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[求助]
求助微谱数据 金币不多 先谢谢各位大虫了
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（1） 150.5,115.0,110.9,103.0,92.4,79.3,76.3,58.8,48.6,43.6,38.3,33.8,27.8,25.8,22.4,22.3,18.9,18.3 氯仿做的 （2）150.5,115.0,110.9,103.0,92.4,79.3,76.3,58.8,48.6,43.6,38.3,33.8,27.8,26.7,25.8,23.0,22.4,22.3,18.9,18.3 氯仿做的 |
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wq0616
铁杆木虫 (正式写手)
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化合物1： 1 . 7β,12α-dihydroxy-13-epi-manoyl oxide C20H34O3 相似度:60% Planta Medica 2009 75 1344-1348 Terpenoids from Roots of Chloranthus henryi Xianwen Gan, LeiMa, Qigang Chen, Qiuqun Chen, Qiang Yu, Lihong Hu Structure 13C NMR 碳谱模拟图 2 . taveuniamide E C19H22Cl3NO3 相似度:57.8% Tetrahedron 2004 60 7025-7033 Taveuniamides: new chlorinated toxins from a mixed assemblage of marine cyanobacteria R.Thomas Williamson, Inder Pal Singh, William H. Gerwick Structure 13C NMR 碳谱模拟图 3 . 13α(or 13β)-isopropenyl-1,5,5-trimethyl-8-methylene-4β,7α-12,14-dioxatricyclo[9.3.0.0(4,7)]-tetradecane C19H30O2 相似度:57.8% Russian Journal of Organic Chemistry 2002 38 519-524 Reactions of Caryophyllene 4β,5α-Epoxide with Carbonyl Compounds on Clay L. E. Tatarova, D. V. Korchagina and V. A. Barkhash Structure 13C NMR 碳谱模拟图 4 . 1a ,7a ,10a ,11a -tetrahydro-derivative 相似度:55.5% Chemical & Pharmaceutical Bulletin 2001 49(12) 1558-1566 Medicinal Foodstuffs. XXVIII.1) Inhibitors of Nitric Oxide Production and New Sesquiterpenes, Zedoarofuran, 4-Epicurcumenol,Neocurcumenol, Gajutsulactones A and B, and Zedoarolides A and B, from Zedoariae Rhizoma Hisashi MATSUDA, Toshio MORIKAWA, Iwao TOGUCHIDA, Kiyofumi NINOMIYA, and Masayuki YOSHIKAWA Structure 13C NMR 碳谱模拟图 5 . 1-O-acetylageratriol 相似度:55.5% Phytochemistry 1999 51 555-558 Further constituents of Achillea ageratum Anake Kijjoa, Luis M. Vieira, Jose A. Pereira, Artur M.S. Silva, Werner Herz Structure 13C NMR 碳谱模拟图 6 . macnabin C15H25O3 相似度:55.5% Phytochemistry 1995 40 857-859 A secoamorphane tri-ether from Cupressus macnabiana foliage Laurence G. Cool, Keni Jiang Structure 13C NMR 碳谱模拟图 7 . compound 25 相似度:55.5% Tetrahedron Letters 2000 41 6643-6647 An enantiospecific approach to thapsanes from R-carvone: synthesis of (−  -thaps-8-en-5-olA. Srikrishna, K. Anebouselvy, T. Jagadeeshwar Reddy Structure 13C NMR 碳谱模拟图 8 . (1R,3S,6R,7R)-7-(tert-butyldimethylsilyloxy)-3,6,10,10-tetramethyltricyclo[4.4.0.01,3]decan-4-one C20H36O2Si 相似度:55.5% Indian Journal of Chemistry 2008 47B 449-459 Enantiospecific synthesis of thaps-8-en-5-ol via stereospecific Srikrishna,A; Anebouselvy,K Structure 13C NMR 碳谱模拟图 9 . (-)-(1S,5S)-3-ethynyl-5-isopropenyl-2,4,4-trimethylcyclohex-2-enyl tert-butyldimethylsilyl ether 相似度:55.5% Indian Journal of Chemistry 2005 44B 1430-1436 Enantiospecific synthesis of B-seco-nortaxanes from two molecules of carvone Srikrishna,A; Kumar,P Praveen; Reddy,T Jagadeeswar Structure 13C NMR 碳谱模拟图 10 . guignardone H C17H24O4 相似度:55.5% Marine Drugs 2012 10 1993-2001 Meroterpenes from Endophytic Fungus A1 of Mangrove Plant Scyphiphora hydrophyllacea Wen-Li Mei, Bo Zheng, You-Xing Zhao, Hui-Ming Zhong, Xun-Li Wu Chen, Yan-Bo Zeng, Wen-Hua Dong, Jiu-Li Huang, Peter Proksch and Hao-Fu Dai Structure 13C NMR 碳谱模拟图 11 . tricycloalternarene F C17H22O4 相似度:55.5% Phytochemistry Letters 2012 5 519-523 Meroterpenes isolated from the endophytic fungus Guignardia mangiferae Denise O. Guimarães, Norberto P. Lopes, Mônica T. Pupo Structure 13C NMR 碳谱模拟图 12 . guignardiaene D 相似度:55.5% Chinese Traditional and Herbal Drugs 2012 43 856-860 Secondary metabolites of endophytic Guignardia mangiferae from Smilax glabra and their antitumor activities LIANG Fa-liang; LI Dong-li; CHEN Yu-chan; TAO Mei-hua; ZHANG Wei-min; ZHANG De-zhi Structure 13C NMR 碳谱模拟图 13 . netidiol B diacetate 相似度:55% Phytochemistry 1998 47 251-254 Abietane diterpenes from Nepeta teydea Braulio M. Fraga, Melchor G. Hernández, Teresa Mestres, JoséM. Arteaga Structure 13C NMR 碳谱模拟图 14 . ent-3α-hydroxy-16-kauren-15-one C20H30O2 相似度:55% Phytochemistry 1996 42 1641-1646 Sesquiterpenoids and diterpenoids from the liverwort Jungermannia truncata Malcolm S. Buchanan, Joseph D. Connolly, Azizol A. Kadir, David S. Rycroft Structure 13C NMR 碳谱模拟图 15 . kaurane-3α,13,16α-triol C20H34O3 相似度:55% Phytochemistry 1989 28 1675-1679 Diterpenoids of the wood of Agathis vitiensis Richard C. Cambie,Jan M. Coddington,Martin J. Stone,Nobutoshi Tanaka,Yong Hua Li,Sayuti Arigayo Structure 13C NMR 碳谱模拟图 16 . (12S,13S)-8,13-epoxy-14-labden-12-ol C20H34O2 相似度:55% Acta Chemica Scandinavica 1977 31 453-459 Tobacco Chemistry. 46. Syntheses of (12R,13S)- and (12S,13R)-8,12-Epoxy-14-labden-13-ol and (12S,13R)-8,13-Epoxy-14-labden-12-ol, Three Tobacco Diterpenoids. Wahlberg, Inger; Curvall, Margareta; Enzell, Curt R. Structure 13C NMR 碳谱模拟图 17 . 7α-acetoxymarrubiin 相似度:55% Journal of the Chemical Society, Perkin Transactions 1 1977 322-324 Structures of three new diterpenoids from Ballota species Giuseppe Savona, Franco Piozzi, James R. Hanson and Michael Siverns Structure 13C NMR 碳谱模拟图 18 . rac-(4R,6aS,11bR)-2,3,4,5,6,6a-Hexahydro-3-phenethyl-1H-4,11b-methanobenzofuro[3,2-d]azocine-10-ol C22H25NO2 相似度:55% Bioorganic & Medicinal Chemistry 2011 19 4330-4337 Probes for narcotic receptor mediated phenomena. 43. Synthesis of the ortho-a and para-a, and improved synthesis and optical resolution of the ortho-b and para-b oxide-bridged phenylmorphans: Compounds with moderate to low opioid-receptor affinity Feng Li, John E. Folk, Kejun Cheng, Muneaki Kurimura, Jason A. Deck, Jeffrey R. Deschamps, Richard B. Rothman, Christina M. Dersch, Arthur E. Jacobson, Kenner C. Rice Structure 13C NMR 碳谱模拟图 19 . rac-(4S,6aR,11bS)-2,3,4,5,6,6a-Hexahydro-3-phenethyl-1H-4,11b-methanobenzofuro[3,2-d]azocine-10-ol C22H25NO2 相似度:55% Bioorganic & Medicinal Chemistry 2011 19 4330-4337 Probes for narcotic receptor mediated phenomena. 43. Synthesis of the ortho-a and para-a, and improved synthesis and optical resolution of the ortho-b and para-b oxide-bridged phenylmorphans: Compounds with moderate to low opioid-receptor affinity Feng Li, John E. Folk, Kejun Cheng, Muneaki Kurimura, Jason A. Deck, Jeffrey R. Deschamps, Richard B. Rothman, Christina M. Dersch, Arthur E. Jacobson, Kenner C. Rice Structure 13C NMR 碳谱模拟图 20 . Ent-3α-hydroxykaur-16-ene 相似度:55% Journal of the Brazilian Chemical Society 2004 15 767-772 Terpenoid Constituents from Leaves of Guarea kunthiana Fernanda R. Garcez, Walmir S. Garcez, Ana Francisca G. da Silva, Rita de Cássia Bazzo and Ubirazilda M. Resende Structure 13C NMR 碳谱模拟图 21 . pachycladin C C22H34O4 相似度:54.5% Journal of Natural Products 2010 73 848-853 Pachycladins A−E, Prostate Cancer Invasion and Migration Inhibitory Eunicellin-Based Diterpenoids from the Red Sea Soft Coral Cladiella pachyclados Hossam M. Hassan, Mohammad A. Khanfar, Ahmed Y. Elnagar, Rabab Mohammed, Lamiaa A. Shaala, Diaa T. A. Youssef, Mohamed S. Hifnawy and Khalid A. El Sayed Structure 13C NMR 碳谱模拟图 22 . compound 18 C19H30O6 相似度:52.6% Planta Medica 2001 67 647-653 New Sesquiterpene Lactones from Elephantopus mollis and Their Leishmanicidal Activities Hiroyuki Fuchino, Tatsuo Koide, Marii Takahashi, Setsuko Sekita, Motoyoshi Satake Structure 13C NMR 碳谱模拟图 23 . (5β,10β)-1-,13-二甲氧基-4,4,10-三甲基-1,2,3,4,5,6,7,10-八氢菲 C19H28O2 相似度:52.6% Chemical Journal of Chinese Universities 2006 27 2101-2105 Synthesis and Anti-tumor Activities of a Series of Novel Tricycle Diterpenes XIONG Yi,WANG Kui-Wu,PAN Yuan-Jiang, SUN Hong-Xiang Structure 13C NMR 碳谱模拟图 化合物2： 1 . 7β,12α-dihydroxy-13-epi-manoyl oxide C20H34O3 相似度:60% Planta Medica 2009 75 1344-1348 Terpenoids from Roots of Chloranthus henryi Xianwen Gan, LeiMa, Qigang Chen, Qiuqun Chen, Qiang Yu, Lihong Hu Structure 13C NMR 碳谱模拟图 2 . pachycladin C C22H34O4 相似度:59.0% Journal of Natural Products 2010 73 848-853 Pachycladins A−E, Prostate Cancer Invasion and Migration Inhibitory Eunicellin-Based Diterpenoids from the Red Sea Soft Coral Cladiella pachyclados Hossam M. Hassan, Mohammad A. Khanfar, Ahmed Y. Elnagar, Rabab Mohammed, Lamiaa A. Shaala, Diaa T. A. Youssef, Mohamed S. Hifnawy and Khalid A. El Sayed Structure 13C NMR 碳谱模拟图 3 . compound 25 相似度:57.8% Tetrahedron Letters 2000 41 6643-6647 An enantiospecific approach to thapsanes from R-carvone: synthesis of (− -thaps-8-en-5-olA. Srikrishna, K. Anebouselvy, T. Jagadeeshwar Reddy Structure 13C NMR 碳谱模拟图 4 . (1R,3S,6R,7R)-7-(tert-butyldimethylsilyloxy)-3,6,10,10-tetramethyltricyclo[4.4.0.01,3]decan-4-one C20H36O2Si 相似度:57.8% Indian Journal of Chemistry 2008 47B 449-459 Enantiospecific synthesis of thaps-8-en-5-ol via stereospecific Srikrishna,A; Anebouselvy,K Structure 13C NMR 碳谱模拟图 5 . 12-Amino-13-methoxytotara-8,11,13-triene 相似度:57.8% Bioorganic & Medicinal Chemistry 2000 8 1653-1662 The synthesis and antibacterial activity of totarol derivatives. part 2: modifications at C-12 and O-13 Gary B Evans, Richard H Furneaux Structure 13C NMR 碳谱模拟图 6 . taveuniamide E C19H22Cl3NO3 相似度:57.8% Tetrahedron 2004 60 7025-7033 Taveuniamides: new chlorinated toxins from a mixed assemblage of marine cyanobacteria R.Thomas Williamson, Inder Pal Singh, William H. Gerwick Structure 13C NMR 碳谱模拟图 7 . 13α(or 13β)-isopropenyl-1,5,5-trimethyl-8-methylene-4β,7α-12,14-dioxatricyclo[9.3.0.0(4,7)]-tetradecane C19H30O2 相似度:57.8% Russian Journal of Organic Chemistry 2002 38 519-524 Reactions of Caryophyllene 4β,5α-Epoxide with Carbonyl Compounds on Clay L. E. Tatarova, D. V. Korchagina and V. A. Barkhash Structure 13C NMR 碳谱模拟图 8 . (13R,18R)-5,18:13,18-diepoxyserrulaten-8-ol C20H28O3 相似度:57.8% Australian Journal of Chemistry 1985 38 1837-1845 The Structure of a Stable Serrulatane Diterpenoid Acetal From Eremophila-Rotundifolia AD Abell, E Horn, GP Jones, MR Snow, RA Massywestropp and R Riccio Structure 13C NMR 碳谱模拟图 9 . 3,4-dihydroxyclerodan-13Z-en-15-oic acid 相似度:55% Journal of Natural Products 2006 69 768-773 Bioactive Diterpenes from the Fruits of Detarium microcarpum Anne-Laure Cavin, Anne-Emmanuelle Hay, Andrew Marston, Helen Stoeckli-Evans, Rosario Scopelliti, Drissa Diallo, and Kurt Hostettmann Structure 13C NMR 碳谱模拟图 10 . polasol A C20H32O2 相似度:55% Journal of Natural Products 1998 61 945-947 Polasols A-C, Three New Diterpenes from the Marine Sponge Epipolasis sp. Akemi Umeyama, Miharu Nozaki, and Shigenobu Arihara Structure 13C NMR 碳谱模拟图 11 . netidiol B diacetate 相似度:55% Phytochemistry 1998 47 251-254 Abietane diterpenes from Nepeta teydea Braulio M. Fraga, Melchor G. Hernández, Teresa Mestres, JoséM. Arteaga Structure 13C NMR 碳谱模拟图 12 . ent-3α-hydroxy-16-kauren-15-one C20H30O2 相似度:55% Phytochemistry 1996 42 1641-1646 Sesquiterpenoids and diterpenoids from the liverwort Jungermannia truncata Malcolm S. Buchanan, Joseph D. Connolly, Azizol A. Kadir, David S. Rycroft Structure 13C NMR 碳谱模拟图 13 . triptoquinone C C20H28O4 相似度:55% Phytochemistry 1994 35 731-737 Tripterygium wilfordii var. regelii which are interleukin-1 inhibitors Kozo Shishido, Kimiko Nakano, Noriko Wariishi, Hideo Tateishi, Tomoki Omodani, Masayuki Shibuya, Kiyoto Goto, Yukihisa Ono, Yoshihisa Takaishi Structure 13C NMR 碳谱模拟图 14 . Cladieunicellin D C20H32O5 相似度:55% Chemical & Pharmaceutical Bulletin 2011 59(3) 353-358 Cladieunicellins A-E, New Eunicellins from an Indonesian Soft Coral Cladiella sp. Yung-Husan CHEN, Chia-Ying TAI, Yueh-Hsiung KUO, Chia-Ying KAO, Jan-Jung LI,Tsong-Long HWANG, Lee-Shing FANG, Wei-Hsien WANG, Jyh-Horng SHEU, and Ping-Jyun SUNG Structure 13C NMR 碳谱模拟图 15 . kaurane-3α,13,16α-triol C20H34O3 相似度:55% Phytochemistry 1989 28 1675-1679 Diterpenoids of the wood of Agathis vitiensis Richard C. Cambie,Jan M. Coddington,Martin J. Stone,Nobutoshi Tanaka,Yong Hua Li,Sayuti Arigayo Structure 13C NMR 碳谱模拟图 16 . ent-(13S),15β-dihydroxy-atis-16-ene-3,14-dione C20H28O4 相似度:55% Phytochemistry 1990 29 1925-1935 Ent-atisane diterpenes from Euphorbia fidjiana Allick R. Lal,Richard C. Cambie,Peter S. Rutledge,Paul D. Woodgate Structure 13C NMR 碳谱模拟图 17 . 3α-Hinokiol 相似度:55% Pharmazie 2002 57 343-345 Terpenes from Juniperus przewalskii and their antitumor activities Wen-Shu Wang - Er-Wei Li - Zhong-Jian Jia Structure 13C NMR 碳谱模拟图 18 . (12S,13S)-8,13-epoxy-14-labden-12-ol C20H34O2 相似度:55% Acta Chemica Scandinavica 1977 31 453-459 Tobacco Chemistry. 46. Syntheses of (12R,13S)- and (12S,13R)-8,12-Epoxy-14-labden-13-ol and (12S,13R)-8,13-Epoxy-14-labden-12-ol, Three Tobacco Diterpenoids. Wahlberg, Inger; Curvall, Margareta; Enzell, Curt R. Structure 13C NMR 碳谱模拟图 19 . neoverrucosanol 相似度:55% Chemistry Letters 1997 26 489-490 Umabanol, a New Tetracyclic Diterpene from a Marine Sponge Junichi Tanaka, Irvina Nurrachmi and Tatsuo Higa Structure 13C NMR 碳谱模拟图 20 . 7α-acetoxymarrubiin 相似度:55% Journal of the Chemical Society, Perkin Transactions 1 1977 322-324 Structures of three new diterpenoids from Ballota species Giuseppe Savona, Franco Piozzi, James R. Hanson and Michael Siverns Structure 13C NMR 碳谱模拟图 21 . (4R,7S)-1-(tert-butyldiphenylsilanyloxy)-9-([1,3]dithian-2-yl)-7-methyl-6-methylene-nonan-4-ol C31H46O2S2Si 相似度:55% Canadian Journal of Chemistry 2004 82 120-130 Diastereoselectivity in asymmetric allylations: The role of vicinal chirality in the allyl nucleophile for SE2′ reactions with aldehydes David R Williams, Kevin G Meyer, Khalida Shamim, Samarjit Patnaik Structure 13C NMR 碳谱模拟图 22 . rac-(4R,6aS,11bR)-2,3,4,5,6,6a-Hexahydro-3-phenethyl-1H-4,11b-methanobenzofuro[3,2-d]azocine-10-ol C22H25NO2 相似度:55% Bioorganic & Medicinal Chemistry 2011 19 4330-4337 Probes for narcotic receptor mediated phenomena. 43. Synthesis of the ortho-a and para-a, and improved synthesis and optical resolution of the ortho-b and para-b oxide-bridged phenylmorphans: Compounds with moderate to low opioid-receptor affinity Feng Li, John E. Folk, Kejun Cheng, Muneaki Kurimura, Jason A. Deck, Jeffrey R. Deschamps, Richard B. Rothman, Christina M. Dersch, Arthur E. Jacobson, Kenner C. Rice Structure 13C NMR 碳谱模拟图 23 . rac-(4S,6aR,11bS)-2,3,4,5,6,6a-Hexahydro-3-phenethyl-1H-4,11b-methanobenzofuro[3,2-d]azocine-10-ol C22H25NO2 相似度:55% Bioorganic & Medicinal Chemistry 2011 19 4330-4337 Probes for narcotic receptor mediated phenomena. 43. Synthesis of the ortho-a and para-a, and improved synthesis and optical resolution of the ortho-b and para-b oxide-bridged phenylmorphans: Compounds with moderate to low opioid-receptor affinity Feng Li, John E. Folk, Kejun Cheng, Muneaki Kurimura, Jason A. Deck, Jeffrey R. Deschamps, Richard B. Rothman, Christina M. Dersch, Arthur E. Jacobson, Kenner C. Rice Structure 13C NMR 碳谱模拟图 24 . Ent-3α-hydroxykaur-16-ene 相似度:55% Journal of the Brazilian Chemical Society 2004 15 767-772 Terpenoid Constituents from Leaves of Guarea kunthiana Fernanda R. Garcez, Walmir S. Garcez, Ana Francisca G. da Silva, Rita de Cássia Bazzo and Ubirazilda M. Resende Structure 13C NMR 碳谱模拟图 |
2楼2013-03-21 15:43:44