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zyz943

银虫 (小有名气)

[求助] 什么是CMS方法

今天看文献,文献中提到CMS method,我不太明白,不知有人是否做过。给我指教指教。具体实验方法如下:
PbMoO4 dendritic nanocrystals have been synthesized by the CMS
method. Typically, 3 g of LiNO3 and KNO3 with mass ratio of 1:2
were mixed in a Teflon vessel of 25 mL capacity. Then, 1 mmol of
Pb(NO3)2 and H2MoO4 and 4 mL ammonia solution (pH 9) were
added in the Teflon vessel. After reacting at 180 ◦C for 23 h in a
furnace, the vessel was taken out and allowed to cool at room temperature
naturally. Finally, the sample was obtained after washing
the product several times with distilled water and absolute ethanol.
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freelover

铁杆木虫 (著名写手)

没做过……
看到文献里有人写成“composite-molten-salt (CMS) method”,大概如此。
2楼2013-01-24 08:55:34
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