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杨大松

至尊木虫 (文坛精英)

[求助] 求助微谱数据,谢谢

碳谱数据如下:
19.0,19.3,24.6,27.9,31.3,33.1,34.4,40.1,42.1,124.8,125.3,134.1,145.1,173.1
辛苦各位了,非常感谢
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【答案】应助回帖

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杨大松: 金币+15, ★★★★★最佳答案 2013-01-21 15:47:15
1 .     macrophyllic acid A
C15H22O2     相似度:80%
Journal of Natural Products          2001          64          466-471
Sesquiterpenes and Monoterpenes from the Bark of Inula macrophylla
Bao-Ning Su,Yoshihisa Takaishi, Tetsuya Yabuuchi, Takenori Kusumi, Motoo Tori,Shigeru Takaoka,Gisho Honda, Michiho Ito, Yoshio Takeda, Olimjon K. Kodzhimatov, and Ozodbek Ashurmetov
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     macrophyllic acid A
C15H22O2     相似度:80%
Tetrahedron Letters          2000          41          2395-2400
The structures and absolute configurations of macrophyllic acids A–E, five new rearranged eudesmane sesquiterpene acids from the bark of Inula macrophylla
Bao-Ning Su, Yoshihisa Takaishi, Tetsuya Yabuuchi, Takenori Kusumi, Motoo Tori, Shigeru Takaoka
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     γ-selinene
    相似度:73.3%
Journal of Natural Products          1996          59          409-411
Constituents of Persea japonica
Chao-Chiun Wang, Chang-Sheng Kuoh and Tian-Shung Wu
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     γ-Costol
C15H24O     相似度:73.3%
Phytochemistry          1996          41          243-246
Two guaiane and eudesmane-type sesquiterpenoids from Neocallitropsis pancheri
Phila Raharivelomanana, Jean-Pierre Bianchini, Robert Faure, Aimé Cambon, Marcel Azzaro
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

5 .     γ-costic acid methyl esther[methyl 2-((2R,4aR)-4a,8-dimethyl-1,2,3,4,4a,5,6,7-octahydronaphthalen-2-yl)acrylate]
C16H24O2     相似度:68.7%
Bioorganic & Medicinal Chemistry          2009          17          6251-6256
Tessaric acid derivatives induce G2/M cell cycle arrest in human solid tumor cell lines
Leticia G. León, Osvaldo J. Donadel, Carlos E. Tonn, José M. Padrón
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

6 .     1β-hydroxyeudesma-4,11(13)-dien-12-oic acid
C15H22O3     相似度:66.6%
Chemical & Pharmaceutical Bulletin          1987          35          2272-2279
Studies on the Sesquiterpenes from Ambrosia elatior LINNÉ
TAICHI OHMOTO,KEIJI IKEDA,SACHIYO NOMURA,MASARU SHIMIZU and SACHI SAITO
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

7 .     9-oxo-4,11(13)-eudesmedien-12-oic acid
    相似度:66.6%
Phytochemistry          1990          29          877-879
Sesquiterpenes and flavonoids from Tessaria species
E. Guerreiro,M.J. Pestchanker,L.Del Vitto,O.S. Giordano
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

8 .     compound 2
    相似度:66.6%
Pharmazie          2002          57          59-61
Microbiological conversion of a - and -eudesmol mixture by Rhizopus
G.T. Maatooq - J.J. Hoffmann
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

9 .     γ-eudesmol
    相似度:66.6%
Zeitschrift für Naturforschung C          2002          57          654-659
Microbial Transformation of a b- and g-Eudesmols Mixture
G. T. Maatooq
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

10 .     γ-costic acid[2-((2R,4aR)-4a,8-dimethyl-1,2,3,4,4a,5,6,7-octahydronaphthalen-2-yl)acrylic acid]
C15H22O2     相似度:64.7%
Bioorganic & Medicinal Chemistry          2009          17          6251-6256
Tessaric acid derivatives induce G2/M cell cycle arrest in human solid tumor cell lines
Leticia G. León, Osvaldo J. Donadel, Carlos E. Tonn, José M. Padrón
2楼2013-01-21 15:44:35
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杨大松

至尊木虫 (文坛精英)

辛苦你了,非常感谢。
碧雪清谭
3楼2013-01-21 15:47:32
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