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Data collections were performed at 20 °C on a Rigaku RAXIS RAPID IP diffractometer, using graphite-monochromated Mo Ka radiation (l = 0.71073 Å . The determination of crystal class and unit cell parameters was carried out by the Rapid-AUTO (Rigaku 2000) program package. The raw frame data were processed using Crystal Structure (Rigaku/MSC 2000) to yield the reflection data file. The structure was solved by use of SHELXTL program. Refinement was performed on F2 anisotropically for all the non-hydrogen atoms by the full-matrix least-squares method. The hydrogen atoms were placed at the calculated positions and were included in the structure calculation without further refinement of the parameters. |
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