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香港麦兜

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[求助] 求JCPDS 895012和895416 已有1人参与

金属刻蚀制备硅纳米线，XRD表征找不到Si和SiO2对应卡片，求JCPDS 895012和895416.在线等，谢谢！

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1楼 2013-12-12 20:50:03

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xhtangxh

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【答案】应助回帖

★ ★ ★ ★ ★
感谢参与，应助指数 +1
香港麦兜: 金币+5 2013-12-13 11:00:13

PDF#89-5012: QM=Uncommon(?); d=Calculated; I=(Unknown)
Silicon
Si
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=28.442-88.029 I/Ic(RIR)=4.55
Ref: Level-1 PDF

Cubic, Fd-3m(227) Z=8 mp=
CELL: 5.43086 x 5.43086 x 5.43086 <90.0 x 90.0 x 90.0> P.S=
Density(c)=2.32 Density(m)= Mwt= Vol=160.2
Ref: Ibid.

Strong Lines: 3.14/X 1.92/6 1.64/3 1.11/1 1.25/1 1.36/1
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
28.442 3.1355 100.0 ( 1 1 1) 14.221 0.1595 2.0039 3
47.302 1.9201 55.5 ( 2 2 0) 23.651 0.2604 3.2723 8
56.122 1.6375 30.1 ( 3 1 1) 28.061 0.3053 3.8371 11
58.856 1.5677 0.1 ( 2 2 2) 29.428 0.3189 4.0078 12
69.129 1.3577 7.0 ( 4 0 0) 34.564 0.3683 4.6277 16
76.376 1.2459 9.6 ( 3 3 1) 38.188 0.4013 5.0430 19
88.029 1.1086 11.6 ( 4 2 2) 44.015 0.4510 5.6678 24

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2楼2013-12-13 10:30:44

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

xhtangxh

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CMEI: 6
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虫号: 428580
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专业: 催化化学

【答案】应助回帖

PDF#89-5416: QM=Calculated; d=Calculated; I=(Unknown)
ITQ-9
SiO2
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=7.985-46.597 I/Ic(RIR)=3.71
Ref: Level-1 PDF

Triclinic,  I-1(2) Z=32 mp=
CELL: 14.7685 x 18.1793 x 7.3823 <89.14 x 110.679 x 90.945> P.S=
Density(c)=1.662 Density(m)= Mwt= Vol=1854.0
Ref: Ibid.

Strong Lines: 10.94/X  11.06/X  9.09/2  4.53/1  7.29/1  4.58/1  3.45/1  4.67/1
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
7.985 11.0631 99.3 (-1 1 0) 3.993 0.0452 0.5679
8.078 10.9363 100.0 ( 1 1 0) 4.039 0.0457 0.5745
9.724 9.0880 18.9 ( 0 2 0) 4.862 0.0550 0.6914
12.127 7.2921 7.6 (-1 0 1) 6.064 0.0686 0.8616
12.804 6.9080 1.4 ( 2 0 0) 6.402 0.0724 0.9096
13.660 6.4771 4.5 ( 0 1 1) 6.830 0.0772 0.9701
13.750 6.4351 5.6 ( 0-1 1) 6.875 0.0777 0.9764
15.284 5.7925 0.4 (-2 1 1) 7.642 0.0863 1.0847
15.439 5.7344 1.1 (-1 2 1) 7.720 0.0872 1.0957
15.694 5.6418 0.7 (-1-2 1) 7.847 0.0886 1.1137
15.889 5.5732 0.5 (-1 3 0) 7.944 0.0897 1.1274
16.030 5.5243 0.5 (-2 2 0) 8.015 0.0905 1.1374
16.196 5.4681 0.2 ( 2 2 0) 8.098 0.0914 1.1491
19.002 4.6666 6.7 ( 1-2 1) 9.501 0.1071 1.3464
19.378 4.5768 7.3 ( 0 3 1) 9.689 0.1092 1.3728
19.569 4.5325 11.3 ( 0 4 0) 9.785 0.1103 1.3863
19.814 4.4770 3.7 (-3 1 0) 9.907 0.1117 1.4034
19.929 4.4516 5.2 ( 3 1 0) 9.964 0.1123 1.4114
20.492 4.3305 0.2 (-2 3 1) 10.246 0.1155 1.4509
20.893 4.2483 0.1 (-2-3 1) 10.446 0.1177 1.4790
21.221 4.1833 0.1 (-3 2 1) 10.611 0.1195 1.5020
21.711 4.0900 2.4 ( 2-1 1) 10.855 0.1222 1.5362
22.867 3.8857 4.5 (-1 4 1) 11.434 0.1287 1.6170
23.217 3.8280 3.4 (-1-4 1) 11.609 0.1306 1.6414
23.283 3.8173 3.7 (-2 4 0) 11.641 0.1310 1.6460
23.544 3.7756 1.7 ( 2 4 0) 11.772 0.1324 1.6641
24.113 3.6877 0.4 (-3 3 0) 12.057 0.1356 1.7038
24.397 3.6454 1.0 (-2 0 2) 12.199 0.1372 1.7236
24.671 3.6056 3.1 (-1 1 2) 12.336 0.1387 1.7426
24.795 3.5879 5.7 (-4 1 1) 12.397 0.1394 1.7512
24.968 3.5633 2.3 (-4-1 1) 12.484 0.1403 1.7633
25.237 3.5259 2.5 (-1 5 0) 12.619 0.1418 1.7820
25.452 3.4966 3.0 ( 1 5 0) 12.726 0.1430 1.7969
25.530 3.4862 2.7 ( 1-4 1) 12.765 0.1434 1.8023
25.772 3.4540 7.2 ( 4 0 0) 12.886 0.1448 1.8191
26.161 3.4036 1.2 (-2 2 2) 13.080 0.1469 1.8461
26.469 3.3646 1.6 (-2-2 2) 13.235 0.1486 1.8675
26.578 3.3511 1.9 (-3 1 2) 13.289 0.1492 1.8750
26.769 3.3276 2.6 (-3-1 2) 13.384 0.1503 1.8882
27.110 3.2865 0.2 (-3 4 1) 13.555 0.1521 1.9118
27.519 3.2386 3.0 ( 0 2 2) 13.759 0.1544 1.9401
27.702 3.2175 2.7 ( 0-2 2) 13.851 0.1554 1.9528
28.314 3.1493 0.3 (-4 3 1) 14.157 0.1588 1.9951
28.579 3.1208 0.3 ( 3 2 1) 14.290 0.1602 2.0133
28.842 3.0930 0.1 (-2-5 1) 14.421 0.1617 2.0314
29.147 3.0613 0.4 ( 1 1 2) 14.573 0.1633 2.0525
29.207 3.0551 0.4 ( 1-1 2) 14.604 0.1637 2.0566
29.461 3.0293 3.2 (-4 0 2) 14.731 0.1651 2.0741
29.886 2.9872 1.2 (-3 3 2) 14.943 0.1674 2.1034
30.277 2.9496 2.2 (-5 0 1) 15.138 0.1695 2.1302
30.373 2.9404 2.1 (-3-3 2) 15.186 0.1700 2.1368
30.848 2.8962 0.1 (-4 2 2) 15.424 0.1726 2.1694
31.136 2.8701 0.2 (-3 5 0) 15.568 0.1742 2.1892
31.214 2.8631 0.1 (-4-2 2) 15.607 0.1746 2.1945
31.509 2.8369 0.2 ( 3 5 0) 15.755 0.1762 2.2148
31.770 2.8142 0.2 (-5 2 1) 15.885 0.1777 2.2327
32.158 2.7812 0.5 (-2 6 0) 16.079 0.1798 2.2592
32.342 2.7658 0.9 (-4 4 0) 16.171 0.1808 2.2718
32.727 2.7341 0.7 ( 0-4 2) 16.364 0.1829 2.2981
32.807 2.7276 0.8 ( 2 0 2) 16.403 0.1833 2.3035
33.153 2.6999 0.3 ( 4-1 1) 16.577 0.1852 2.3272
33.282 2.6897 0.6 ( 4 1 1) 16.641 0.1859 2.3360
33.411 2.6797 1.3 ( 3 4 1) 16.705 0.1866 2.3447
33.862 2.6450 0.9 ( 1-6 1) 16.931 0.1890 2.3755
34.072 2.6292 0.1 (-5-1 2) 17.036 0.1902 2.3898
34.326 2.6103 0.1 ( 2 2 2) 17.163 0.1915 2.4071
34.496 2.5978 0.3 (-1 5 2) 17.248 0.1925 2.4186
34.955 2.5648 0.5 (-1-5 2) 17.477 0.1949 2.4498
35.058 2.5575 0.5 (-1 7 0) 17.529 0.1955 2.4568
35.207 2.5470 1.2 (-4 4 2) 17.603 0.1963 2.4669
35.516 2.5255 0.1 (-5 3 0) 17.758 0.1980 2.4879
35.605 2.5194 0.1 (-3-6 1) 17.803 0.1985 2.4939
35.856 2.5023 0.3 ( 5 3 0) 17.928 0.1998 2.5109
35.989 2.4934 0.5 (-5 4 1) 17.994 0.2005 2.5199
36.157 2.4822 0.3 ( 4 3 1) 18.078 0.2014 2.5313
36.571 2.4551 0.5 (-5 3 2) 18.285 0.2037 2.5592
36.766 2.4425 0.3 (-6 1 1) 18.383 0.2047 2.5724
36.830 2.4384 0.3 ( 0 7 1) 18.415 0.2051 2.5768
36.951 2.4307 0.5 (-2-1 3) 18.475 0.2057 2.5849
37.087 2.4221 0.3 ( 0-7 1) 18.543 0.2064 2.5941
37.230 2.4131 0.8 (-1 0 3) 18.615 0.2072 2.6038
37.374 2.4041 0.5 (-2 7 1) 18.687 0.2080 2.6135
37.982 2.3670 0.1 ( 3-1 2) 18.991 0.2112 2.6545
38.133 2.3580 0.1 (-3 2 3) 19.066 0.2120 2.6646
38.222 2.3527 0.2 ( 1-5 2) 19.111 0.2125 2.6706
38.447 2.3395 0.2 (-1 2 3) 19.224 0.2137 2.6857
38.553 2.3333 0.2 ( 2-4 2) 19.276 0.2143 2.6928
38.795 2.3193 0.1 (-4 1 3) 19.397 0.2156 2.7091
38.937 2.3112 0.1 (-2-6 2) 19.468 0.2163 2.7186
39.122 2.3007 0.3 ( 6 0 0) 19.561 0.2173 2.7310
39.262 2.2928 0.2 (-6 3 1) 19.631 0.2181 2.7404
39.293 2.2910 0.2 (-2 3 3) 19.646 0.2182 2.7425
39.471 2.2811 0.3 ( 0-1 3) 19.736 0.2192 2.7545
39.609 2.2735 0.1 (-3 7 0) 19.804 0.2199 2.7637
39.716 2.2676 0.1 (-2-3 3) 19.858 0.2205 2.7708
40.042 2.2499 0.1 ( 3 7 0) 20.021 0.2222 2.7927
40.143 2.2445 0.1 ( 3-6 1) 20.071 0.2228 2.7994
40.254 2.2385 0.1 (-6 2 0) 20.127 0.2234 2.8068
40.342 2.2339 0.1 ( 3 6 1) 20.171 0.2238 2.8127
40.476 2.2268 0.1 ( 5 2 1) 20.238 0.2245 2.8217
40.586 2.2210 0.2 ( 3 3 2) 20.293 0.2251 2.8290
40.746 2.2126 0.2 (-5 5 0) 20.373 0.2260 2.8397
40.852 2.2071 0.2 ( 2 7 1) 20.426 0.2265 2.8468
41.240 2.1872 0.2 (-5 0 3) 20.620 0.2286 2.8726
41.393 2.1795 0.3 (-1 8 1) 20.697 0.2294 2.8829
41.461 2.1761 0.3 ( 4 5 1) 20.731 0.2298 2.8874
41.605 2.1689 0.2 (-5 5 2) 20.802 0.2305 2.8969
41.664 2.1660 0.3 (-2 8 0) 20.832 0.2308 2.9009
41.806 2.1589 0.5 (-1-8 1) 20.903 0.2316 2.9103
41.975 2.1506 0.3 ( 1 0 3) 20.987 0.2325 2.9215
42.147 2.1422 0.2 ( 0-3 3) 21.074 0.2334 2.9330
42.248 2.1374 0.1 (-5 2 3) 21.124 0.2339 2.9397
42.430 2.1286 0.3 (-5-5 2) 21.215 0.2349 2.9518
42.523 2.1242 0.2 (-4-6 2) 21.262 0.2354 2.9580
42.629 2.1191 0.1 (-1-4 3) 21.315 0.2359 2.9650
42.949 2.1041 1.4 (-1-7 2) 21.475 0.2376 2.9862
43.048 2.0995 0.9 ( 4 0 2) 21.524 0.2382 2.9927
43.258 2.0898 0.2 ( 1-2 3) 21.629 0.2393 3.0066
43.433 2.0817 0.1 (-3 7 2) 21.717 0.2402 3.0182
44.068 2.0532 0.5 (-6 5 1) 22.034 0.2435 3.0601
44.246 2.0454 0.4 (-7 1 2) 22.123 0.2445 3.0719
44.437 2.0370 0.1 (-7-1 2) 22.218 0.2455 3.0845
44.597 2.0301 0.3 ( 2 6 2) 22.299 0.2463 3.0951
44.739 2.0240 0.7 ( 2-6 2) 22.370 0.2470 3.1044
44.931 2.0158 0.3 (-6 1 3) 22.465 0.2480 3.1170
45.131 2.0073 0.1 (-6-1 3) 22.565 0.2491 3.1302
45.420 1.9952 0.1 ( 3 5 2) 22.710 0.2506 3.1492
45.661 1.9852 0.1 ( 1-7 2) 22.831 0.2519 3.1650
45.795 1.9797 0.1 (-4 5 3) 22.898 0.2526 3.1738
46.008 1.9711 0.3 ( 2-1 3) 23.004 0.2537 3.1877
46.165 1.9647 0.2 (-7 1 0) 23.083 0.2545 3.1980
46.443 1.9536 0.3 (-7 3 2) 23.222 0.2559 3.2162
46.597 1.9475 0.3 (-4-5 3) 23.298 0.2567 3.2262

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3楼2013-12-13 10:31:26

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香港麦兜

新虫 (初入文坛)

应助: 0 (幼儿园)
金币: 9.5
帖子: 14
在线: 39小时
虫号: 1347879
注册: 2011-07-16
专业: 催化化学

引用回帖:

2楼: Originally posted by xhtangxh at 2013-12-13 10:30:44
PDF#89-5012: QM=Uncommon(?); d=Calculated; I=(Unknown)
Silicon
Si
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=28.442-88.029 I/Ic(RIR)=4.55
Ref: Level-1 PDF

Cubic, Fd-3m(227) Z=8 m ...

您好，请问您的JCPDS是哪个版本的？

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4楼2013-12-13 13:20:41

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xhtangxh

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CMEI: 6
应助: 773 (博后)
金币: 17832.4
红花: 107
帖子: 2676
在线: 599.3小时
虫号: 428580
注册: 2007-08-04
专业: 催化化学

PDF-2 2004.

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5楼2013-12-14 11:34:51

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