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32.6,44.0,44.3,53.5,62.2,62.9,63.9,100.8,102.9,102.9,106.9,107.0,125.9,127.6,132.0,138.1,145.8,146.2 溶剂：CDCl3 [ 来自科研家族 Natural Products家族 ] |
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audreygc
铁杆木虫 (正式写手)
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【答案】应助回帖
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感谢参与，应助指数 +1
jiangchunyong: 金币+1, 谢谢 2012-12-27 17:32:03
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感谢参与，应助指数 +1
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???????????鵽32????????(???????????ο?) -------------------------------------------------------------------------------- 1 . Crinine C16H17NO3 ?????:88.8% Phytochemistry 1995 40 961-965 Further alkaloids from Brunsvigia josephinae Francesc Viladomat, Carles Codina, Jaume Bastida, Shaheed Mathee, William E. Campbell Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . crinine ?????:83.3% European Journal of Organic Chemistry 2011 740-750 Construction of the 5,10b-Phenanthridine Skeleton Using [3+2]-Cycloaddition of a Non-Stabilized Azomethine Ylide: Total Synthesis of (??)-Maritidine and (??)-Crinine Alkaloids Ganesh Pandey, Nishant R. Gupta and Smita R. Gadre Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . buphanisine C17H19NO3 ?????:72.2% Phytochemistry 1998 48 371-376 Alkaloids from Crinum amabile Lam Huong Pham, Werner Döpke, J??rgen Wagner, Clemens M??gge Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . (-)-buphanisine ?????:72.2% Journal of Natural Products 1993 Vol 56 1331 Cytotoxic and Antimalarial Alkaloids from the Bulbs of Crinum amabile Kittisak Likhitwitayawuid, Cindy K. Angerhofer, Heebyung Chai, John M. Pezzuto, Geoffrey A. Cordell, Nijsiri Ruangrungsi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . Buphanisine C17H19NO3 ?????:72.2% Phytochemistry 1995 40 961-965 Further alkaloids from Brunsvigia josephinae Francesc Viladomat, Carles Codina, Jaume Bastida, Shaheed Mathee, William E. Campbell Structure 13C NMR ??????? -------------------------------------------------------------------------------- 6 . epi-crinine ?????:72.2% European Journal of Organic Chemistry 2011 740-750 Construction of the 5,10b-Phenanthridine Skeleton Using [3+2]-Cycloaddition of a Non-Stabilized Azomethine Ylide: Total Synthesis of (??)-Maritidine and (??)-Crinine Alkaloids Ganesh Pandey, Nishant R. Gupta and Smita R. Gadre Structure 13C NMR ??????? -------------------------------------------------------------------------------- 7 . O-acctylcrinine C18H19NO4 ?????:66.6% Phytochemistry 1986 25 2399-2401 Oxocrinine and other alkaloids from Crinum americanum A.A. Ali, H.M. El Saved, O.M. Abdalliah, W. Steglich Structure 13C NMR ??????? -------------------------------------------------------------------------------- 8 . Epibuphanisine C17H19NO3 ?????:61.1% Phytochemistry 1995 40 307-311 Alkaloids from Boophane flava Francesc Viladomat, Jaume Bastida, Carles Codina, William E. Campbell, Shaheed Mathee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 9 . 1-[10-(1,3-dioxolan-2-ylmethyl)-4,5-methylenedioxy-9-azatricyclo-[7.2.1.0(2,7)]dodeca-2,4,6-trien-11??-yl]ethanone C18H21NO5 ?????:61.1% European Journal of Organic Chemistry 2011 4571-4587 One-Step Stereospecific Strategy for the Construction of the Core Structure of the 5,11-Methanomorphanthridine Alkaloids in Racemic as well as in Optically Pure Form: Synthesis of (??)-Pancracine and (??)-Brunsvigine Ganesh Pandey, Ravindra Kumar, Prabal Banerjee and Vedavati G. Puranik Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . flexinine C16H17NO4 ?????:55.5% Phytochemistry 1999 51 1185-1191 Alkaloids from Ammocharis tinneana A. Machocho, S.C. Chhabra, F. Viladomat, C. Codina, J. Bastida Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . augustine C17H19NO4 ?????:55.5% Phytochemistry 1998 48 371-376 Alkaloids from Crinum amabile Lam Huong Pham, Werner Döpke, J??rgen Wagner, Clemens M??gge Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . (-)-augustine ?????:55.5% Journal of Natural Products 1993 Vol 56 1331 Cytotoxic and Antimalarial Alkaloids from the Bulbs of Crinum amabile Kittisak Likhitwitayawuid, Cindy K. Angerhofer, Heebyung Chai, John M. Pezzuto, Geoffrey A. Cordell, Nijsiri Ruangrungsi Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . augustine ?????:55.5% Phytochemistry 1981 20 1735-1738 Relative configuration of the alkaloid augustine A. W. Frahm, A. A. Ali, H. Kating Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . oxocrinine C16H15NO3 ?????:55.5% Phytochemistry 1986 25 2399-2401 Oxocrinine and other alkaloids from Crinum americanum A.A. Ali, H.M. El Saved, O.M. Abdalliah, W. Steglich Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . flexinine C16H17NO4 ?????:55.5% Phytochemistry 1986 25 2399-2401 Oxocrinine and other alkaloids from Crinum americanum A.A. Ali, H.M. El Saved, O.M. Abdalliah, W. Steglich Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . oxo-crinine C16H15NO3 ?????:55.5% European Journal of Organic Chemistry 2011 740-750 Construction of the 5,10b-Phenanthridine Skeleton Using [3+2]-Cycloaddition of a Non-Stabilized Azomethine Ylide: Total Synthesis of (??)-Maritidine and (??)-Crinine Alkaloids Ganesh Pandey, Nishant R. Gupta and Smita R. Gadre Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . {(6R,7S,8S,9R)-7-[(1,3-dioxolan-2-yl)methyl]-5,7,8,9-tetrahydro-6,9-methano[1,3]dioxolo[4',5':4,5]benzo[1,2-c]azepin-8-yl}methanol C17H21NO5 ?????:55.5% European Journal of Organic Chemistry 2011 4571-4587 One-Step Stereospecific Strategy for the Construction of the Core Structure of the 5,11-Methanomorphanthridine Alkaloids in Racemic as well as in Optically Pure Form: Synthesis of (??)-Pancracine and (??)-Brunsvigine Ganesh Pandey, Ravindra Kumar, Prabal Banerjee and Vedavati G. Puranik Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . macowine C16H19NO3 ?????:55% Phytochemistry 2000 54 945-950 Alkaloids from Crinum macowanii J.J. Nair, A.K. Machochoa, W.E. Campbell, R. Brun, F. Viladomat, C. Codina, J. Bastida Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . ethyl (6R,7S,8S,9R)-7-[(1,3-dioxolan-2-yl)methyl]-5,7,8,9-tetrahydro-6,9-methano[1,3]dioxolo[4',5':4,5]benzo[1,2-c]azepine-8-carboxylate C19H23NO6 ?????:52.6% European Journal of Organic Chemistry 2011 4571-4587 One-Step Stereospecific Strategy for the Construction of the Core Structure of the 5,11-Methanomorphanthridine Alkaloids in Racemic as well as in Optically Pure Form: Synthesis of (??)-Pancracine and (??)-Brunsvigine Ganesh Pandey, Ravindra Kumar, Prabal Banerjee and Vedavati G. Puranik Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . 11-hydroxyvittatine ?????:50% Chemistry & Biodiversity 2008 Vol. 5 332-339 Phytochemical and Biological Investigation of Hymenocallis littoralis Salisb Amina H. Abou-Donia, Soad M. Toaima, Hala M. Hammoda, Eman Shawky, Eri Kinoshita, Hiromitsu Takayama Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . jussiaeiine C C16H24N2O3 ?????:50% Journal of Natural Products 2000 63 201-204 New Quinolizidine Alkaloids from Ulex jussiaei Patr??cia M??ximo and Ana Lourenço Structure 13C NMR ??????? -------------------------------------------------------------------------------- 22 . apohaemanthamine ?????:50% Phytochemistry 2000 53 587-591 Bioactive alkaloids from Brunsvigia radulosa William E. Campbell, Jerald J. Nair, David W. Gammon, Carles Codina, Jaume Bastida, Francesc Viladomat, Peter J. Smith, Carl F. Albrecht Structure 13C NMR ??????? -------------------------------------------------------------------------------- 23 . gardenin C ?????:50% Natural Product Sciences 2003 9 56-59 Polysubstituted Flavonoids from the Leaves of Murraya paniculata (Rutaceae) Sukari, Mohd Aspollah; Azziz, Saripah Salbiah Syed Abd.; Rahmani, Mawardi; Ali, Abdul Manaf; Aimi, Norio; Kitajima, Mariko Structure 13C NMR ??????? -------------------------------------------------------------------------------- 24 . Hamoyne C16H17NO4 ?????:50% Phytochemistry 1994 35 809-812 Alkaloids from Brunsvigia josephinæ Francesc Viladomat, Jaume Bastida, Carles Codina, William E. Campbell, Shaheed Mathee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 25 . 4'-demethyl-4-deoxypodophyllotoxin (DDPT) ?????:50% Chemical Research in Chinese Universities 2010 26 753-756 Synthesis and Biological Activity of Novel Spin Labeled Derivatives of 4'-Demethyl-4-deoxypodophyllotoxin XU Jing, SUN Xiao-hua, ZHANG Jia-qiang, ZHANG Zhi-wei and TIAN Xuan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 26 . (7S,8R)-3,3',5-Trimethoxy-4',7-epoxy-8,5'-neolignan-4,9,9'-triol C21H26O7 ?????:50% Helvetica Chimica Acta 2010 93 2467-2477 Neolignans and Caffeoyl Derivatives from Selaginella moellendorffii Yue-Hu Wang, Qian-Yun Sun, Fu-Mei Yang, Chun-Lin Long, Fu-Wei Zhao, Gui-Hua Tang, Hong-Mei Niu, Huan Wang, Qiao-Qin Huang, Jin-Jin Xu and Li-Juan Ma Structure 13C NMR ??????? -------------------------------------------------------------------------------- 27 . calycinine C18H17NO4 ?????:50% Chinese Journal of Natural Medicines 2005 3 151-154 Studies on the Active Constituents of Fissistigma oldhamii ZHENG Zong-Ping; LIANG Jing-Yu; HU Li-Hong Structure 13C NMR ??????? -------------------------------------------------------------------------------- 28 . xylopine C18H17NO3 ?????:50% Chinese Journal of Natural Medicines 2005 3 151-154 Studies on the Active Constituents of Fissistigma oldhamii ZHENG Zong-Ping; LIANG Jing-Yu; HU Li-Hong Structure 13C NMR ??????? -------------------------------------------------------------------------------- 29 . ethyl 2-((1R,3aR,3a1S,12bS)-1-acetoxy-3a,3a1,4,5,7,12b-hexahydro-1H-[1,3]dioxolo[4,5-j]pyrrolo[3,2,1-de]phenanthridin-3a-yl)acetate C22H25NO6 ?????:50% Bioorganic & Medicinal Chemistry 2011 19 7252-7261 In search of a cytostatic agent derived from the alkaloid lycorine: Synthesis and growth inhibitory properties of lycorine derivatives Nikolai M. Evdokimov, Delphine Lamoral-Theys, V??ronique Mathieu, Anna Andolfi, Liliya V. Frolova, Stephen C. Pelly, Willem A.L. van Otterlo, Igor V. Magedov, Robert Kiss, Antonio Evidente, Alexander Kornienko Structure 13C NMR ??????? -------------------------------------------------------------------------------- 30 . roemerine ?????:50% Journal of the Chinese Chemical Society 1998 45 103-110 Chemical Constituents of Neolitsea parvigemma and Neolitsea Konishii ????B(Keh-Shaw Chen);?????s(Fang-Rong Chang);?Z???(Yi-Chen Chia);?????p(Tian-Shung Wu);??????(Yang-Chang Wu) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 31 . 3,8,11-Tribromonantenine C20H18Br3NO4 ?????:50% Bioorganic & Medicinal Chemistry 2011 19 5861-5868 New aporphinoid 5-HT2A and ??1A antagonists via structural manipulations of nantenine Sandeep Chaudhary, Shashikanth Ponnala, Onica LeGendre, Junior A. Gonzales, Hern??n A. Navarro, Wayne W. Harding Structure 13C NMR ??????? -------------------------------------------------------------------------------- 32 . compound 6c C18H23NO3 ?????:50% Journal of Medicinal Chemistry 1987 30 1355-1359 Berbanes: a new class of selective .alpha.2-adrenoceptor antagonists E. Sylvester Vizi, Istvan Toth, George T. Somogyi, Lajos Szabo, Laszlo G. Harsing Jr., Csaba Szantay Structure 13C NMR ??????? |
2楼2012-12-27 15:53:52
