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求助!!编辑提出要修改G类错误,不知如何处理
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编辑提出: In REFINEMENT item, please, indicate the number of Friedel pairs in the X-ray experiment - see REFLT03_ALERT_4_G; REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 27.70 From the CIF: _reflns_number_total 1994 Count of symmetry unique reflns 1200 Completeness (_total/calc) 166.17% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 794 Fraction of Friedel pairs measured 0.662 Are heavy atom types Z>Si present yes 恳求高手给予帮助!! |
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2楼2007-09-09 12:48:02
celerya
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3楼2007-09-09 13:16:36
paopaomeng
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