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yu19891206银虫 (正式写手)
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[求助]
求助微谱数据 谢谢啦
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| 溶剂是氘代氯仿和氘代甲醇 碳谱数据从大到小是150.41/149.23/147.79/145.34/126.01/124.79/123.48/122.97/122.66/110.12/109.38/106.61/103.25/103.02/93.59/79.04/78.71/78.39/56.61/56.13/55.33/54.28/49.94/49.73/49.51/49.30/49.09/48.87/48.66/45.06/42.96/40.41/36.52/24.79/24.22 我给出的数据没有去除溶剂峰 万分感谢了！！！！！ |
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2楼2013-11-03 10:29:06
yu19891206
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3楼2013-11-03 10:53:26
yu19891206
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4楼2013-11-03 10:57:00
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【答案】应助回帖
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感谢参与，应助指数 +1
yu19891206: 金币+15, ★★★★★最佳答案, 谢谢啦 2013-11-03 12:59:55
感谢参与，应助指数 +1
yu19891206: 金币+15, ★★★★★最佳答案, 谢谢啦 2013-11-03 12:59:55
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查询结果：共查到26个化合物(查询结果仅供参考) 1 . protopine hydrochloride 相似度:62.0% Chinese Traditional and Herbal Drugs 2011 42 1939-1944 Investigation on structure of protopine alkaloid ion-pair compounds ZHANG, Xue, ZENG, Jian-guo, DU, Fang-lu, LI, Wen-liang, LIU, Fa-bao Structure 13C NMR 碳谱模拟图 2 . Isotylocrebrine C24H27O4 相似度:56% Phytochemistry 1995 39 695-699 Phenanthroindolizidine alkaloids from Tylophora tanakae Fumiko Abe, Yukiko Iwase, Tatsuo Yamauchi, Keiichi Honda, Nanao Hayashi Structure 13C NMR 碳谱模拟图 3 . 6-甲氧基-5,6-二羟基两面针碱 C22H21NO5 相似度:56% Chinese Traditional and Herbal Drugs 2009 40 93-95 两面针的化学成分和飞龙掌血酮内酯的晶体结构 杨国红 Structure 13C NMR 碳谱模拟图 4 . 4-Hydroxy-3-methoxy-17-methyl-(2',3'-dihydro-3',6'-bis-trifluoromethyl-pyridazino)[4',5'-6,7]-morphinan C22H23F6N3O2 相似度:56% Archiv der Pharmazie 1997 330 163-168 Syntheses of Novel Pyridazinomorphinans by Inverse Electron Demand Cycloaddition and their Binding to μ and κ Receptors Thilo Klindert, Isabel Stroetmann, Gunther Seitz, Georg Höfner, Klaus Th. Wanner, Gerlinde Frenzen and Brigitta Eckhoff Structure 13C NMR 碳谱模拟图 5 . allocryptopine hydrochloride 相似度:56% Chinese Traditional and Herbal Drugs 2011 42 1939-1944 Investigation on structure of protopine alkaloid ion-pair compounds ZHANG, Xue, ZENG, Jian-guo, DU, Fang-lu, LI, Wen-liang, LIU, Fa-bao Structure 13C NMR 碳谱模拟图 6 . (5-((6,7,10,11-Tetramethoxy-3,4-dihydrodibenzo [f,h]isoquinolin-2(1H)-yl)methyl)furan-2-yl)methanol C27H29NO6 相似度:53.8% Bioorganic & Medicinal Chemistry 2012 20 5893-5900 Synthesis and evaluation of the anti-proliferative and NF-κB activities of a library of simplified tylophorine analogs Micah J. Niphakis, Bryant C. Gay, Kwon Ho Hong, Nicholas P. Bleeker, Gunda I. Georg Structure 13C NMR 碳谱模拟图 7 . N,N-Pentamethylene-2-(9-demethoxyberberine bromide-9-yl)hydroxyacetamide C26H27N2O5 相似度:53.8% Chemistry of Natural Compounds 2013 48 1047-1053 Synthesis of berberine bromide analogs containing tertiary amides of acetic acid in the 9-O-position I. V. Nechepurenko, N. I. Komarova, V. G. Vasil’ev Structure 13C NMR 碳谱模拟图 8 . protopine salicylic acid 相似度:53.8% Chinese Traditional and Herbal Drugs 2011 42 1939-1944 Investigation on structure of protopine alkaloid ion-pair compounds ZHANG, Xue, ZENG, Jian-guo, DU, Fang-lu, LI, Wen-liang, LIU, Fa-bao Structure 13C NMR 碳谱模拟图 9 . cis-3-(3,4-dimethoxyphenyl)-4-[(E)-2,4,5-trimethoxystryl]cyclohex-1-ene C25H30O5 相似度:52% Chemical & Pharmaceutical Bulletin 1980 28 2948-2959 Further Characterization of the Constituents of a Thai Medicinal Plant, Zingiber cassumunar ROXB. MASANORI KUROYANAGI,SEIGO FUKUSHIMA,KUNITOSHI YOSHIHIRA,SHINSAKU NATORI,THAWEEPHOL DECHATIWONGSE,KUNIHIDE MIHASHI,MASATOSHI NISHI and SHUUJI HARA Structure 13C NMR 碳谱模拟图 10 . (–)-N-methylcorydalisol 相似度:52% Natural Product Research 2009 23 982-987 Alkaloids from Mongolian species Hypecoum lactiflorum Kar. et Kir. Pazij Stefan Philipov; Ralitsa Istatkova; Pavletta Denkova; Selenge Dangaa; Javzan Samdan; Marieta Krosnova; Chogsom Munkh-Amgalan Structure 13C NMR 碳谱模拟图 11 . 7-Demethyltylophorine C23H25NO4 相似度:52% Phytochemistry 1995 39 695-699 Phenanthroindolizidine alkaloids from Tylophora tanakae Fumiko Abe, Yukiko Iwase, Tatsuo Yamauchi, Keiichi Honda, Nanao Hayashi Structure 13C NMR 碳谱模拟图 12 . 1-(3,4-Dimethoxyphenylmethyl)-3-phenyl-6,7,8-trimethoxy- 1,2,3,4-tetrahydro isoquinoline C27H31NO5 相似度:52% Journal of Heterocyclic Chemistry 2005 42 109-111 Synthesis of 1-(3,4-dimethoxyphenylmethyl)-3-phenyl-6,7,8-trimethoxy-3,4-dihydroisoquinoline Adriana F. Ibañez Structure 13C NMR 碳谱模拟图 13 . pachycanthine C20H19NO4 相似度:52% Indian Journal of Chemistry Section B 2008 47B 945-951 Pachycanthine: A new isoquinoline alkaloid and its antihepatotoxic activity from Berberis pachycantha Koehne Ahmed,Bahar; Masoodi,Mubashir H; Khan,Shamshir Structure 13C NMR 碳谱模拟图 14 . compound 10 相似度:52% Tetrahedron Letters 2003 44 6915-6918 Synthesis and absolute configuration of cordiaquinone K, antifungal and larvicidal meroterpenoid isolated from the Panamanian plant, Cordia curassavica Arata Yajima, Fumihiro Saitou, Mayu Sekimoto, Shoichiro Maetoko, Goro Yabuta Structure 13C NMR 碳谱模拟图 15 . compound 3 C25H29N3O4 相似度:52% Tetrahedron Letters 2003 44 7091-7094 A new efficient synthetic process for the construction of the pentacyclic core of marine alkaloid ecteinascidins Ye-Feng Tang, Zhan-Zhu Liu, Shi-Zhi Chen Structure 13C NMR 碳谱模拟图 16 . 6,7-Dimethoxy-1,2-dimethyl-3-(3,4-methylenedioxyphenyl)isoquinolinium methosulfate C21H23NO8S 相似度:52% Bioorganic & Medicinal Chemistry 1996 4 781-791 Coralyne and related compounds as mammalian topoisomerase I and topoisomerase II poisons Darshan Makhey, Barbara Gatto, Chiang Yu, Angela Liu, Leroy F. Liu, Edmond J. LaVoie Structure 13C NMR 碳谱模拟图 17 . 2,3,9,10-Tetramethoxybenz[a]acridine C21H19NO4 相似度:52% Bioorganic & Medicinal Chemistry 2000 8 1171-1182 Substituted benz[a]acridines and benz[c]acridines as mammalian topoisomerase poisons Darshan Makhey, Chiang Yu, Angela Liu, Leroy F. Liu, Edmond J. LaVoie Structure 13C NMR 碳谱模拟图 |
5楼2013-11-03 12:05:54
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