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oyf8888

银虫 (小有名气)

[求助] 微谱数据求助,万分感谢!

溶剂  氘代氯仿
碳谱数据14.391,16.410,17.632,18.300,18.482,21.244,22.238,22.534,24.932,25.722,28.021,28.127,28.249,33.910,35.921,36.027,36.407,37.166,39.025,39.420,41.803,44.299,47.016,50.947,53.027,57.512,88.619,114.800,125.228,130.919,148.655
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yaolan123

禁虫 (职业作家)

【答案】应助回帖

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感谢参与,应助指数 +1
oyf8888: 金币+20, ★★★很有帮助, 非常感谢您!祝您事事如意! 2013-06-01 14:40:59
???????????鵽123????????(???????????ο?)  
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1 .     parkeyl acetate
C32H52O2     ?????:87.0%
Journal of Natural Products          1989          Vol 52          1136
Isolation of Lanosta-9( 11),24-dien-3??-yl Acetate from Leuzea carthamoides
S. A. Khalid, E. Varga, K. Szendrei, Helmut Duddeck
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

2 .     3??-methoxy-lanost-9(11)-ene
    ?????:87.0%
Journal of the Brazilian Chemical Society          2002          13          135-139
Saponins and Sapogenins from Brachiaria decumbens Stapf
Viviane S. Pires, Alexandre T.C. Taketa, Grace Gosmann and Eloir P. Schenkel
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

3 .     (24S)-3??-methoxy-5??-lanost-9(11)-ene-24,25-diol
C31H54O3     ?????:83.8%
Acta Botanica Sinica          2004          46          1002-1008
Terpenoids and Phenols from Taiwania flousiana
XIANG Ying, YANG Sheng-Ping, ZHAN Zha-Jun, YUE Jian-Min
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

4 .     24-ethyl-3??-methoxylanost-9(11)-en-25-ol
C33H58O2     ?????:81.8%
Chemical & Pharmaceutical Bulletin          2007          55(6)          908-911
Lanostane-Type Triterpenoids from Diospyros discolor
Chiy-Rong CHEN,Chao-Wen CHENG,Min-Hsiung PAN,Yun-Wen LIAO,Chih-Ying TZENG,and Chi-I CHANG
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

5 .     3??-methoxy-24-methylenelanost- 9(11)-en-25-ol
C32H54O2     ?????:81.2%
Chemical & Pharmaceutical Bulletin          2007          55(6)          908-911
Lanostane-Type Triterpenoids from Diospyros discolor
Chiy-Rong CHEN,Chao-Wen CHENG,Min-Hsiung PAN,Yun-Wen LIAO,Chih-Ying TZENG,and Chi-I CHANG
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

6 .     3??-methoxy-24- methyllanosta-9(11),25-dien-24-ol
C32H54O2     ?????:81.2%
Chemical & Pharmaceutical Bulletin          2007          55(6)          908-911
Lanostane-Type Triterpenoids from Diospyros discolor
Chiy-Rong CHEN,Chao-Wen CHENG,Min-Hsiung PAN,Yun-Wen LIAO,Chih-Ying TZENG,and Chi-I CHANG
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

7 .     25,26,27-trisno??-3??-methoxy-lanost-9(11)-en-24-oic acid
C28H46O3     ?????:80.6%
Journal of Natural Products          2000          63          1055-1057
Four New Trisnorlanostene-Type Triterpenoids from the Stem Bark of Pinus luchuensis
Shun-ich Wada and Reiko Tanaka
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

8 .     Pinusyunnanol
C31H54O4     ?????:80.6%
Helvetica Chimica Acta          2010          93          490-496
Three New Terpenoids from Pinus yunnanensis
Bin Wang, Jing Ju, Xiu-Feng He, Tao Yuan and Jian-Min Yue
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

9 .     (24S)-24,25-isopropylidenedioxy-3??-methoxy-5??-lanost-9(11)-ene
C34H58O3     ?????:78.7%
Journal of the Chinese Chemical Society          1991          38          61-64
The Constituents of the Bark of Armand Pine
??????(Jim-Min Fang);????(Wei-Yu Tsai);?????(Yu-Shia Cheng)
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

10 .     agrostophyllinol
C31H52O     ?????:77.4%
Phytochemistry          2003                   591-596
Triterpenoids from the orchids Agrostophyllum brevipes and Agrostophyllum callosum
P.L. Majumder, S. Majumder, S. Sen
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

11 .     3??-hydroxy-24S,25R-epoxylanost-9(11)-en-27-oic Acid
    ?????:77.4%
Chemistry of Natural Compounds          1990          26          545-548
STRUCTURE OF A NEW TRITERPENOID FROM THE BARK OF THE SIBERIAN LARCH
G. F. Chernenko, I. Yu. Bagryanskaya,and E. N. Shmidt
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

12 .     (24S)-5??-lanost-9(11)-ene-3??,24,25-triol
C30H52O3     ?????:77.4%
Acta Botanica Sinica          2004          46          1002-1008
Terpenoids and Phenols from Taiwania flousiana
XIANG Ying, YANG Sheng-Ping, ZHAN Zha-Jun, YUE Jian-Min
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

13 .     Retusenol
C30H52O     ?????:77.4%
Zeitschrift f??r Naturforschung B          2012          67          426-432
A New Triterpene from Atalantia retusa Merr.
Consolacion Y. Ragasa, Dinah L. Espineli, Emelina H. Mandia, Dennis D. Raga, Ming-Jaw Don, and Chien-Chang Shen
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

14 .     O-methyllaureolol
C35H60O     ?????:77.1%
Chinese Chemical Letters          1995          6          873-874
O-METHYLLAUREOLOL FROM SKIMMIA LAUREOLA
HONG JIE ZHANG,XIN FENG GAO,MING ZHE ZHANG
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

15 .     24,24-dimethyl-5??-lanosta-9(11),25-dien-3??-yl acetate
C34H56O2     ?????:76.4%
Phytochemistry          1996          42          1109-1113
Tetracyclic triterpenoids from Glycosmis arborea
Ajit K. Chakravarty, Binayak Das, Kazuo Masuda, Hiroyuki Ageta
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

16 .     O-methylclausenol
C34H58O     ?????:76.4%
Phytochemistry          1989          28          943-945
A triterpene alcohol,lansiol, from Clausena lansium
V. Lakshmi,K. Raj,R.S. Kapil
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

17 .     (24S)-24-Methyl-5a-lanosta-9(11),25-dien-3fl-yl acetate
C33H54O2     ?????:75.7%
Phytochemistry          1996          42          1109-1113
Tetracyclic triterpenoids from Glycosmis arborea
Ajit K. Chakravarty, Binayak Das, Kazuo Masuda, Hiroyuki Ageta
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

18 .     lansiol
C33H56O     ?????:75.7%
Phytochemistry          1989          28          943-945
A triterpene alcohol,lansiol, from Clausena lansium
V. Lakshmi,K. Raj,R.S. Kapil
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

19 .     24-methyllenelanost-9(11)-en-3??-ol acetate
    ?????:75.7%
Journal of Integrative Plant Biology          2005          47          1016-1020
Chemical Constituents of the Roots of Vernonia cumingiana Benth.
Qing-Hua LIU, Jing-Quan YUAN, Mao-Rong SUO and Jun-Shan YANG*
Structure      13C NMR   ???????
--------------------------------------------------------------------------------

20 .     3??-hydroxy-lanost-9(11),24(25)-dien-26-oic acid
C30H48O3     ?????:74.1%
Chemical & Pharmaceutical Bulletin          2003          51(10)          1174-1176
Micranoic Acids A and B: Two New Octanortriterpenoids from Schisandra micrantha
Rong-Tao LI, Quan-Bin HAN, Ai-Hua ZHAO, and Han-Dong SUN
Structure      13C NMR   ???????
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