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123飞鸟

铜虫 (小有名气)

[求助] 求助微谱数据

化合物1:16.2, 16.9, 17.2, 17.9, 19.5, 19.6, 22.7, 22.9, 25.6, 25.9, 26.6, 28.9, 29.2, 29.3, 32.4, 34.9, 35.0, 36.6, 38.5, 38.7, 38.8, 42.0, 43.7, 50.8, 51.2, 51.8, 51.9, 76.2, 77.2, 78.4 (125 MHz, CD3OD)
化合物2:15.4, 17.6, 18.3, 20.1, 22.9, 24.3, 25.0, 26.1, 26.4, 26.5, 27.5, 27.6, 28.1, 29.1, 33.1, 35.8, 37.5, 37.6, 39.8, 40.9, 44.9, 45.7, 56.7, 57.8, 70.5, 76.2, 85.0, 85.8, 87.8, 89.7 (125 MHz, CDCL3)
结果越详细越好,谢谢!邮箱 kyzhy01@163.com
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木虫 (小有名气)

【答案】应助回帖

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123飞鸟: 金币+20, ★★★很有帮助, 谢谢! 2013-01-21 16:44:50
化合物1
1 .     atriplicoide B
C30H48O4     相似度:73.3%
Natural Product Communications          2011          6          179-182
Two New Triterpenoids from Zygophyllum eurypterum
Shazia Iqbal, Afsar Khan, Viqar Uddin Ahma, Murad Ali Khan, Sadia Bader, Umar Farooq, Saleha Suleman Khan, Aqib Zahoor and Rasool Bakhsh Tareen
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     phyllolactone B
C30H46O5     相似度:70%
Tetrahedron          2001          57          5731-5738
Phyllolactones A-E: new bishomoscalarane sesterterpenes from the marine sponge Phyllospongia lamellosa
Leng Chee Chang, Sarah Otero-Quintero, Gillian M Nicholas, Carole A Bewley
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     betalnoside B
C35H60O7     相似度:68.5%
Phytochemistry Letters          2011          4          179-182
Three new dammarane glycosides from Betula alnoides
Minh Giang Phan, Thi To Chinh Truong, Tong Son Phan, Katsuyoshi Matsunami, Hideaki Otsuka
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     betulin
C30H50O2     相似度:66.6%
Chinese Journal of Natural Medicines          2003          1          82-84
Chemical Constituents of Chaenomeles sinensis(Thouin)Koehne
GAO Hui Yuan; WU Li Jun; KUROYANAGI Masanori
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

5 .     olean-12-ene-3β,29-diol
C30H50O2     相似度:66.6%
Natural Product Communications          2006          1          613-617
Triterpenoids, Including One with Smooth Muscle RelaxantActivity, from Rubus idaeus (Raspberry) Leaves
Janne Rojas Vera, b, Christopher G. Dacke, Asmita V. Patel and Gerald Blunden
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

6 .     sapinmusaponin A
C42H72O13     相似度:66.6%
Journal of Agricultural and Food Chemistry          2005          53          4722-4727
New Dammarane-Type Saponins from the Galls of Sapindus mukorossi
Yao-Haur Kuo, Hui-Chi Huang, Li-Ming Yang Kuo, Ya-Wen Hsu, Kuo-Hsiung Lee, Fang-Rong Chang, and Yang-Chang Wu
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

7 .     ophirapstanol trisulfate
C31H53O12S3Na3     相似度:64.5%
Journal of Natural Products          1994          Vol 57          1751
Ophirapstanol Trisulfate, a New Biologically Active Steroid Sulfate from the Deep Water Marine Sponge Topsentia ophiraphidites
Sarath P. Gunasekera, Susan H. Sennett, Michelle Kelly-Borges, Robert W. Bryant
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

8 .     phyllolactone A
C31H48O5     相似度:64.5%
Tetrahedron          2001          57          5731-5738
Phyllolactones A-E: new bishomoscalarane sesterterpenes from the marine sponge Phyllospongia lamellosa
Leng Chee Chang, Sarah Otero-Quintero, Gillian M Nicholas, Carole A Bewley
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

9 .     sapinmusaponin D
C43H74O14     相似度:64.5%
Journal of Agricultural and Food Chemistry          2005          53          4722-4727
New Dammarane-Type Saponins from the Galls of Sapindus mukorossi
Yao-Haur Kuo, Hui-Chi Huang, Li-Ming Yang Kuo, Ya-Wen Hsu, Kuo-Hsiung Lee, Fang-Rong Chang, and Yang-Chang Wu
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

10 .     serrulatin E
C30H50O6     相似度:63.3%
Helvetica Chimica Acta          2008          Vol. 91          665
Triterpenoids from the Edible Leaves of Photinia serrulata
Ya-Ling Song, Yue-Hu Wang, Qing Lu, Hui-Jun Qiao, and Yong-Xian Cheng

化合物2:
1 .     Soyasapooenol G
C31H48O4     相似度:70.9%
Phytochemistry          1996          41          1573-1577
Triterpenoids from Melilotus messanensis; soyasapogenol G, the first natural carbonate derivative
Francisco A. Macías*, Ana M. Simonet, M. Dolores Esteban, Juan Carlos G. Galindo
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     3α,5α,19β,28-diepoxy-A-neo-18α-oleane
C30H48O2     相似度:70%
Chemistry of Natural Compounds          2006          42          618-619
STRUCTURE OF THE MINOR OZONOLYSIS PRODUCT OF 19b,28-EPOXY-A-neo-18a-OLEAN-3(5)-ENE
N. I. Medvedeva, O. B. Flekhter,A. Gzella, and L. Zaprutko
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     soyasapogenol
C30H50O3     相似度:70%
Acta Pharmaceutica Sinica          1993          28          116-121
STUDIES ON THE TRITERPENOIDS FROM ROOTS OF GLYCYRRHIZA SQUAMULOSA FROANCH
H Liang and RY Zhang
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     Soyasapogenol B
C30H50O3     相似度:70%
Journal of Asian Natural Products Research          2005          7          237-243
Three new isoprenylated flavonoids from the roots of Sophora flavescens
PEI-LAN DING, AI-JUN HOU and DAO-FENG CHEN
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

5 .     Soyasapogenol B
    相似度:70%
Phytochemistry          1996          41          1573-1577
Triterpenoids from Melilotus messanensis; soyasapogenol G, the first natural carbonate derivative
Francisco A. Macías*, Ana M. Simonet, M. Dolores Esteban, Juan Carlos G. Galindo
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

6 .     19β,28-Epoxy-A-neo-5β-methyl-25-nor-18α-olean-9-ene
C30H48O     相似度:70%
Chemistry of Natural Compounds          2011          Vol. 47, No. 4          579-582
ALLYLIC OXIDATION OF 19β,28-EPOXY-A-NEO-5 -METHYL-25-NOR-18α-OLEAN-9-ENE
O. B. Kazakova, E. F. Khusnutdinova, A. N. Lobov,N. I. Medvedeva, and L. V. Spirikhin
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

7 .     soyasapogenol B
    相似度:70%
China Journal of Chinese Materia Medica          2010          35          607-609
Chemical constituents in Flos Sophorae Carbonisatus
LI Raorao*; WANG Caifang; LEI Peilin; HUANG Lanlan; YUAN Sitong
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

8 .     Artabotryol A
C30H48O3     相似度:70%
Helvetica Chimica Acta          2010          93          1925-1932
Artabotryols A – E, New Lanostane Triterpenes from the Seeds of Artabotrys odoratissimus
Chitrasen Gupta, Subedar Prasad, Mahendra Sahai, Teigo Asai, Noriyuki Hara and Yoshinori Fujimoto
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

9 .     Artabotryol B
C30H50O3     相似度:70%
Helvetica Chimica Acta          2010          93          1925-1932
Artabotryols A – E, New Lanostane Triterpenes from the Seeds of Artabotrys odoratissimus
Chitrasen Gupta, Subedar Prasad, Mahendra Sahai, Teigo Asai, Noriyuki Hara and Yoshinori Fujimoto
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

10 .     Soyasapogenol B
    相似度:70%
Chinese Journal of Medicinal Chemistry          2008          18          142-156
Chemical constituents of processed Astragalus membranaceus Bunge
LIU Wei, WANG Zhi-cheng, LIANG Fei-fei, LI Xian, WANG Jin-hui
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