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Rio2016

木虫 (小有名气)

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phu_grassman: 金币+5, thanks 2013-04-12 08:53:47
飘落江南: 金币+25, 翻译EPI+1, ★★★★★最佳答案 2013-04-15 19:43:25
When it reaches -10° C, he
keeps it at this temperature for a couple of hours,
then filters out the crystals.
当它达到-10° C,在这个温度保持两小时,然后滤掉结晶物。
They are rinsed a couple of times with ether or another solvent such
as hexane, then, while still wet with ether, added
to a large flask or beaker containing 2000 ml of
water.
用乙醚或其他溶剂例如正己烷冲洗两次,然后,保持带有乙醚的湿的状态,并转移到一个带有2000ml水的大瓶或烧杯中。
They are dissolved by stirring, then the
flask or beaker is cooled down to 0° C by packing
it in ice mixed with salt. When it reaches this
temperature, 200 ml of glacial acetic acid is
added to it with vigorous stirring.
搅拌使其溶解,然后把瓶子或烧杯埋到冰盐混合物中使其降到 0° C 。当它降到这个温度,向里面加200 ml 冰醋酸,边加边搅拌。
The chemist must make sure that the temperature does not go
up more than a few degrees while he is adding it.
filters the crystals off it and rinses them a few
times with water.
操作者必须保证,在添加的过程中不能使温度升高几度,滤去结晶物,用水冲洗几次。

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