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qianfang85

木虫 (小有名气)

[求助] 求助 苯甲酸钠结晶

请教各路高手,我现在想要做苯甲酸钠,用结晶法。可是我用乙醇或丙酮为什么都析不出来啊??
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sbhuihai

金虫 (小有名气)

用乙醇还是可以的  可能是你操作上的问题或者粗品纯度比较低
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2楼2012-10-29 15:53:33
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qianfang85

木虫 (小有名气)

引用回帖:
2楼: Originally posted by sbhuihai at 2012-10-29 15:53:33
用乙醇还是可以的  可能是你操作上的问题或者粗品纯度比较低

我用乙醇析晶,析出来的是软膏状的,像凡士林那样,怎么回事?难道是纯度太低??
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3楼2012-10-31 16:23:35
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sbhuihai

金虫 (小有名气)

引用回帖:
3楼: Originally posted by qianfang85 at 2012-10-31 16:23:35
我用乙醇析晶,析出来的是软膏状的,像凡士林那样,怎么回事?难道是纯度太低??...

多重结晶一次看看  另外控制结晶时温度变化速度和搅拌速度
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4楼2012-11-01 15:28:49
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