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zhiwu1983

木虫 (正式写手)

[求助] 求助微谱数据查询

碳谱数据下:75.3,73.9,67.9,58.3,56.1,54.1,50.7,41.1,38.7,36.6,36.1,34.4,31.5,28.8,25.9,24.1,23.8,22.6,20.4,13.5,12.4
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zhiwu1983: 金币+15, ★★★★★最佳答案 2013-04-28 08:00:58
1 .     (20S)-20-hydroxy-5α-pregnan-3β-yl acetate
    相似度:78.2%
Steroids          2010          75          721-725
Stereoselectivity of sodium borohydride reduction of saturated steroidal ketones utilizing conditions of Luche reduction
Eva Šťastná, Ivan Černý, Vladimír Pouzar, Hana Chodounská
Structure      13C NMR   碳谱模拟图
2 .     3β,4α-dihydroxypregnan-21-one
C21H34O3     相似度:76.1%
Phytochemistry          2008          69          1319-1327
Structural elucidation of limonoids and steroids from Trichilia connaroides
Xiao-Ning Wang, Cheng-Qi Fan, Sheng Yin, Li-She Gan, Jian-Min Yue
Structure      13C NMR   碳谱模拟图
3 .     20S-pregn-5-ene3,20-diol 3-monoacetate
C23H36O3     相似度:76.1%
Chemical & Pharmaceutical Bulletin          1982          30          3932-3941
Studies on the Constituents of Asclepiadaceae Plants. LI. Oxidation at the 18-Methyl Group of C/D-cis-Pregnane Type Steroids and 13C-Nuclear Magnetic Resonance Spectra of 18-Oxygenated Pregnanes and Related Compounds
MASAHIKO KIMURA,KOJI HAYASHI,HIROSHI NARITA and HIROSHI MITSUHASHI
Structure      13C NMR   碳谱模拟图
4 .     4-pregnene-3β,20α-diol
    相似度:76.1%
Steroids          1986          47          249-259
Synthesis and characteristics of allylic 4-pregnene-3,20-diols found in gonadal and breast tissues
J. P. Wiebe, Vinod Dave, J. B. Stothers
Structure      13C NMR   碳谱模拟图
5 .     (2α,3α,5α,20R)-2,3-epoxypregnan-20-ol
C21H34O2     相似度:76.1%
Steroids          2012          77          1403-1418
Solid-phase chemical synthesis and in vitro biological evaluation of novel 2β-piperazino-(20R)-5α-pregnane-3α,20-diol N-derivatives as anti-leukemic agents
Hajer Jegham, René Maltais, Philippe Dufour, Jenny Roy, Donald Poirier
Structure      13C NMR   碳谱模拟图
6 .     Terminaline
C23H41NO2     相似度:72.7%
Steroids          2005          70          295-303
Cholinesterase inhibitory pregnane-type steroidal alkaloids from Sarcococca hookeriana
M. Iqbal Choudhary, Krishna Prasad Devkota, Sarfraz Ahmad Nawaz, Rosa Ranjit, Atta-ur- Rahman
Structure      13C NMR   碳谱模拟图
7 .     (20R)-20-hydroxy-5α-pregnan-3β-yl acetate
    相似度:69.5%
Steroids          2010          75          721-725
Stereoselectivity of sodium borohydride reduction of saturated steroidal ketones utilizing conditions of Luche reduction
Eva Šťastná, Ivan Černý, Vladimír Pouzar, Hana Chodounská
Structure      13C NMR   碳谱模拟图
8 .     Methyl 6α-hydroxy-5α-cholanoate
C25H42O3     相似度:68%
Steroids          1993          58          362-369
Potential bile acid metabolites. 20. A new synthetic route to stereoisomeric 3,6,-dihydroxy- and 6-hydroxy-5α-cholanoic acids
Takashi Iida, Tamaaki Tamaru, Frederic C. Chang, Toshifumi Niwa, Junichi Goto, Toshio Nambara
Structure      13C NMR   碳谱模拟图
9 .     20R-pregn-5-ene3,20-diol 3-monoacetate
C23H36O3     相似度:66.6%
Chemical & Pharmaceutical Bulletin          1982          30          3932-3941
Studies on the Constituents of Asclepiadaceae Plants. LI. Oxidation at the 18-Methyl Group of C/D-cis-Pregnane Type Steroids and 13C-Nuclear Magnetic Resonance Spectra of 18-Oxygenated Pregnanes and Related Compounds
MASAHIKO KIMURA,KOJI HAYASHI,HIROSHI NARITA and HIROSHI MITSUHASHI
Structure      13C NMR   碳谱模拟图
10 .     5β-pregnane
    相似度:66.6%
Journal of Natural Products          1991          Vol 54          1651
Verrucoside, a New Cytotoxic Pregnane Glycoside from a Gorgonian Eunicella verrucosa
Y. Kashman, D. Green, C. Garcia, D. Garcia Arevalos
Structure      13C NMR   碳谱模拟图
11 .     ent-17-chloro-(13S),16β-dihydroxyatisane-3,14-dione
C20H29ClO4     相似度:66.6%
Phytochemistry          1990          29          1925-1935
Ent-atisane diterpenes from Euphorbia fidjiana
Allick R. Lal,Richard C. Cambie,Peter S. Rutledge,Paul D. Woodgate
Structure      13C NMR   碳谱模拟图
12 .     ent-16α,17-dihydroxyatisan-3-one
C19H29O2     相似度:66.6%
Phytochemistry          1990          29          1925-1935
Ent-atisane diterpenes from Euphorbia fidjiana
Allick R. Lal,Richard C. Cambie,Peter S. Rutledge,Paul D. Woodgate
Structure      13C NMR   碳谱模拟图
13 .     Disodium 3β,6 α-dihydroxy-5a-pregnan-20-onedisulfate
C21H32O9S2Na2     相似度:66.6%
Steroids          1999          64          335-340
Evaluation of the antiviral activity of natural sulfated polyhydroxysteroids and their synthetic derivatives and analogs
María J. Comin, Marta S. Maier, Alejandro J. Roccatagliata, Carlos A. Pujol, Elsa B. Damonte
Structure      13C NMR   碳谱模拟图
14 .     3β-hydroxy-5β-pregnane-20-one
    相似度:66.6%
Steroids          1995          60          337-352
Microbial transformation of steroids: Contribution to 14α-hydroxylations
Shang-hui Hu, Gilles Genain, Robert Azerad
Structure      13C NMR   碳谱模拟图
15 .     3'-HO-Stanozolol
    相似度:66.6%
Steroids          1992          57          537-550
17-Epimerization of 17α-methyl anabolic steroids in humans: metabolism and synthesis of 17α-hydroxy-17β-methyl steroids
Willi Schänzer, Georg Opfermann, Manfred Donike
Structure      13C NMR   碳谱模拟图
16 .     ent-16α,17-Dihydroxyatisan-3-one
C20H32O3     相似度:66.6%
Chinese Traditional and Herbal Drugs          2004          35          611-613
Diterpenoids from Euphorbia wallichii
WANG Huan; ZHANG Xiao-feng; MA Yun-bao; CAI Xiang-hai; WU Da-gang; LUO Xiao-dong
Structure      13C NMR   碳谱模拟图
17 .     ent-lαbdα-13(16),14-diene-3α-ol
C20H34O     相似度:66.6%
Food Chemistry          2010          119          1399-1408
Antibacterial labdane diterpenoids of Ulva fasciata Delile from southwestern coast of the Indian Peninsula
Kajal Chakraborty, A.P. Lipton, R. Paul Raj, K.K. Vijayan
Structure      13C NMR   碳谱模拟图
18 .     (5α,20R)-pregn-2-en-20-ol
C21H34O     相似度:66.6%
Steroids          2012          77          1403-1418
Solid-phase chemical synthesis and in vitro biological evaluation of novel 2β-piperazino-(20R)-5α-pregnane-3α,20-diol N-derivatives as anti-leukemic agents
Hajer Jegham, René Maltais, Philippe Dufour, Jenny Roy, Donald Poirier
Structure      13C NMR   碳谱模拟图
19 .     3β,4α-dihydroxypregnan-16-one
C21H34O3     相似度:66.6%
Canadian Journal of Chemistry          2003          81          253-257
A pentanortriterpenoid with a novel carbon skeleton and a new pregnane from Trichilia connaroides
Hua-Ping Zhang, Shao-Hua Wu, Yue-Mao Shen, Yun-Bao Ma, Da-Gang Wu, Shu-Hua Qi, Xiao-Dong Luo
Structure      13C NMR   碳谱模拟图
20 .     5α-Pregnane
C21H36     相似度:66.6%
Organic Magnetic Resonance          1977          9          439-464
13C N.m.r. Spectra of steroids—A Survey and Commentary
J.W.Blunt and J.B.Stothers
Structure      13C NMR   碳谱模拟图
21 .     5α-Pregnane-3β,20-diol
C21H36O2     相似度:66.6%
Organic Magnetic Resonance          1977          9          439-464
13C N.m.r. Spectra of steroids—A Survey and Commentary
J.W.Blunt and J.B.Stothers
Structure      13C NMR   碳谱模拟图
22 .     5β-Pregnane
C21H36     相似度:66.6%
Organic Magnetic Resonance          1977          9          439-464
13C N.m.r. Spectra of steroids—A Survey and Commentary
J.W.Blunt and J.B.Stothers
Structure      13C NMR   碳谱模拟图
23 .     3β-Hydroxy-5β-pregnan-20-one
C21H34O2     相似度:66.6%
Organic Magnetic Resonance          1977          9          439-464
13C N.m.r. Spectra of steroids—A Survey and Commentary
J.W.Blunt and J.B.Stothers
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
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