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杨大松

至尊木虫 (文坛精英)

[求助] 求助微谱数据,谢谢

碳谱数据如下,溶剂氯仿:
14.2,17.9,18.0,21.6,21.9,25.7,25.8,29.7,60.4,103.4,105.5,109.8,121.2,121.6,127.5,128.6,130.0,131.1,134.5,135.4,136.3,144.7,152.3,155.7,159.9,175.7
辛苦各位了,非常感谢
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碧雪清谭
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jasminelw

铁杆木虫 (正式写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
jiangchunyong: 金币+1, 谢谢 2013-04-23 13:37:14
杨大松(jiangchunyong代发): 金币+15 2013-04-23 13:37:19
1 .     parvifolixanthone A
C28H32O6     相似度:74.0%
Chinese Traditional and Herbal Drugs          2012          43          436-439
Chemical constituents from stem barks of Garcinia paucinervis
FAN Qing-fei; NA Zhi; HU Hua-bin; XU You-kai; TANG Ting
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

2 .     abyssinone-IV-4-O-methyl ether
C26H30O4     相似度:73.0%
Journal of Natural Products          2006          69          1572-1576
Protein Tyrosine Phosphatase-1B Inhibitory Activity of Isoprenylated Flavonoids Isolated from Erythrina mildbraedii
MinKyun Na, JunPil Jang, Dieudonn Njamen, Joseph Tanyi Mbafor,Zacharias Tanee Fomum, Bo Yeon Kim, Won Keun Oh, and Jong Seog Ahn
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

3 .     vogelin D
C26H30O5     相似度:73.0%
Journal of Natural Products          2002          65          403-406
Prenylated Isoflavonoids from the Root Bark of Erythrina vogelii
Emerson F. Queiroz, Kagoyire K. Atindehou, Christian Terreaux, Sandor Antus, and Kurt Hostettmann
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

4 .     papyriflavonol A
    相似度:73.0%
Fitoterapia          2001          72          456-458
Papyriflavonol A, a new prenylated flavonol from Broussonetia papyrifera
K.H. Son, S.J. Kwon, H.W. Chang, H.P. Kim,S.S. Kang
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

5 .     
    相似度:73.0%
Fitoterapia          2000          71          607-609
Two novel xanthones from Garcinia mangostana
Geetha Gopalakrishnan, Banumathy Balaganesan
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

6 .     glyasperin A
    相似度:73.0%
Phytochemistry          1995          38          535-537
Isoprenylated flavonols of formosan Broussonetia papyrifera
Song-Chwan Fang, Bor-Jinn Shieh, Ru-Rong Wu, Chun-Nan Lin
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

7 .     Na-benzyl-2-isoprenyl-6-methoxytryptophan ethyl ester
    相似度:73.0%
Bioorganic & Medicinal Chemistry          2008          16          4626-4651
Synthesis and structure–activity relationship studies on tryprostatin A, an inhibitor of breast cancer resistance protein
Hiteshkumar D. Jain, Chunchun Zhang, Shuo Zhou, Hao Zhou, Jun Ma, Xiaoxiang Liu, Xuebin Liao, Amy M. Deveau, Christine M. Dieckhaus, Michael A. Johnson, Kirsten S. Smith, Timothy L. Macdonald, Hideaki Kakeya, Hiroyuki Osada, James M. Cook
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

8 .     bannaxanthone E
    相似度:70.3%
China Journal of Chinese Materia Medica          2009          34          2338-2342
Chemical constituents from twigs of Garcinia xipshuanbannaensis
NA Zhi, XU Youkai
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

9 .     latisxanthone-C
C28H30O6     相似度:70.3%
Chemical & Pharmaceutical Bulletin          1997          45          1403-1415
A Novel Depsidone and Some New Xanthones from Garcinia species
Chihiro ITO,Yoshiaki MIYAMOTO,Minako NAKAYAMA,Yuko KAWAI,K. Sundar RAO and Hiroshi FURUKAWA
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

10 .     Mappain
    相似度:70.3%
Helvetica Chimica Acta          2010          93          829-836
First Total Synthesis of Mappain with a Prenylated and Geranylated Stilbene
Lakkoju Chakrapani, Eun Mi Jung and Yong Rok Lee
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

11 .     ethyl 4-(4-bromophenyl)-6-({[4-(4-chlorophenyl)-3-cyano-5,6,7,8-tetrahydroquinolin-2-yl]thio}methyl)-1-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
C31H28BrClN4O3S     相似度:70.3%
Tetrahedron          2012          68          9729-9737
The Thorpe–Ziegler-type reaction of 3-cyanopyridine-2(1H)-thiones with Biginelli 6-bromomethyl-3,4-dihydropyrimidin-2(1H)-ones: cascade assembling of tetra- and pentacyclic heterocyclic scaffolds
Iryna O. Lebedyeva, Victor V. Dotsenko, Vladimir V. Turovtsev, Sergey G. Krivokolysko, V'yacheslav M. Povstyanoy, Mikhaylo V. Povstyanoy
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

12 .     adenaflorin B
C25H28O5     相似度:69.2%
Journal of Natural Products          2004          67          451-453
New Cytotoxic Naphthopyrane Derivatives from Adenaria floribunda
Ahmed A. Hussein, Icela Barberena, Todd L. Capson, Thomas A. Kursar, Phyllis D. Coley, Pablo N. Solis, and Mahabir P. Gupta
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

13 .     cudratricusxanthone K
C24H26O6     相似度:69.2%
Journal of Natural Products          2007          70          1207-1209
Prenylated Xanthones from the Root Bark of Cudrania tricuspidata
Ji Hye Hwang,Seong Su Hong,Xiang Hua Han, Ji Sang Hwang, Dongho Lee, Heesoon Lee, Yeo Pyo Yun,Youngsoo Kim, Jai Seup Ro, and Bang Yeon Hwang
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

14 .     7-O-methylisolupalbigenin
C26H28O5     相似度:69.2%
Journal of Natural Products          2002          65          175-178
Flavonoids from Ulex airensis and Ulex europaeus ssp. Europaeus
Patrícia Máximo, Ana Lourenço, Sónia Savluchinske Feio,and José Carlos Roseiro
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

15 .     chiricanine C
    相似度:69.2%
Journal of Natural Products          2001          64          710-715
Five New Prenylated Stilbenes from the Root Bark of Lonchocarpus chiricanus
Jean-Robert Ioset,Andrew Marston, Mahabir P. Gupta, and Kurt Hostettmann
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

16 .     broussonol D
C25H26O7     相似度:69.2%
Journal of Natural Products          2001          64          1206-1209
Five New Diprenylated Flavonols from the Leaves of Broussonetia kazinoki
Pei-Cheng Zhang, Si Wang, Yan Wu, Ruo-Yun Chen, and De-Quan Yu
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

17 .     broussonol E
C25H26O7     相似度:69.2%
Journal of Natural Products          2001          64          1206-1209
Five New Diprenylated Flavonols from the Leaves of Broussonetia kazinoki
Pei-Cheng Zhang, Si Wang, Yan Wu, Ruo-Yun Chen, and De-Quan Yu
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

18 .     cudraxanthone F
C24H26O6     相似度:69.2%
Planta Medica          1990          56          399-402
Structures of Three New Isoprenylated Xanthones,Cudraxanthones E, F, and G
Yoshio Hano, Yutaka Matsumoto, Jin-Yun Sun, and Taro Nomura
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

19 .     5,7,3'-trihydroxy-4'-methoxy-6,5'-di(γ,γ-dimethylallyl)-isoflavanone
C26H30O6     相似度:69.2%
Natural Product Research          2009          23          1089-1094
Three new isoflavanones from Erythrina costaricensis
Hitoshi Tanaka; Hisanori Hattori; Tomoko Oh-Uchi; Masaru Sato; Magoichi Sako; Yoichi Tateishi; Ghazala Hafeez Rizwani
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

20 .     lupalbigenin
    相似度:69.2%
Phytochemistry          1999          52          87-94
Six diprenylisoflavones, derrisisoflavones A-F, from Derris scandens
Toshikazu Sekine, Miyuki Inagaki, Fumio Ikegami, Yuichi Fujii, Nijsiri Ruangrungsi
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

21 .     dorsmanin D
    相似度:69.2%
Phytochemistry          1998          48          349-354
Geranylated and prenylated flavonoids from the twigs of Dorstenia mannii
Bonaventure T. Ngadjui, Berhanu M. Abegaz, Etienne Dongo, Helene Tamboue, Kouam Fogue
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

22 .     gartanin
    相似度:69.2%
Journal of Natural Products          1990          Vol 53          1463
Synthesis of Minor Xanthones from Garcinia mangostana
Graham. J. Bennett, Hiok-Huang Lee, Liak-Phong Lee
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

23 .     gartanin
    相似度:69.2%
Natural Product Sciences          2006          12          138-143
[γ-mangostin and Rubraxanthone, Two Potential Lead Compounds for Anti-cancer Activity against CEM-SS Cell Line
Ee, G.C.L.; Izzaddin, S.A.; Rahmani, M.; Sukari, M.A.; Lee, H.L.
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

24 .     Macarangaflavanone B
C25H28O5     相似度:69.2%
Phytochemistry          1995          40          1273-1277
Prenylated flavanones from leaves of Macaranga pleiostemona
Barbara A. Schütz, Anthony D. Wright, Topul Rali, Otto Sticher
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

25 .     Euchrestaflavanone A
    相似度:69.2%
Phytochemistry          1995          40          1273-1277
Prenylated flavanones from leaves of Macaranga pleiostemona
Barbara A. Schütz, Anthony D. Wright, Topul Rali, Otto Sticher
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

26 .     Ethyl 1,1',2',5-Tetrahydro-1'-methyl-2',5-dioxo-2-propylspiro[4H-indeno[1,2-b]pyridine-4,3'-[3H]-indole]-3-carboxylate
C26H24N2O4     相似度:69.2%
Helvetica Chimica Acta          2011          Vol. 94          1628-1637
A New Four-Component Reaction for the Synthesis of Spiro[4H-indeno-[1, 2-b]pyridine-4, 3'-[3H]indoles]
Afsaneh Feiz, Ghazaleh Imani Shakibaei, Zahra Yasaei, Hamid Reza Khavasi, and Ayoob Bazgir
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

27 .     6,8-diprenylorobol
    相似度:69.2%
Phytochemistry          1989          28          2522-2526
8-prenylluteone,a prenylated isoflavone from Erythrina eriotriocha
Augustin E. Nkengfack,Dale R. Sanson,Z.Tanee Fomum,Michael S. Tempesta
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

28 .     (±)-(Z)-3,7-dimethyl-2-methoxy-7-[2-(5-methyl)furyl]-1-phenylsulfenyl-3-phenylsulfonyl-1-octene
C28H34O4S2     相似度:69.2%
Heterocycles          2004          62          583-618
Intramolecular [4+3] Cycloadditions. Towards a Synthesis of Widdrol
Michael Harmata,* Mehmet Kahraman, Gilbert Adenu, and Charles L. Barnes
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

29 .     broussoflavonol F
    相似度:69.2%
Chinese Traditional and Herbal Drugs          2010          41          191-195
Chemical constituents in stem bark of Morus cathayana
NI Gang; ZHANG Qing-jian; ZHENG Zhong-fei; CHEN Ruo-yun; YU De-quan
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

30 .     8-Lavandulylkaempferol
C25H27O6     相似度:69.2%
Archives of Pharmacal Research          2005          28          1333-1336
A new lavandulylated flavonoid with free radical and onoo-scavenging activities fromSophora flavescens
Jin Jung, Sam Sik Kang, Ju Jung Woo and Jae Sue Choi
Structure      13C NMR   碳谱模拟图
2楼2013-04-23 10:32:25
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杨大松

至尊木虫 (文坛精英)

辛苦了,非常感谢
碧雪清谭
3楼2013-04-23 13:54:17
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