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杨大松

至尊木虫 (文坛精英)

[求助] 求助微谱数据,谢谢

碳谱数据如下,溶剂氯仿:
18.9,72.5,80.2,81.8,104.8,109.9,111.1,112.0,130.7,143.5,143.7,151.8
辛苦各位了,谢谢
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碧雪清谭
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jasminelw

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【答案】应助回帖

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感谢参与,应助指数 +1
杨大松: 金币+15, ★★★★★最佳答案 2013-04-23 10:36:43
1 .     (1Z)-atractylodin
C13H10O     相似度:92.3%
Planta Medica          2001          67          437-442
Further Phenols and Polyacetylenes from the Rhizomes of Atractylodes lancea and their Anti-Inflammatory Activity
M. Resch, J. Heilmann, A. Steigel, R. Bauer
Structure      13C NMR   碳谱模拟图

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2 .     bis(5-((1E,7E)-nona-1,7-dien-3,5-diyn-1-yl)furan-2-yl)methane
    相似度:78.5%
Fitoterapia          2012          83          199-203
A new 9-nor-atractylodin from Atractylodes lancea and the antibacterial activity of the atractylodin derivatives
Yanjun Chen, Yuxue Wu, Hexiang Wang, Kun Gao
Structure      13C NMR   碳谱模拟图

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3 .     9-Nor-atractylodin
    相似度:76.9%
Fitoterapia          2012          83          199-203
A new 9-nor-atractylodin from Atractylodes lancea and the antibacterial activity of the atractylodin derivatives
Yanjun Chen, Yuxue Wu, Hexiang Wang, Kun Gao
Structure      13C NMR   碳谱模拟图

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4 .     1-(2-furyl)-(1E,7Z)-nonadiene-3,5-diyne-9-ol
    相似度:76.9%
Fitoterapia          2012          83          199-203
A new 9-nor-atractylodin from Atractylodes lancea and the antibacterial activity of the atractylodin derivatives
Yanjun Chen, Yuxue Wu, Hexiang Wang, Kun Gao
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

5 .     trand-1,3,5,11-tridecatetraen-7,9-diyne
C13H12     相似度:69.2%
Phytochemistry          1997          45          695-699
Phototoxic polyacetylenes from Viguiera annua and adaptations of a chrysomelid beetle, Zygogramma continua, feeding on this plant
Gabriel Guillet, Denise Chauret, John T. Arnason
Structure      13C NMR   碳谱模拟图

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6 .     acetylatractylodinol
C15H12O3     相似度:66.6%
China Journal of Chinese Materia Medica          2005          30          675-677
Studies on chemical constituents in roots of Peucedanum praeruptorum
ZHANG Cun, XIAO Yongqing, TANIGUCH Massahiko, BABA Kimiye
Structure      13C NMR   碳谱模拟图

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7 .     angelidiol A
C14H14O5     相似度:64.2%
Chinese Chemical Letters          1993          4          885-886
TWO NEW COUMARINS FROM ANGELCIA PUBESCENS F.BISERRTA
JIANG HUA LIU,YING JIE GUO,SUI XU XU,XIN SHENG YAO
Structure      13C NMR   碳谱模拟图

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8 .     andangelidiol
C14H14O5     相似度:64.2%
Journal of Chinese Pharmaceutical Sciences          1997          6          122-422
Further Isolation of Coumarin from Angelica pubescence Maxim f.biserrata Shanet Yuan
Jiang-Hua Liu, Sui-Xu Xu, Zhi-Yun Meng, Xin-Sheng Yao and Yu-Qiang Wu
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

9 .     heramandiol
C14H14O5     相似度:64.2%
Acta Pharmaceutica Sinica          1996          31          63-67
FURTHER STUDIES ON CHEMICAL CONSTITUENTS OF ANGELICA PUBESCENS F BISERRATA
JH Liu; SX Xu; XS Yao and YQ Wu
Structure      13C NMR   碳谱模拟图

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10 .     bis(5-((1E,7E)-nona-1,7-dien-3,5-diyn-1-yl)furan-2-yl)isopropane
    相似度:62.5%
Fitoterapia          2012          83          199-203
A new 9-nor-atractylodin from Atractylodes lancea and the antibacterial activity of the atractylodin derivatives
Yanjun Chen, Yuxue Wu, Hexiang Wang, Kun Gao
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

11 .     1,cis-3,trans-5,trans-11-tridecatetraen-7,9-diyne
C13H12     相似度:61.5%
Phytochemistry          1997          45          695-699
Phototoxic polyacetylenes from Viguiera annua and adaptations of a chrysomelid beetle, Zygogramma continua, feeding on this plant
Gabriel Guillet, Denise Chauret, John T. Arnason
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

12 .     3,8,9,10-tetrahydroxy-6H-dibenzo[b,d]pyran-6-one
C13H8O6     相似度:61.5%
Journal of Agricultural and Food Chemistry          2008          56          393-400
Identification of Urinary and Intestinal Bacterial Metabolites of Ellagitannin Geraniin in Rats
Hideyuki Ito, Ayumu Iguchi and Tsutomu Hatano
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

13 .     3-deoxy-3-iodo-1,2-O-isopropylidene-6-O-tosyl-α-D-allofuranose
    相似度:61.5%
Journal of Agricultural and Food Chemistry          2000          48          5283-5287
Synthesis and Antifungal Activity of Novel Bisdithiocarbamate Derivatives of Carbohydrates against Fusarium oxysporum f. sp. lini
Catherine Rafin, Etienne Veignie, and Michel SancholleDenis Postel, Christophe Len, Pierre Villa, and Gino Ronco
Structure      13C NMR   碳谱模拟图

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14 .     5-(2,2-dimethyl-(4R)-1,3-dioxolan-4-yl)-6-(2-furyl)-2,2-diemthyl-(3aR,5R,6R,6aR)-perhydrofuro-[2,3-d][1,3]-dioxol-6-ol
C15H18O7     相似度:60%
Tetrahedron          2002          58          3801-3812
Synthesis of spiro carbon linked disaccharides from d-glucose, d- and l-arabinose
G.V.M Sharma, V.Goverdhan Reddy, Palakodety Radha Krishna, A.Ravi Sankar, A.C Kunwar
Structure      13C NMR   碳谱模拟图

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15 .     1-(1,3-Dihydro-4-hydroxy-1-isobenzofuranyl)butan-2,3-diol
    相似度:58.3%
Journal of Natural Products          2002          65          876-882
Biologically Active Polyketide Metabolites from an Undetermined Fungicolous Hyphomycete Resembling Cladosporium
Ulrich Höller,James B. Gloer, and Donald T. Wicklow
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

16 .     1-(1,3-Dihydro-4-hydroxy-1-isobenzofuranyl)butan-2,3-diol
    相似度:58.3%
Journal of Natural Products          2002          65          876-882
Biologically Active Polyketide Metabolites from an Undetermined Fungicolous Hyphomycete Resembling Cladosporium
Ulrich Höller,James B. Gloer, and Donald T. Wicklow
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

17 .     Esculetin
C9H6O4     相似度:58.3%
Acta Botanica Yunnanica          2007          29(2)          263-264
Chemical Constituents from Ceratophyllum demersum (Ceratophyllaceae)
LU Xiao-Li,QIAO Ying, ZHANG Xian-Min, MA Bo-Lin, QIU Ming-Hua
Structure      13C NMR   碳谱模拟图

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18 .     Scopoletin
C10H8O4     相似度:58.3%
Chemistry of Natural Compounds          2009          45          896-897
CHEMICAL CONSTITUENTS FROM THE AERIALPARTS OF Sophora mollis
Dong-Qing Fei, Mohammad Arfan,Jamal Rafiq, and Kun Gao
Structure      13C NMR   碳谱模拟图

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19 .     scosoletin
C10H8O4     相似度:58.3%
Acta Botanica Sinica          2003          45          1003-1007
Two New Triterpenes from Neonauclea sessilifolia
KANG Wen-Yi, LI Guo-Hong, HAO Xiao-Jiang
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

20 .     4H-1-benzopyran-4-one,5,7-dihydroxy-2-methyl
C10H8O4     相似度:58.3%
Acta Botanica Sinica          2003          45          1003-1007
Two New Triterpenes from Neonauclea sessilifolia
KANG Wen-Yi, LI Guo-Hong, HAO Xiao-Jiang
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

21 .     esculetin
C9H6O4     相似度:58.3%
Journal of Chinese Pharmaceutical Sciences          1994          3          91-96
active constituents of Viola prionantha Bge.
Bo Qin, Qing-Ping Chen and Zhi-Cen Lou
Structure      13C NMR   碳谱模拟图
2楼2013-04-23 10:25:49
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杨大松

至尊木虫 (文坛精英)

辛苦了,非常感谢
碧雪清谭
3楼2013-04-23 10:36:55
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