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When it reaches -10¡ã C, he
keeps it at this temperature for a couple of hours,
then filters out the crystals. They are rinsed a
couple of times with ether or another solvent such
as hexane, then, while still wet with ether, added
to a large flask or beaker containing 2000 ml of
water. They are dissolved by stirring, then the
flask or beaker is cooled down to 0¡ã C by packing
it in ice mixed with salt. When it reaches this
temperature, 200 ml of glacial acetic acid is
added to it with vigorous stirring. The chemist
must make sure that the temperature does not go
up more than a few degrees while he is adding it.
filters the crystals off it and rinses them a few
times with water. The crystals must now be kept
moist in order for them to be turned into.
In a 2000 ml flask, he puts
700 ml of concentrated sulfuric acid. It is cooled
down to -10¡ã C by packing the flask in a mixture
of salt and ice, then magnetic stirring is begun.
The crystals are slowly added to the sulfuric acid.
They must be moist, or he will get a mess. It takes
about an hour to add the crystals to the sulfuric
acid. Once they are added, the flask is heated in a
pan of boiling water and swirled around to dissolve
the crystals. After they have dissolved, the
flask is heated for a couple more minutes, then
removed from the pan of boiling water. It is
cooled down slowly to 0¡ã C by first letting it cool
down, then packing it in ice.
chemist puts 1700 ml of water
in a 3000 ml flask. Half of the sulfuric acid
solution is added to it. It is heated in a pan of
boiling water for a couple of hours. It is given a
couple of good shakes every 15 minute
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phu_grassman: ½ð±Ò+5, thanks 2013-04-12 08:53:47
Æ®Âä½­ÄÏ: ½ð±Ò+25, ·­ÒëEPI+1, ¡ï¡ï¡ï¡ï¡ï×î¼Ñ´ð°¸ 2013-04-15 19:43:25
When it reaches -10¡ã C, he
keeps it at this temperature for a couple of hours,
then filters out the crystals.
µ±Ëü´ïµ½-10¡ã C£¬ÔÚÕâ¸öζȱ£³ÖÁ½Ð¡Ê±£¬È»ºóÂ˵ô½á¾§Îï¡£
They are rinsed a couple of times with ether or another solvent such
as hexane, then, while still wet with ether, added
to a large flask or beaker containing 2000 ml of
water.
ÓÃÒÒÃÑ»òÆäËûÈܼÁÀýÈçÕý¼ºÍé³åÏ´Á½´Î£¬È»ºó£¬±£³Ö´øÓÐÒÒÃѵÄʪµÄ״̬£¬²¢×ªÒƵ½Ò»¸ö´øÓÐ2000mlË®µÄ´óÆ¿»òÉÕ±­ÖС£
They are dissolved by stirring, then the
flask or beaker is cooled down to 0¡ã C by packing
it in ice mixed with salt. When it reaches this
temperature, 200 ml of glacial acetic acid is
added to it with vigorous stirring.
½Á°èʹÆäÈܽ⣬Ȼºó°ÑÆ¿×Ó»òÉÕ±­Âñµ½±ùÑλìºÏÎïÖÐʹÆä½µµ½ 0¡ã C ¡£µ±Ëü½µµ½Õâ¸öζȣ¬ÏòÀïÃæ¼Ó200 ml ±ù´×Ëᣬ±ß¼Ó±ß½Á°è¡£
The chemist must make sure that the temperature does not go
up more than a few degrees while he is adding it.
filters the crystals off it and rinses them a few
times with water.
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2Â¥2013-04-11 21:25:01
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