of Salacia chinensis Seikou Nakamura, Yi Zhang, Yutana Pongpiriyadacha, Tao Wang, Hisashi Matsuda, and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 |
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