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[求助]
【求助】哪位高手有JCPDS 卡片
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【求助】哪位高手能帮忙找一下能与Gd2(MoO)3匹配的JCPDS 70-1397 非常感谢！ |
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gyliu
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PDF#70-1397: QM=Calculated(C); d=Calculated; I=Calculated Gadolinium Molybdenum Oxide Gd2 ( Mo O4 )3 Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=8.256-70.058 I/Ic(RIR)=1.96 Ref: Calculated from ICSD using POWD-12++ (1997) Orthorhombic - (Unknown), Pba2 (32) Z=4 mp= CELL: 10.3881 x 10.4194 x 10.7007 <90.0 x 90.0 x 90.0> P.S=oP68 (?) Density(c)=4.554 Density(m)=4.565 Mwt=794.31 Vol=1158.22 F(30)=45.1(.0125,53/0) Ref: Jeitschko, W. Acta Crystallogr., Sec. B, v28 p60 (1972) Strong Lines: 3.48/X 3.03/9 3.73/9 3.29/9 4.67/9 3.68/7 5.35/7 2.94/7 3.57/6 1.98/5 FIZ=002707: ATF See PDF 01-071-0915. A comprehensive X-ray study of the ferroelectric-ferroelastic and paraelectric-paraelastic phases of Gd2 (Mo O4)3 c17 (PBA2) A2B3X12 2-Theta d(?) I(v) ( h k l ) Theta 1/(2d) 2pi/d n^2 8.256 10.7007 7.3 ( 0 0 1) 4.128 0.0467 0.5872 12.021 7.3565 <1 ( 1 1 0) 6.010 0.0680 0.8541 14.600 6.0622 17.4 ( 1 1 1) 7.300 0.0825 1.0365 16.555 5.3503 42.4 ( 0 0 2) 8.278 0.0935 1.1744 17.005 5.2097 5.4 ( 0 2 0) 8.503 0.0960 1.2061 17.005 5.2097 5.4 ( 2 0 0) 8.503 0.0960 1.2061 18.977 4.6727 58.6 ( 1 2 0) 9.488 0.1070 1.3447 18.977 4.6727 58.6 ( 2 0 1) 9.488 0.1070 1.3447 20.509 4.3270 6.5 ( 1 1 2) 10.254 0.1156 1.4521 20.785 4.2701 1.5 ( 2 1 1) 10.393 0.1171 1.4715 20.785 4.2701 1.5 ( 1 2 1) 10.393 0.1171 1.4715 23.819 3.7325 76.6 ( 0 2 2) 11.910 0.1340 1.6833 23.819 3.7325 76.6 ( 2 0 2) 11.910 0.1340 1.6833 24.176 3.6783 64.5 ( 2 2 0) 12.088 0.1359 1.7082 24.943 3.5669 57.0 ( 0 0 3) 12.471 0.1402 1.7615 25.587 3.4785 92.3 ( 2 2 1) 12.794 0.1437 1.8063 27.048 3.2939 85.6 ( 3 1 0) 13.524 0.1518 1.9075 27.048 3.2939 85.6 ( 1 3 0) 13.524 0.1518 1.9075 27.773 3.2095 11.1 ( 1 1 3) 13.886 0.1558 1.9577 28.389 3.1412 14.8 ( 3 1 1) 14.195 0.1592 2.0002 28.389 3.1412 14.8 ( 1 3 1) 14.195 0.1592 2.0002 29.444 3.0311 100.0 ( 2 2 2) 14.722 0.1650 2.0729 30.344 2.9432 75.5 ( 2 0 3) 15.172 0.1699 2.1348 30.344 2.9432 75.5 ( 0 2 3) 15.172 0.1699 2.1348 31.591 2.8298 1.9 ( 1 2 3) 15.795 0.1767 2.2203 31.591 2.8298 1.9 ( 2 1 3) 15.795 0.1767 2.2203 31.935 2.8001 48.6 ( 3 1 2) 15.968 0.1786 2.2439 31.935 2.8001 48.6 ( 1 3 2) 15.968 0.1786 2.2439 33.469 2.6752 7.2 ( 0 0 4) 16.734 0.1869 2.3487 34.400 2.6049 20.0 ( 0 4 0) 17.200 0.1919 2.4121 34.507 2.5970 27.1 ( 4 0 0) 17.254 0.1925 2.4194 35.013 2.5607 4.5 ( 2 2 3) 17.507 0.1953 2.4537 35.438 2.5309 2.3 ( 0 4 1) 17.719 0.1976 2.4826 35.542 2.5238 3.6 ( 4 0 1) 17.771 0.1981 2.4896 35.542 2.5238 3.6 ( 1 4 0) 17.771 0.1981 2.4896 35.598 2.5199 3.7 ( 4 1 0) 17.799 0.1984 2.4934 36.510 2.4590 0.7 ( 1 4 1) 18.255 0.2033 2.5552 36.605 2.4528 0.8 ( 4 1 1) 18.303 0.2038 2.5616 36.605 2.4528 0.8 ( 3 3 0) 18.303 0.2038 2.5616 37.121 2.4199 11.0 ( 3 1 3) 18.561 0.2066 2.5965 37.121 2.4199 11.0 ( 1 3 3) 18.561 0.2066 2.5965 37.600 2.3902 20.8 ( 3 3 1) 18.800 0.2092 2.6287 38.403 2.3420 1.6 ( 0 4 2) 19.202 0.2135 2.6828 38.636 2.3284 20.8 ( 2 4 0) 19.318 0.2147 2.6985 38.709 2.3242 26.1 ( 4 2 0) 19.354 0.2151 2.7033 39.578 2.2752 1.8 ( 2 4 1) 19.789 0.2198 2.7616 39.649 2.2713 1.7 ( 4 2 1) 19.824 0.2201 2.7664 40.149 2.2441 0.3 ( 3 2 3) 20.075 0.2228 2.7998 40.149 2.2441 0.3 ( 2 3 3) 20.075 0.2228 2.7998 40.430 2.2292 0.1 ( 3 3 2) 20.215 0.2243 2.8186 41.714 2.1635 1.9 ( 2 2 4) 20.857 0.2311 2.9042 42.191 2.1401 2.9 ( 0 0 5) 21.095 0.2336 2.9359 42.297 2.1350 6.2 ( 2 4 2) 21.148 0.2342 2.9429 42.364 2.1318 5.9 ( 4 2 2) 21.182 0.2345 2.9474 42.959 2.1036 20.0 ( 0 4 3) 21.480 0.2377 2.9868 43.048 2.0995 26.8 ( 4 0 3) 21.524 0.2382 2.9927 43.547 2.0766 7.3 ( 3 1 4) 21.773 0.2408 3.0257 43.547 2.0766 7.3 ( 1 3 4) 21.773 0.2408 3.0257 43.876 2.0618 3.1 ( 1 4 3) 21.938 0.2425 3.0475 44.029 2.0549 11.7 ( 1 1 5) 22.014 0.2433 3.0576 44.296 2.0432 11.9 ( 1 5 0) 22.148 0.2447 3.0752 44.296 2.0432 11.9 ( 4 3 1) 22.148 0.2447 3.0752 44.426 2.0375 15.3 ( 5 1 0) 22.213 0.2454 3.0838 44.815 2.0207 63.2 ( 3 3 3) 22.407 0.2474 3.1094 45.140 2.0069 8.5 ( 1 5 1) 22.570 0.2491 3.1308 45.268 2.0015 10.4 ( 5 1 1) 22.634 0.2498 3.1392 45.798 1.9796 73.6 ( 0 2 5) 22.899 0.2526 3.1740 45.798 1.9796 73.6 ( 2 0 5) 22.899 0.2526 3.1740 46.251 1.9612 2.5 ( 3 2 4) 23.126 0.2549 3.2037 46.251 1.9612 2.5 ( 2 3 4) 23.126 0.2549 3.2037 46.539 1.9498 29.3 ( 2 4 3) 23.270 0.2564 3.2225 46.602 1.9473 31.3 ( 4 2 3) 23.301 0.2568 3.2266 47.601 1.9087 6.7 ( 1 5 2) 23.801 0.2620 3.2918 47.724 1.9041 9.9 ( 5 1 2) 23.862 0.2626 3.2998 47.724 1.9041 9.9 ( 2 5 1) 23.862 0.2626 3.2998 47.856 1.8992 4.4 ( 5 2 1) 23.928 0.2633 3.3084 48.754 1.8663 3.6 ( 0 4 4) 24.377 0.2679 3.3667 48.834 1.8634 4.0 ( 4 0 4) 24.417 0.2683 3.3719 49.216 1.8498 7.8 ( 2 2 5) 24.608 0.2703 3.3967 49.521 1.8391 8.7 ( 4 4 0) 24.761 0.2719 3.4164 49.661 1.8343 5.8 ( 4 1 4) 24.830 0.2726 3.4254 50.111 1.8189 0.5 ( 2 5 2) 25.056 0.2749 3.4545 50.297 1.8126 1.2 ( 4 4 1) 25.149 0.2759 3.4665 50.443 1.8077 1.2 ( 3 3 4) 25.222 0.2766 3.4759 50.875 1.7933 11.1 ( 3 1 5) 25.437 0.2788 3.5036 50.875 1.7933 11.1 ( 1 3 5) 25.437 0.2788 3.5036 51.114 1.7855 34.3 ( 3 5 0) 25.557 0.2800 3.5190 51.192 1.7830 37.8 ( 0 0 6) 25.596 0.2804 3.5240 51.192 1.7830 37.8 ( 5 3 0) 25.596 0.2804 3.5240 51.503 1.7729 22.3 ( 1 5 3) 25.752 0.2820 3.5440 51.619 1.7692 29.0 ( 5 1 3) 25.810 0.2826 3.5514 51.873 1.7611 14.8 ( 3 5 1) 25.937 0.2839 3.5677 52.025 1.7563 21.6 ( 2 4 4) 26.013 0.2847 3.5774 52.083 1.7545 20.5 ( 4 2 4) 26.041 0.2850 3.5811 52.663 1.7366 9.1 ( 0 6 0) 26.331 0.2879 3.6182 52.834 1.7313 12.4 ( 6 0 0) 26.417 0.2888 3.6291 52.834 1.7313 12.4 ( 1 1 6) 26.417 0.2888 3.6291 53.406 1.7141 5.8 ( 1 6 0) 26.703 0.2917 3.6655 53.406 1.7141 5.8 ( 0 6 1) 26.703 0.2917 3.6655 53.576 1.7091 8.1 ( 6 0 1) 26.788 0.2925 3.6763 53.576 1.7091 8.1 ( 6 1 0) 26.788 0.2925 3.6763 54.104 1.6937 27.7 ( 3 5 2) 27.052 0.2952 3.7098 54.179 1.6915 29.6 ( 1 6 1) 27.089 0.2956 3.7145 54.179 1.6915 29.6 ( 5 3 2) 27.089 0.2956 3.7145 54.324 1.6873 35.2 ( 2 0 6) 27.162 0.2963 3.7238 54.324 1.6873 35.2 ( 0 2 6) 27.162 0.2963 3.7238 55.110 1.6651 1.0 ( 1 2 6) 27.555 0.3003 3.7734 55.110 1.6651 1.0 ( 2 1 6) 27.555 0.3003 3.7734 55.595 1.6517 25.7 ( 4 0 5) 27.797 0.3027 3.8040 55.595 1.6517 25.7 ( 0 6 2) 27.797 0.3027 3.8040 55.759 1.6473 27.9 ( 2 6 0) 27.880 0.3035 3.8143 55.759 1.6473 27.9 ( 6 0 2) 27.880 0.3035 3.8143 55.922 1.6429 10.2 ( 3 4 4) 27.961 0.3043 3.8246 55.922 1.6429 10.2 ( 4 3 4) 27.961 0.3043 3.8246 56.227 1.6346 8.6 ( 1 4 5) 28.114 0.3059 3.8438 56.227 1.6346 8.6 ( 4 4 3) 28.114 0.3059 3.8438 56.355 1.6313 6.7 ( 4 1 5) 28.177 0.3065 3.8518 56.355 1.6313 6.7 ( 1 6 2) 28.177 0.3065 3.8518 56.485 1.6278 11.2 ( 2 6 1) 28.243 0.3072 3.8599 56.485 1.6278 11.2 ( 6 1 2) 28.243 0.3072 3.8599 56.630 1.6240 13.8 ( 1 5 4) 28.315 0.3079 3.8691 56.630 1.6240 13.8 ( 6 2 1) 28.315 0.3079 3.8691 56.747 1.6209 5.9 ( 5 1 4) 28.373 0.3085 3.8763 57.073 1.6124 32.3 ( 3 3 5) 28.536 0.3101 3.8967 57.287 1.6069 18.0 ( 4 5 1) 28.644 0.3112 3.9102 57.370 1.6048 7.4 ( 2 2 6) 28.685 0.3116 3.9153 57.690 1.5966 11.9 ( 3 5 3) 28.845 0.3132 3.9353 57.762 1.5948 12.7 ( 5 3 3) 28.881 0.3135 3.9397 58.531 1.5757 20.0 ( 2 6 2) 29.265 0.3173 3.9876 58.531 1.5757 20.0 ( 2 4 5) 29.265 0.3173 3.9876 58.738 1.5706 15.1 ( 6 2 2) 29.369 0.3183 4.0005 58.832 1.5683 8.8 ( 1 3 6) 29.416 0.3188 4.0063 58.832 1.5683 8.8 ( 3 1 6) 29.416 0.3188 4.0063 59.279 1.5576 2.1 ( 6 0 3) 29.640 0.3210 4.0340 59.420 1.5542 1.2 ( 5 4 2) 29.710 0.3217 4.0427 59.420 1.5542 1.2 ( 4 5 2) 29.710 0.3217 4.0427 59.619 1.5495 0.4 ( 6 3 0) 29.809 0.3227 4.0550 59.852 1.5440 0.2 ( 1 6 3) 29.926 0.3238 4.0694 60.005 1.5404 0.8 ( 6 1 3) 30.003 0.3246 4.0788 60.187 1.5362 0.8 ( 3 6 1) 30.093 0.3255 4.0900 60.305 1.5335 1.0 ( 6 3 1) 30.152 0.3261 4.0973 60.515 1.5287 0.6 ( 0 0 7) 30.258 0.3271 4.1102 61.095 1.5155 0.2 ( 4 4 4) 30.548 0.3299 4.1458 61.095 1.5155 0.2 ( 3 2 6) 30.548 0.3299 4.1458 62.015 1.4953 10.3 ( 2 6 3) 31.007 0.3344 4.2021 62.152 1.4923 13.8 ( 3 6 2) 31.076 0.3351 4.2104 62.152 1.4923 13.8 ( 6 2 3) 31.076 0.3351 4.2104 62.335 1.4883 6.9 ( 6 3 2) 31.168 0.3359 4.2216 62.487 1.4851 5.4 ( 3 5 4) 31.243 0.3367 4.2308 62.555 1.4836 5.4 ( 5 3 4) 31.277 0.3370 4.2350 62.829 1.4778 20.2 ( 5 4 3) 31.414 0.3383 4.2516 62.829 1.4778 20.2 ( 1 5 5) 31.414 0.3383 4.2516 62.930 1.4757 22.2 ( 5 1 5) 31.465 0.3388 4.2578 63.037 1.4734 18.1 ( 1 7 0) 31.519 0.3393 4.2643 63.126 1.4716 14.4 ( 5 5 0) 31.563 0.3398 4.2697 63.126 1.4716 14.4 ( 0 4 6) 31.563 0.3398 4.2697 63.241 1.4692 11.1 ( 4 0 6) 31.620 0.3403 4.2766 63.241 1.4692 11.1 ( 7 1 0) 31.620 0.3403 4.2766 63.354 1.4668 11.6 ( 2 0 7) 31.677 0.3409 4.2835 63.354 1.4668 11.6 ( 0 2 7) 31.677 0.3409 4.2835 63.702 1.4597 2.9 ( 1 7 1) 31.851 0.3425 4.3046 63.904 1.4555 4.0 ( 7 1 1) 31.952 0.3435 4.3168 63.904 1.4555 4.0 ( 0 6 4) 31.952 0.3435 4.3168 64.004 1.4535 2.2 ( 6 0 4) 32.002 0.3440 4.3228 64.559 1.4423 12.0 ( 6 4 0) 32.280 0.3467 4.3563 64.559 1.4423 12.0 ( 3 3 6) 32.280 0.3467 4.3563 64.699 1.4396 6.5 ( 6 1 4) 32.349 0.3473 4.3647 64.934 1.4349 1.1 ( 2 5 5) 32.467 0.3485 4.3788 65.153 1.4306 7.2 ( 2 7 0) 32.577 0.3495 4.3920 65.153 1.4306 7.2 ( 4 6 1) 32.577 0.3495 4.3920 65.236 1.4290 7.2 ( 6 4 1) 32.618 0.3499 4.3969 65.326 1.4272 4.7 ( 7 2 0) 32.663 0.3503 4.4023 65.673 1.4205 4.1 ( 1 7 2) 32.836 0.3520 4.4231 65.673 1.4205 4.1 ( 6 3 3) 32.836 0.3520 4.4231 65.772 1.4187 5.9 ( 5 5 2) 32.886 0.3524 4.4290 65.772 1.4187 5.9 ( 2 7 1) 32.886 0.3524 4.4290 65.968 1.4149 11.1 ( 7 2 1) 32.984 0.3534 4.4407 65.968 1.4149 11.1 ( 4 2 6) 32.984 0.3534 4.4407 66.141 1.4116 10.2 ( 2 2 7) 33.071 0.3542 4.4510 66.628 1.4025 5.0 ( 2 6 4) 33.314 0.3565 4.4801 66.760 1.4000 6.2 ( 6 2 4) 33.380 0.3571 4.4879 67.101 1.3937 7.8 ( 4 6 2) 33.551 0.3587 4.5082 67.183 1.3922 8.1 ( 6 4 2) 33.592 0.3591 4.5130 67.395 1.3884 4.4 ( 5 4 4) 33.697 0.3601 4.5256 67.395 1.3884 4.4 ( 4 5 4) 33.697 0.3601 4.5256 67.524 1.3860 3.0 ( 3 1 7) 33.762 0.3607 4.5332 67.524 1.3860 3.0 ( 1 3 7) 33.762 0.3607 4.5332 67.730 1.3823 1.9 ( 2 7 2) 33.865 0.3617 4.5454 67.914 1.3790 0.7 ( 7 2 2) 33.957 0.3626 4.5563 68.365 1.3710 0.9 ( 5 3 5) 34.183 0.3647 4.5829 68.365 1.3710 0.9 ( 3 5 5) 34.183 0.3647 4.5829 68.566 1.3675 0.9 ( 3 7 0) 34.283 0.3656 4.5947 68.989 1.3601 14.9 ( 5 5 3) 34.494 0.3676 4.6195 69.202 1.3565 8.8 ( 3 7 1) 34.601 0.3686 4.6320 69.671 1.3485 5.2 ( 0 6 5) 34.835 0.3708 4.6595 69.816 1.3460 6.4 ( 6 0 5) 34.908 0.3715 4.6679 69.961 1.3436 8.6 ( 1 5 6) 34.981 0.3721 4.6764 70.058 1.3420 9.1 ( 3 6 4) 35.029 0.3726 4.6820 70.058 1.3420 9.1 ( 5 1 6) 35.029 0.3726 4.6820 |
2楼2013-01-10 09:24:31