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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ zb6824785: 金币+30, 翻译EPI+1, ★★★★★最佳答案, 非常感谢,同时很抱歉由于这几天事情比较多没能及时评价,望理解! 2014-01-14 18:39:52
Chromatographic conditions
ECD detector cell current 0.5nA, Range 10. 10% OV-17 stationary phase , 2m * 2mm stainless steel packed column ,
High purity nitrogen carrier gas , column flow 35ml/min.Column temperature of 70 ℃, detector temperature 280 ℃, the injection port temperature 150 ℃, injection
300μl headspace .
FID detector , range 10 , high purity nitrogen carrier gas , stainless steel packed column 2m * 2mm, 80 ~ 100 mesh , 10% OV-101
Stationary phase (Shimadzu Corporation) , the column flow rate 30ml/min, column temperature 60 ℃, injection port and detector temperature 150 ℃, the air flow
Speed 300ml/min, hydrogen flow 30ml/min.
FPD detector , range 10 , high purity nitrogen carrier gas , large diameter fused silica capillary column 12m * 0.53mm * 0.25μm,
SE-54 stationary phase column flow 30ml/min, column temperature 60 ℃, detector and injection port temperature 150 ℃, the air flow rate 60ml/min,
Hydrogen flow rate 60ml/min |
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