| 查看: 929 | 回复: 1 | ||
[求助]
急需！！！！！！
|
|
求助 Fe3O4的标准卡(JCPDS 79-0419) γ-Fe2O3的标准卡(JCPDS 39-1346) a-Fe2O3XRD 的标准卡片PDF33-0664 |
回复此楼» 猜你喜欢
江西科技师范大学物理化学课题组接收调剂生，12点开启，速来
已经有0人回复
-
【2026 考研调剂】哈尔滨工程大学 招收学硕调剂生（英语一、数学一）
已经有0人回复
-
无机化学论文润色/翻译怎么收费?
已经有99人回复
-
四川轻化工大学化学与环境工程学院 付昱教授课题组招收调剂硕士研究生
已经有11人回复
-
大连化物所招收有机背景的博士候选人
已经有0人回复
-
在MOF中，有没有羧基参加配位的情况
已经有2人回复
-
招2026年入学上海交通大学博士生，急！！！
已经有1人回复
-
理论计算合作
已经有0人回复
liuxiaocunde
铁杆木虫 (著名写手)
古德里安将军
- 应助: 83 (初中生)
- 贵宾: 2.195
- 金币: 9333.7
- 散金: 3014
- 红花: 20
- 帖子: 1927
- 在线: 716小时
- 虫号: 536180
- 注册: 2008-03-30
- 性别: GG
- 专业: 固体无机化学
|
PDF#79-0419: QM=Calculated(C); d=Calculated; I=Calculated Magnetite Fe3 O4 Radiation=CuKa1 Lambda=1.54060 Filter= Calibration= 2T=18.285-89.598 I/Ic(RIR)=5.14 Ref: Calculated from ICSD using POWD-12++ (1997) Cubic - (Unknown), Fd-3m (227) Z=8 mp= CELL: 8.3969 x 8.3969 x 8.3969 <90.0 x 90.0 x 90.0> P.S=cF56 (Al2 Mg O4) Density(c)=5.194 Density(m)=6.75A Mwt=231.54 Vol=592.05 F(17)=999.9(.0000,18/0) Ref: Fleet, M.E. J. Solid State Chem., v62 p75 (1986) Strong Lines: 2.53/X 1.48/4 2.97/3 1.62/3 2.10/2 1.09/1 4.85/1 1.71/1 2.42/1 1.28/1 FIZ=065341: ATF At least one TF implausible. Specimen from magnetite chlorite schist, Dana Collection. Annealed at 1373 K for 7 days. See PDF 00-019-0629 and 01-082-1533. Calc. density unusual but tolerable. The structure of magnetite: Symmetry of cubic spinels e d a (FD3-MS) AB2X4 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 18.285 4.8479 9.7 ( 1 1 1) 9.142 0.1031 1.2961 3 30.076 2.9688 29.5 ( 2 2 0) 15.038 0.1684 2.1164 8 35.426 2.5318 100.0 ( 3 1 1) 17.713 0.1975 2.4817 11 37.057 2.4240 7.8 ( 2 2 2) 18.528 0.2063 2.5921 12 43.053 2.0992 20.1 ( 4 0 0) 21.527 0.2382 2.9931 16 47.139 1.9264 0.6 ( 3 3 1) 23.569 0.2596 3.2617 19 53.411 1.7140 8.5 ( 4 2 2) 26.705 0.2917 3.6658 24 56.936 1.6160 27.8 ( 5 1 1) 28.468 0.3094 3.8882 27 62.520 1.4844 36.5 ( 4 4 0) 31.260 0.3368 4.2329 32 65.736 1.4193 0.8 ( 5 3 1) 32.868 0.3523 4.4268 35 70.926 1.3277 2.8 ( 6 2 0) 35.463 0.3766 4.7325 40 73.960 1.2805 6.8 ( 5 3 3) 36.980 0.3905 4.9067 43 74.961 1.2659 2.9 ( 6 2 2) 37.481 0.3950 4.9635 44 78.922 1.2120 2.1 ( 4 4 4) 39.461 0.4125 5.1842 48 81.856 1.1758 0.4 ( 7 1 1) 40.928 0.4252 5.3438 51 86.703 1.1221 2.8 ( 6 4 2) 43.352 0.4456 5.5996 56 89.598 1.0932 10.0 ( 7 3 1) 44.799 0.4574 5.7476 59 PDF#33-0664: QM=Star(S); d=Diffractometer; I=Diffractometer Hematite, syn Fe2 O3 Dark reddish brown Radiation=CuKa1 Lambda=1.540598 Filter= Calibration=Internal(Ag) 2T=24.138-147.961 I/Ic(RIR)=2.4 Ref: Natl. Bur. Stand. (U.S.) Monogr. 25, v18 p37 (1981) Rhombohedral - (Unknown), R-3c (167) Z=6 mp=1350-1360$DE CELL: 5.0356 x 5.0356 x 13.7489 <90.0 x 90.0 x 120.0> P.S=hR10 (Al2 O3) Density(c)=5.270 Density(m)=5.260 Mwt=159.69 Vol=301.93 F(30)=69.1(.0111,39/0) Ref: Ibid. Strong Lines: 2.70/X 2.52/7 1.69/5 1.84/4 3.68/3 1.49/3 1.45/3 2.21/2 1.60/1 1.31/1 NOTE: Pattern reviewed by Syvinski, W., McCarthy, G., North Dakota State Univ., Fargo, North Dakota, USA, ICDD Grant-in-Aid (1990). Agress well with experimental and calculated patterns. Sample from Pfizer, Inc., New York, USA, heated at 800 C for 3 days. Additional weak reflection [indicated by brackets] was observed. Also called: crocus mantis. To replace 00-013-0534 and validated by calculated pattern 00-024-0072. Also called: venetian red. Opaque mineral optical data on specimen from Elba, R1R0=30.2, RR2Re=26.1, Disp.=16, VHN=1038 (mean at 100, 200, 300), Color values=1 .299, .309, 29.8, 2 .299, .309, 25.7. Also called: ferrite. Also called: indian red. Also called: crocus. See ICSD 64599 (PDF 01-079-0007). 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 24.138 3.6840 30.0 ( 0 1 2) 12.069 0.1357 1.7055 33.152 2.7000 100.0 ( 1 0 4) 16.576 0.1852 2.3271 35.611 2.5190 70.0 ( 1 1 0) 17.806 0.1985 2.4943 39.276 2.2920 3.0 ( 0 0 6) 19.638 0.2182 2.7414 40.854 2.2070 20.0 ( 1 1 3) 20.427 0.2266 2.8469 43.518 2.0779 3.0 ( 2 0 2) 21.759 0.2406 3.0238 49.479 1.8406 40.0 ( 0 2 4) 24.740 0.2717 3.4137 54.089 1.6941 45.0 ( 1 1 6) 27.045 0.2951 3.7089 56.150 1.6367 1.0 ( 2 1 1) 28.075 0.3055 3.8389 57.428 1.6033 5.0 ( 1 2 2) 28.714 0.3119 3.9189 57.589 1.5992 10.0 ( 0 1 8) 28.794 0.3127 3.9290 62.449 1.4859 30.0 ( 2 1 4) 31.225 0.3365 4.2285 63.989 1.4538 30.0 ( 3 0 0) 31.995 0.3439 4.3219 66.026 1.4138 <1 ( 1 2 5) 33.013 0.3537 4.4442 69.599 1.3497 3.0 ( 2 0 8) 34.799 0.3705 4.6552 71.935 1.3115 10.0 ( 1 0 10) 35.968 0.3812 4.7908 72.260 1.3064 6.0 ( 1 1 9) 36.130 0.3827 4.8095 75.428 1.2592 8.0 ( 2 2 0) 37.714 0.3971 4.9898 77.727 1.2276 4.0 ( 3 0 6) 38.864 0.4073 5.1183 78.758 1.2141 2.0 ( 2 2 3) 39.379 0.4118 5.1752 80.709 1.1896 5.0 ( 1 2 8) 40.354 0.4203 5.2818 82.937 1.1632 5.0 ( 0 2 10) 41.468 0.4298 5.4016 84.913 1.1411 7.0 ( 1 3 4) 42.457 0.4382 5.5063 88.539 1.1035 7.0 ( 2 2 6) 44.269 0.4531 5.6939 91.342 1.0768 2.0 ( 0 4 2) 45.671 0.4643 5.8351 93.712 1.0557 7.0 ( 2 1 10) 46.856 0.4736 5.9517 95.236 1.0428 <1 ( 1 1 12) 47.618 0.4795 6.0253 95.659 1.0393 3.0 ( 4 0 4) 47.830 0.4811 6.0456 102.282 0.9892 4.0 ( 3 1 8) 51.141 0.5055 6.3518 104.910 0.9715 <1 ( 2 2 9) 52.455 0.5147 6.4675 106.619 0.9606 5.0 ( 3 2 4) 53.309 0.5205 6.5409 107.021 0.9581 4.0 ( 0 1 14) 53.511 0.5219 6.5580 108.086 0.9516 5.0 ( 4 1 0) 54.043 0.5254 6.6028 111.514 0.9318 2.0 ( 4 1 3) 55.757 0.5366 6.7431 113.590 0.9206 2.0 ( 0 4 8) 56.795 0.5431 6.8251 116.040 0.9081 5.0 ( 1 3 10) 58.020 0.5506 6.9190 117.753 0.8998 1.0 ( 3 0 12) 58.877 0.5557 6.9829 118.692 0.8954 3.0 ( 2 0 14) 59.346 0.5584 7.0172 122.425 0.8789 6.0 ( 4 1 6) 61.213 0.5689 7.1489 125.923 0.8648 1.0 ( 2 3 8) 62.962 0.5782 7.2655 128.752 0.8543 3.0 ( 4 0 10) 64.376 0.5853 7.3548 131.871 0.8436 5.0 ( 1 2 14) 65.935 0.5927 7.4481 133.234 0.8392 3.0 ( 3 3 0) 66.617 0.5958 7.4871 144.448 0.8089 4.0 ( 3 2 10) 72.224 0.6181 7.7676 147.961 0.8014 4.0 ( 2 4 4) 73.981 0.6239 7.8403 PDF#39-1346: QM=Star(S); d=Diffractometer; I=Diffractometer Maghemite-C, syn Fe2 O3 Light brown Radiation=CuKa Lambda=1.54178 Filter=Graph Calibration=Internal(Si) 2T=14.958-95.103 I/Ic(RIR)=1.4 Ref: Schulz, D., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA. ICDD Grant-in-Aid (1987) Cubic - Single Crystal, P4132 (213) Z=10.667 mp= CELL: 8.3515 x 8.3515 x 8.3515 <90.0 x 90.0 x 90.0> P.S=cP53.33 (?) Density(c)=4.860 Density(m)=4.900 Mwt=159.69 Vol=582.50 F(30)=94.9(.0090,35/0) Ref: Lindsley, D. Min. Soc. of America, Short Course Notes (Wash., D.C.), v3 pL-18 (1976) Strong Lines: 2.52/X 2.95/4 1.48/3 1.61/2 2.09/2 1.70/1 1.09/1 5.92/1 3.74/1 3.41/1 NOTE: Sample from Control Data as used in hard disks. Optical data on specimen from Iron Mountain, Shasta County, California, USA. Space group dependent upon preparation (Bernal et al.). To replace 00-004-0755 and 00-024-0081. Pattern reviewed by Syvinski, W., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA, ICDD Grant-in-Aid (1990). Agrees well with experimental pattern. Additional weak reflections [indicated by brackets] were observed. 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 14.958 5.9180 5.0 ( 1 1 0) 7.479 0.0845 1.0617 2 18.384 4.8220 4.0 ( 1 1 1) 9.192 0.1037 1.3030 3 23.771 3.7400 5.0 ( 2 1 0) 11.886 0.1337 1.6800 5 26.102 3.4110 5.0 ( 2 1 1) 13.051 0.1466 1.8420 6 30.241 2.9530 35.0 ( 2 2 0) 15.120 0.1693 2.1277 8 32.124 2.7840 2.0 ( 2 2 1) 16.062 0.1796 2.2569 9 33.882 2.6435 2.0 ( 3 1 0) 16.941 0.1891 2.3768 10 35.630 2.5177 100.0 ( 3 1 1) 17.815 0.1986 2.4956 11 37.249 2.4119 3.0 ( 2 2 2) 18.625 0.2073 2.6051 12 38.847 2.3163 1.0 ( 3 2 0) 19.423 0.2159 2.7126 13 40.377 2.2320 1.0 ( 3 2 1) 20.188 0.2240 2.8150 14 43.284 2.0886 16.0 ( 4 0 0) 21.642 0.2394 3.0083 16 44.703 2.0255 1.0 ( 4 1 0) 22.352 0.2469 3.1020 17 46.071 1.9685 <1 ( 3 3 0) 23.036 0.2540 3.1919 18 50.007 1.8224 2.0 ( 4 2 1) 25.003 0.2744 3.4478 21 53.733 1.7045 10.0 ( 4 2 2) 26.866 0.2933 3.6862 24 54.924 1.6703 1.0 ( 4 3 0) 27.462 0.2993 3.7617 25 56.106 1.6379 1.0 ( 5 1 0) 28.053 0.3053 3.8361 26 57.271 1.6073 24.0 ( 5 1 1) 28.636 0.3111 3.9092 27 59.568 1.5507 1.0 ( 5 2 0) 29.784 0.3224 4.0518 29 60.685 1.5248 2.0 ( 5 2 1) 30.342 0.3279 4.1207 30 62.925 1.4758 34.0 ( 4 4 0) 31.463 0.3388 4.2575 32 63.994 1.4537 1.0 ( 4 4 1) 31.997 0.3439 4.3222 33 65.072 1.4322 1.0 ( 5 3 0) 32.536 0.3491 4.3871 34 67.201 1.3919 <1 ( 4 4 2) 33.601 0.3592 4.5141 36 68.253 1.3730 1.0 ( 6 1 0) 34.126 0.3642 4.5762 37 69.305 1.3547 1.0 ( 6 1 1) 34.653 0.3691 4.6381 38 71.376 1.3204 3.0 ( 6 2 0) 35.688 0.3787 4.7585 40 72.401 1.3042 1.0 ( 5 4 0) 36.201 0.3834 4.8177 41 74.471 1.2730 5.0 ( 5 3 3) 37.235 0.3928 4.9357 43 75.442 1.2590 2.0 ( 6 2 2) 37.721 0.3971 4.9906 44 76.442 1.2450 <1 ( 6 3 0) 38.221 0.4016 5.0467 45 77.442 1.2314 <1 ( 6 3 1) 38.721 0.4060 5.1025 46 79.446 1.2053 1.0 ( 4 4 4) 39.723 0.4148 5.2130 48 80.423 1.1931 <1 ( 6 3 2) 40.212 0.4191 5.2663 49 81.419 1.1810 1.0 ( 7 1 0) 40.710 0.4234 5.3202 50 85.338 1.1365 <1 ( 7 2 1) 42.669 0.4399 5.5285 54 87.304 1.1159 2.0 ( 6 4 2) 43.652 0.4481 5.6306 56 89.244 1.0966 <1 ( 7 3 0) 44.622 0.4560 5.7297 58 90.226 1.0872 7.0 ( 7 3 1) 45.113 0.4599 5.7792 59 95.103 1.0439 3.0 ( 8 0 0) 47.552 0.4790 6.0190 64 |
2楼2012-11-15 13:09:48
5