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【答案】应助回帖
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Carena: 金币+1, 感谢应助 2013-05-06 21:30:26
一一陌颜: 金币+20, 翻译EPI+1, ★★★很有帮助 2013-10-27 13:56:32
The title compound was prepared under the hydrothermal conditions. A mixture of CuCl2 4H2O (0.1 mmol), Pyrrole (0.1mmol) and dipicolinic acid (pyridine-2,6-dicarboxylic acid) (0.1 mmol), disodium dipicolinate (0.2 mmol) in H2O (30 mL) were placed in a Teflon-lined stainless steel vessel, heated to 440 K for 4 day, and then cooled to room temperature within 24 h. and then the blue block crystals of the title complex were obtained. The blue crystals suitable for X-ray diffraction analysis were collected.
在水热条件下（成功）制备了目标化合物。将四水氯化铜(0.1毫摩尔)、吡咯(0.1毫摩尔)和吡啶二羧酸(2,6羧酸吡啶)(0.1毫摩尔)，二吡啶甲酸二钠 (0.2毫摩尔)溶解在30毫升在水中，然后将此溶液转移至一个聚四氟乙烯内衬的不锈钢反应釜中，加热到440 K并反应4天,然后在24小时之内冷却至室温。之后得到蓝色块状目标产物晶体。将蓝色晶体制备成为可以进行XRD分析的试样。 |
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