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[求助]
求助:各位大侠,谁有氧化钽的PDF标准卡,能给发一份不?急啊~~~~ 已有1人参与
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刚刚接触XRD分析,不是很懂,谁有氧化钽的标准卡,好人帮帮忙啦~~~~![]() ![]() ![]() ![]() ![]() |
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2楼2013-12-13 09:35:23
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
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- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
cai0815: 金币+10, ★★★很有帮助, 偶是新手,金币有点晚了啊,理解万岁啊~~~~~~~~~~~ 2013-12-19 20:11:52
感谢参与,应助指数 +1
cai0815: 金币+10, ★★★很有帮助, 偶是新手,金币有点晚了啊,理解万岁啊~~~~~~~~~~~ 2013-12-19 20:11:52
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PDF#25-0922: QM=Uncommon(?); d=Diffractometer; I=(Unknown) Tantalum Oxide Ta2O5 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= 2T=16.777-74.745 I/Ic(RIR)= Ref: Level-1 PDF Orthorhombic, P21212(18) Z=12 mp= CELL: 6.198 x 40.29 x 3.888 <90.0 x 90.0 x 90.0> P.S= Density(c)=9.069 Density(m)= Mwt= Vol=970.9 Ref: Ibid. Strong Lines: 3.15/X 3.88/9 2.45/8 3.10/4 1.65/4 2.42/4 1.66/3 1.94/3 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 16.777 5.2800 2.0 ( 1 4 0) 8.389 0.0947 1.1900 17.582 5.0400 1.0 ( 0 8 0) 8.791 0.0992 1.2467 22.902 3.8800 85.0 ( 0 0 1) 11.451 0.1289 1.6194 26.370 3.3770 5.0 ( 1 10 0) 13.185 0.1481 1.8606 28.290 3.1520 100.0 ( 1 11 0) 14.145 0.1586 1.9934 28.484 3.1310 4.0 ( 1 4 1) 14.242 0.1597 2.0068 28.794 3.0980 40.0 ( 2 0 0) 14.397 0.1614 2.0281 28.870 3.0900 4.0 ( 2 1 0) 14.435 0.1618 2.0334 28.995 3.0770 2.0 ( 0 8 1) 14.497 0.1625 2.0420 30.262 2.9510 2.0 ( 1 12 0) 15.131 0.1694 2.1292 31.070 2.8760 2.0 ( 0 14 0) 15.535 0.1739 2.1847 32.815 2.7270 3.0 ( 2 7 0) 16.407 0.1834 2.3041 33.941 2.6390 3.0 ( 2 8 0) 16.971 0.1895 2.3809 35.178 2.5490 4.0 ( 2 9 0) 17.589 0.1962 2.4650 36.665 2.4490 75.0 ( 1 11 1) 18.332 0.2042 2.5656 37.072 2.4230 35.0 ( 2 0 1) 18.536 0.2064 2.5931 37.136 2.4190 4.0 ( 2 1 1) 18.568 0.2067 2.5974 38.234 2.3520 2.0 ( 1 12 1) 19.117 0.2126 2.6714 40.339 2.2340 2.0 ( 2 7 1) 20.169 0.2238 2.8125 41.324 2.1830 2.0 ( 2 8 1) 20.662 0.2290 2.8782 42.929 2.1050 3.0 ( 1 18 0) 21.465 0.2375 2.9849 44.323 2.0420 2.0 ( 3 3 0) 22.161 0.2449 3.0770 44.599 2.0300 5.0 ( 2 15 0) 22.300 0.2463 3.0952 44.738 2.0240 6.0 ( 3 4 0) 22.369 0.2470 3.1043 45.138 2.0070 4.0 ( 1 19 0) 22.569 0.2491 3.1306 45.257 2.0020 3.0 ( 3 5 0) 22.629 0.2498 3.1385 46.686 1.9440 25.0 ( 0 0 2) 23.343 0.2572 3.2321 49.183 1.8510 3.0 ( 1 18 1) 24.591 0.2701 3.3945 49.554 1.8380 5.0 ( 3 10 0) 24.777 0.2720 3.4185 49.727 1.8320 17.0 ( 0 22 0) 24.864 0.2729 3.4297 49.960 1.8240 3.0 ( 1 4 2) 24.980 0.2741 3.4447 50.463 1.8070 4.0 ( 1 5 2) 25.231 0.2767 3.4771 50.703 1.7990 18.0 ( 2 15 1) 25.352 0.2779 3.4926 50.794 1.7960 4.0 ( 3 4 1) 25.397 0.2784 3.4984 51.160 1.7840 3.0 ( 0 9 2) 25.580 0.2803 3.5220 51.283 1.7800 2.0 ( 3 5 1) 25.642 0.2809 3.5299 51.909 1.7600 3.0 ( 3 12 0) 25.955 0.2841 3.5700 54.405 1.6850 1.0 ( 1 10 2) 27.203 0.2967 3.7289 55.258 1.6610 7.0 ( 3 10 1) 27.629 0.3010 3.7828 55.439 1.6560 30.0 ( 0 22 1) 27.720 0.3019 3.7942 55.476 1.6550 35.0 ( 1 11 2) 27.738 0.3021 3.7965 55.768 1.6470 15.0 ( 0 13 2) 27.884 0.3036 3.8149 55.805 1.6460 9.0 ( 2 1 2) 27.903 0.3038 3.8172 56.289 1.6330 12.0 ( 3 11 1) 28.144 0.3062 3.8476 56.326 1.6320 8.0 ( 2 21 0) 28.163 0.3064 3.8500 56.629 1.6240 2.0 ( 1 12 2) 28.314 0.3079 3.8690 57.478 1.6020 2.0 ( 3 12 1) 28.739 0.3121 3.9221 58.518 1.5760 9.0 ( 2 22 0) 29.259 0.3173 3.9868 59.640 1.5490 4.0 ( 2 20 1) 29.820 0.3228 4.0563 59.682 1.5480 4.0 ( 4 1 0) 29.841 0.3230 4.0589 59.810 1.5450 3.0 ( 4 2 0) 29.905 0.3236 4.0668 61.615 1.5040 2.0 ( 2 21 1) 30.807 0.3324 4.1777 62.679 1.4810 3.0 ( 4 8 0) 31.339 0.3376 4.2425 62.726 1.4800 3.0 ( 3 19 0) 31.363 0.3378 4.2454 63.491 1.4640 2.0 ( 4 9 0) 31.746 0.3415 4.2918 63.637 1.4610 10.0 ( 2 22 1) 31.818 0.3422 4.3006 64.426 1.4450 1.0 ( 3 17 1) 32.213 0.3460 4.3482 64.727 1.4390 3.0 ( 0 28 0) 32.363 0.3475 4.3664 64.777 1.4380 3.0 ( 4 1 1) 32.389 0.3477 4.3694 64.929 1.4350 1.0 ( 4 2 1) 32.465 0.3484 4.3785 66.333 1.4080 1.0 ( 3 3 2) 33.166 0.3551 4.4625 66.654 1.4020 3.0 ( 3 4 2) 33.327 0.3566 4.4816 66.978 1.3960 2.0 ( 1 19 2) 33.489 0.3582 4.5008 67.692 1.3830 3.0 ( 3 19 1) 33.846 0.3615 4.5432 70.478 1.3350 3.0 ( 3 10 2) 35.239 0.3745 4.7065 70.600 1.3330 6.0 ( 0 22 2) 35.300 0.3751 4.7136 71.401 1.3200 7.0 ( 4 16 0) 35.700 0.3788 4.7600 72.350 1.3050 3.0 ( 2 28 0) 36.175 0.3831 4.8147 72.933 1.2960 4.0 ( 0 0 3) 36.466 0.3858 4.8481 74.745 1.2690 2.0 ( 4 15 1) 37.373 0.3940 4.9513 |
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3楼2013-12-13 10:25:51
xhtangxh
木虫 (著名写手)
有木有虫
- CMEI: 6
- 应助: 773 (博后)
- 金币: 17832.4
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- 帖子: 2676
- 在线: 599.3小时
- 虫号: 428580
- 注册: 2007-08-04
- 专业: 催化化学
【答案】应助回帖
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PDF#54-0514: QM=Common(+); d=Diffractometer; I=(Unknown) Tantalum Oxide Ta2O5 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= 2T=14.739-118.171 I/Ic(RIR)=6.2 Ref: Level-1 PDF Orthorhombic, Ibam(72) Z=6 mp= CELL: 7.34252 x 10.44496 x 6.95092 <90.0 x 90.0 x 90.0> P.S= Density(c)=8.2 Density(m)= Mwt= Vol=533.1 Ref: Ibid. Strong Lines: 3.00/X 2.89/6 6.01/6 2.52/4 1.81/3 2.61/2 1.55/2 1.50/1 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 14.739 6.0054 59.0 ( 1 1 0) 7.369 0.0833 1.0463 16.968 5.2209 11.0 ( 0 2 0) 8.484 0.0958 1.2035 24.223 3.6712 7.0 ( 2 0 0) 12.111 0.1362 1.7115 24.512 3.6286 5.0 ( 1 2 1) 12.256 0.1378 1.7316 25.611 3.4753 7.0 ( 0 0 2) 12.806 0.1439 1.8080 28.349 3.1456 12.0 ( 1 3 0) 14.175 0.1590 1.9975 28.777 3.0998 1.0 ( 2 1 1) 14.389 0.1613 2.0270 29.721 3.0034 100.0 ( 2 2 0) 14.861 0.1665 2.0920 30.879 2.8934 62.0 ( 0 2 2) 15.439 0.1728 2.1716 34.316 2.6110 19.0 ( 0 4 0) 17.158 0.1915 2.4064 35.541 2.5238 35.0 ( 2 0 2) 17.771 0.1981 2.4896 37.719 2.3829 2.0 ( 3 1 0) 18.860 0.2098 2.6367 37.860 2.3744 1.0 ( 2 3 1) 18.930 0.2106 2.6462 38.574 2.3321 6.0 ( 1 3 2) 19.287 0.2144 2.6943 38.795 2.3193 3.0 ( 1 4 1) 19.397 0.2156 2.7091 39.630 2.2723 3.0 ( 2 2 2) 19.815 0.2200 2.7651 42.444 2.1279 1.0 ( 2 4 0) 21.222 0.2350 2.9527 42.793 2.1114 1.0 ( 3 2 1) 21.396 0.2368 2.9758 43.303 2.0877 3.0 ( 0 4 2) 21.651 0.2395 3.0096 44.483 2.0350 2.0 ( 1 2 3) 22.242 0.2457 3.0875 45.085 2.0093 3.0 ( 1 5 0) 22.542 0.2488 3.1271 45.251 2.0023 7.0 ( 3 3 0) 22.625 0.2497 3.1380 46.145 1.9655 4.0 ( 3 1 2) 23.072 0.2544 3.1967 47.157 1.9257 1.0 ( 2 1 3) 23.579 0.2596 3.2629 49.616 1.8358 6.0 ( 4 0 0) 24.808 0.2724 3.4225 50.231 1.8148 33.0 ( 2 4 2) 25.116 0.2755 3.4622 52.014 1.7567 1.0 ( 2 5 1) 26.007 0.2846 3.5767 52.237 1.7497 1.0 ( 4 1 1) 26.118 0.2858 3.5909 52.624 1.7378 14.0 ( 0 0 4) 26.312 0.2877 3.6157 52.888 1.7297 6.0 ( 3 4 1) 26.444 0.2891 3.6325 53.631 1.7075 1.0 ( 2 3 3) 26.815 0.2928 3.6798 54.344 1.6868 1.0 ( 1 4 3) 27.172 0.2964 3.7250 54.960 1.6693 2.0 ( 1 1 4) 27.480 0.2995 3.7640 55.697 1.6489 2.0 ( 0 2 4) 27.848 0.3032 3.8104 55.814 1.6458 4.0 ( 1 6 1) 27.907 0.3038 3.8178 56.662 1.6231 1.0 ( 4 0 2) 28.331 0.3080 3.8710 57.496 1.6015 1.0 ( 3 2 3) 28.748 0.3122 3.9232 57.998 1.5889 1.0 ( 3 5 0) 28.999 0.3147 3.9545 58.310 1.5811 1.0 ( 4 3 1) 29.155 0.3162 3.9739 58.643 1.5729 7.0 ( 2 6 0) 29.321 0.3179 3.9945 59.323 1.5565 8.0 ( 0 6 2) 29.662 0.3212 4.0367 59.596 1.5500 15.0 ( 4 2 2) 29.798 0.3226 4.0536 60.849 1.5211 2.0 ( 1 3 4) 30.424 0.3287 4.1307 61.612 1.5041 14.0 ( 2 2 4) 30.806 0.3324 4.1775 61.721 1.5017 12.0 ( 4 4 0) 30.860 0.3330 4.1841 63.575 1.4623 1.0 ( 1 7 0) 31.787 0.3419 4.2969 63.969 1.4542 1.0 ( 5 1 0) 31.984 0.3438 4.3207 64.342 1.4467 6.0 ( 0 4 4) 32.171 0.3456 4.3432 65.027 1.4331 1.0 ( 2 6 2) 32.514 0.3489 4.3844 65.428 1.4253 1.0 ( 4 1 3) 32.714 0.3508 4.4084 65.993 1.4144 1.0 ( 3 4 3) 32.997 0.3535 4.4422 66.545 1.4040 1.0 ( 3 1 4) 33.272 0.3561 4.4751 67.308 1.3900 1.0 ( 3 6 1) 33.654 0.3597 4.5204 68.570 1.3674 1.0 ( 1 6 3) 34.285 0.3657 4.5950 69.711 1.3478 2.0 ( 1 7 2) 34.856 0.3710 4.6618 70.084 1.3415 1.0 ( 5 1 2) 35.042 0.3727 4.6836 71.754 1.3144 2.0 ( 1 5 4) 35.877 0.3804 4.7804 71.880 1.3124 2.0 ( 3 3 4) 35.940 0.3810 4.7877 72.310 1.3056 1.0 ( 0 8 0) 36.155 0.3830 4.8124 74.403 1.2740 1.0 ( 3 7 0) 37.202 0.3925 4.9319 75.092 1.2640 3.0 ( 1 8 1) 37.546 0.3956 4.9709 75.237 1.2619 3.0 ( 4 0 4) 37.618 0.3962 4.9790 75.457 1.2588 2.0 ( 5 4 1) 37.729 0.3972 4.9914 77.800 1.2266 1.0 ( 4 2 4) 38.900 0.4076 5.1223 79.091 1.2098 1.0 ( 3 6 3) 39.545 0.4133 5.1935 79.759 1.2014 1.0 ( 5 5 0) 39.879 0.4162 5.2301 80.174 1.1962 1.0 ( 3 7 2) 40.087 0.4180 5.2527 80.556 1.1915 1.0 ( 6 2 0) 40.278 0.4196 5.2735 80.907 1.1872 3.0 ( 4 6 2) 40.454 0.4212 5.2925 82.126 1.1726 1.0 ( 3 5 4) 41.063 0.4264 5.3582 82.679 1.1662 3.0 ( 2 6 4) 41.340 0.4288 5.3879 83.247 1.1596 3.0 ( 2 8 2) 41.624 0.4312 5.4182 83.719 1.1543 1.0 ( 6 0 2) 41.860 0.4332 5.4432 85.363 1.1362 4.0 ( 4 4 4) 42.681 0.4400 5.5298 85.856 1.1310 1.0 ( 0 2 6) 42.928 0.4421 5.5556 87.372 1.1152 1.0 ( 5 1 4) 43.686 0.4483 5.6341 88.073 1.1081 1.0 ( 5 6 1) 44.037 0.4512 5.6701 88.409 1.1048 1.0 ( 2 0 6) 44.204 0.4526 5.6872 90.075 1.0886 1.0 ( 1 9 2) 45.037 0.4593 5.7716 90.235 1.0871 1.0 ( 1 3 6) 45.118 0.4599 5.7797 91.583 1.0746 1.0 ( 1 6 5) 45.791 0.4653 5.8470 92.358 1.0676 1.0 ( 5 3 4) 46.179 0.4683 5.8853 92.767 1.0640 1.0 ( 4 8 0) 46.384 0.4699 5.9055 93.709 1.0557 2.0 ( 6 4 2) 46.854 0.4736 5.9515 94.543 1.0486 1.0 ( 3 9 0) 47.272 0.4768 5.9920 94.780 1.0466 1.0 ( 5 7 0) 47.390 0.4777 6.0034 95.111 1.0438 1.0 ( 0 8 4) 47.555 0.4790 6.0193 95.345 1.0419 1.0 ( 3 1 6) 47.673 0.4799 6.0306 96.392 1.0333 1.0 ( 6 3 3) 48.196 0.4839 6.0805 96.618 1.0315 1.0 ( 3 8 3) 48.309 0.4847 6.0912 97.124 1.0275 1.0 ( 3 7 4) 48.562 0.4866 6.1151 97.716 1.0228 1.0 ( 1 10 1) 48.858 0.4888 6.1429 98.406 1.0175 2.0 ( 2 4 6) 49.203 0.4914 6.1751 100.125 1.0046 2.0 ( 2 10 0) 50.063 0.4977 6.2544 100.601 1.0011 2.0 ( 6 6 0) 50.300 0.4994 6.2760 101.749 0.9929 1.0 ( 3 6 5) 50.874 0.5036 6.3279 102.427 0.9882 1.0 ( 5 5 4) 51.214 0.5060 6.3583 103.229 0.9827 1.0 ( 6 2 4) 51.614 0.5088 6.3939 103.674 0.9797 1.0 ( 4 0 6) 51.837 0.5104 6.4135 105.721 0.9663 1.0 ( 5 8 1) 52.861 0.5175 6.5025 106.006 0.9645 2.0 ( 0 6 6) 53.003 0.5184 6.5147 106.252 0.9629 2.0 ( 4 2 6) 53.126 0.5193 6.5253 106.582 0.9608 1.0 ( 6 5 3) 53.291 0.5204 6.5393 107.217 0.9569 1.0 ( 1 9 4) 53.609 0.5225 6.5663 108.081 0.9516 1.0 ( 3 10 1) 54.040 0.5254 6.6026 109.318 0.9443 1.0 ( 1 10 3) 54.659 0.5295 6.6539 110.744 0.9361 1.0 ( 3 5 6) 55.372 0.5341 6.7121 114.122 0.9178 1.0 ( 8 0 0) 57.061 0.5448 6.8458 115.550 0.9105 1.0 ( 5 9 0) 57.775 0.5491 6.9005 116.184 0.9074 2.0 ( 4 8 4) 58.092 0.5510 6.9245 117.870 0.8992 1.0 ( 5 8 3) 58.935 0.5560 6.9871 118.171 0.8978 1.0 ( 3 9 4) 59.086 0.5569 6.9982 |
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