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lcyscau木虫 (正式写手)
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[求助]
微谱数据求助 已有1人参与
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碳谱如下，溶剂氘代丙酮，可以不考虑溶剂： 55.0,113.6,126.6,128.3,129.3,131.6,163.5 |
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至尊木虫 (职业作家)
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lcyscau: 金币+20, ★★★★★最佳答案 2013-12-25 18:51:54
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lcyscau: 金币+20, ★★★★★最佳答案 2013-12-25 18:51:54
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???????????鵽1068????????(???????????ο?) -------------------------------------------------------------------------------- 1 . 4-phenylfuran-2(5H)-one ?????:75% Heterocycles 2010 80 269-279 Synthesis of 4-Aryl-Substituted Butenolides and Pentenolides by Copper-Catalyzed Hydroarylation Yoshihiko Yamamoto and Naohiro Kirai Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . compound 1g ?????:75% Archiv der Pharmazie 2007 340 456-465 1-Cinnamyl-4-(2-methoxyphenyl)piperazines: Synthesis,Binding Properties,and Docking to Dopamine (D2) and Serotonin (5-HT1A) Receptors Jelena Penjišević, Vladimir Šukalović, Deana Andrić, Sladjana Kostić-Rajačić, Vukić Šoškić and Goran Roglić Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . (E)-4-Methoxycinnamyl alcohol. C10H12O2 ?????:75% Bioorganic & Medicinal Chemistry 1996 4 1747-1753 Nitric oxide-induced oxidation of ??-tocopherol Marco d'Ischia, Luisa Novellino Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . (E)-3-(4-methoxyphenyl)prop-2-en-1-ol ?????:75% Heterocycles 2012 86 745-757 Direct Asymmetric ??-Allylation of Ketones with Allylic Alcohols via Pd/Enamine Cooperative Function Shigeo Yasuda, Naoya Kumagai,* and Masakatsu Shibasaki Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . 4-chloro-2,6-diphenyl-pyranylium perchlorate ?????:71.4% Journal of Heterocyclic Chemistry 2006 43 963-977 Azulene-substituted pyranylium salts. Syntheses and products characterization Alexandru C. 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Compound 5 ?????:71.4% Magnetic Resonance in Chemistry 2005 43 535-542 Ring-substituted benzohydroxamic acids: 1H, 13C and 15N NMR spectra and NHOH proton exchange Jan Schraml, Marcela Tkadlecov??, Statis Pataridis, Ludmila Soukupov??, Vratislav Blechta, Jana Roithov?? and Otto Exner Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . compound 2b C9H10O3 ?????:71.4% Tetrahedron Letters 2001 42 5113-5116 Amberlyst-15 mediated decomposition of ??-diazo carbonyl compounds Sengodagounder Muthusamy, Srinivasarao Arulananda Babu, Chidambaram Gunanathan, Raksh Vir Jasra Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . trans-4,4'-dimethoxy-stilbene C16H16O2 ?????:71.4% Tetrahedron Letters 2002 43 1789-1792 Glycolate aldol reactions with boron enolates of bis-4-methoxyphenyl dioxanone Merritt B Andrus, Kris G Mendenhall, Erik L Meredith, B.B.V Soma Sekhar Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . compound 7(stereo isomer ?????:71.4% Tetrahedron Letters 2005 46 7311-7314 Synthesis and properties of 1,6-methano[10]annuleno[3,4-c]thiophene and its 1,3-dicyano derivative Shigeyasu Kuroda, Mitsunori Oda, Mizuho Nagai, Yuko Wada, Ryuta Miyatake, Tatsuki Fukuda, Hiroaki Takamatsu, Nguyen Chung Thanh, Masaru Mouri, Yanmei Zhang, Mayumi Kyogoku Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . 2-Fluoro-3-phenyl-acrylonitrile C9H6FN ?????:71.4% Tetrahedron 2012 68 603-607 Stereoselective cyanation of ??-bromo-??-fluorostyrenes using potassium cyanide and promoted by (CH3CN)4Cu+ BF4− Said Eddarir, Mohammed Kajjout, Christian Rolando Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . (E)-4,4'-Dimethoxystilbene C16H16O2 ?????:71.4% Tetrahedron 2012 68 3899-3907 Syntheses of polyfunctionalized resveratrol derivatives using Wittig and Heck protocols Malik Chalal, Dominique Vervandier-Fasseur, Philippe Meunier, H??l??ne Cattey, Jean-Cyrille Hierso Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . 2-(4-Chlorophenyl)-4,5-dihydrooxazole ?????:71.4% European Journal of Organic Chemistry 2012 1626-1632 Solvent-Free Tandem Synthesis of 2-Thiazolines and 2-Oxazolines Catalyzed by a Copper Catalyst Xiangnan Li, Baoyue Zhou, Jin Zhang, Mengyao She, Shujuan An, Haixia Ge, Cong Li, Bing Yin, Jianli Li and Zhen Shi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . 1,3-Bis(4,5-dihydrooxazol-2-yl)benzene ?????:71.4% European Journal of Organic Chemistry 2012 1626-1632 Solvent-Free Tandem Synthesis of 2-Thiazolines and 2-Oxazolines Catalyzed by a Copper Catalyst Xiangnan Li, Baoyue Zhou, Jin Zhang, Mengyao She, Shujuan An, Haixia Ge, Cong Li, Bing Yin, Jianli Li and Zhen Shi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . (E)-1-[3-Ethoxy-1-(4-methoxyphenyl)prop-1-en-1-yl]-2-(methoxymethoxy)benzene ?????:71.4% European Journal of Organic Chemistry 2012 1603-1615 A One-Pot Three-Step Synthesis of Z-Trisubstituted Olefins from Arylalkynes and Their Cyclization into 4-Aryl-2H-chromenes Evelia Rasolofonjatovo, Bret Tr??guier, Olivier Provot, Abdallah Hamze, Jean-Daniel Brion and Mouâd Alami Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . 5-phenyl-1,2,3-triazole-4-carbonitrile C9H6N4 ?????:71.4% Bioorganic & Medicinal Chemistry 2011 19 7318-7337 Arylcyanoacrylamides as inhibitors of the Dengue and West Nile virus proteases Christoph Nitsche, Christian Steuer, Christian D. Klein Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . 4-methoxybenzaldehyde C8H8O2 ?????:71.4% Russian Journal of Organic Chemistry 2008 44 823-829 Oxidation reactions of some natural volatile aromatic compounds: anethole and eugenol E. M. Elgendy and S. A. Khayyat Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . 4,4'-dimethoxy-trans-stilbene C16H16O2 ?????:71.4% Indian Journal of Chemistry Section B 1988 27B 597-599 Isolation of 4,4'-dimethoxy-trans-stibene & Flavonoids from Leaves & Twigs of Vitex negundo Linn. J BANERJI, B DAS & R CHAKRABARTY Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . 4-methoxybenzaldehyde ?????:71.4% The Chinese Pharmaceutical Journal 2000 52 251-259 Constituents From the Stems of Dendrobium Moniliforme ?????x(Tzong-Huei Lin), ?????(Shu-Jen Chang), ?????(Chung-Chuan Chen) Structure 13C NMR ??????? |
2楼2013-12-25 18:39:51