| 查看: 882 | 回复: 14 | |||
[求助]
重金酬谢，望各位高手帮忙解一晶体！
|
| 重金酬谢，望各位高手帮忙解一晶体！只要R1值在0.07以下，S值越接近1越好，没有A类错误就行了。先谢谢了1[ Last edited by Giji521 on 2012-9-6 at 21:14 ] |
回复此楼» 本帖附件资源列表
-
欢迎监督和反馈：小木虫仅提供交流平台，不对该内容负责。
本内容由用户自主发布，如果其内容涉及到知识产权问题，其责任在于用户本人，如对版权有异议，请联系邮箱：xiaomuchong@tal.com - 附件 1 : GJ0238.rar
2012-09-06 21:14:40, 10.76 M
» 猜你喜欢
26年博士招生
已经有16人回复
-
江西理工大学功能晶态材料方向刘遂军课题组招收2026年秋季入学博士研究生
已经有11人回复
-
无机化学论文润色/翻译怎么收费?
已经有275人回复
-
宁夏大学团簇新材料团队招收材料/化学/化工专业博士生
已经有0人回复
-
MIL-101有单晶样品吗
已经有1人回复
-
已删除
已经有3人回复
-
收调剂研究生
已经有2人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有3人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有1人回复
-
广州大学环环境大分子材料研究所2026年研究生招生简章
已经有0人回复
» 本主题相关价值贴推荐，对您同样有帮助:
- 急求高人帮忙解一晶体！1000金币
已经有17人回复
- acta E编辑的修改意见，有些问题不懂，麻烦各位高手解释下~重金酬谢~
已经有5人回复
- 现洒100个金币求高手帮忙解一晶体
已经有4人回复
- 计算机读博选择无线传感器方向怎么样？重金酬谢
已经有8人回复
- 本人菜鸟 有一晶体 想请高手帮忙解一下
已经有8人回复
- oringin绘图求助 在线等侯 重金酬谢
已经有3人回复
- 请高人帮忙解一晶体！
已经有6人回复
- 各位高手，帮忙修改下参考文献啊，重金酬谢！感激 啊
已经有4人回复
- 求一高手帮忙解一晶体数据，不胜感激
已经有7人回复
- 【求助】向高手求助帮忙一个C类错误（重金酬谢）
已经有5人回复
- 【讨论】化工类的考什么证书好？麻烦大家告知下 重金酬谢
已经有15人回复
- 【求助】重金求助晶体解析问题
已经有9人回复
- 【求助】请帮解决两个A类问题，有酬谢
已经有3人回复
2楼2012-09-07 01:05:33
panperfect
金虫 (小有名气)
- 应助: 31 (小学生)
- 金币: 697.2
- 红花: 2
- 帖子: 286
- 在线: 96.3小时
- 虫号: 560927
- 注册: 2008-05-20
- 专业: 无机超分子化学
3楼2012-09-07 01:42:20
4楼2012-09-07 09:09:00
huangpeking 
金虫 (小有名气)
- 应助: 29 (小学生)
- 金币: 170.6
- 散金: 600
- 帖子: 112
- 在线: 325.4小时
- 虫号: 1245162
- 注册: 2011-03-25
- 专业: 无机材料化学
5楼2012-09-07 10:45:11
6楼2012-09-07 11:59:32
yytsnake
至尊木虫 (职业作家)
- 应助: 357 (硕士)
- 贵宾: 0.01
- 金币: 18204.3
- 散金: 5
- 红花: 36
- 帖子: 3189
- 在线: 444.6小时
- 虫号: 92066
- 注册: 2005-09-08
- 性别: GG
7楼2012-09-07 14:01:17
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ...
感谢参与，应助指数 +1
linhua0402313: 金币+2, 高手啊，单看数据很完美啊，欢迎常来晶体板块 2012-09-07 15:05:30
Giji521: 金币+200, ★★★★★最佳答案 2012-09-07 16:19:45
感谢参与，应助指数 +1
linhua0402313: 金币+2, 高手啊，单看数据很完美啊，欢迎常来晶体板块 2012-09-07 15:05:30
Giji521: 金币+200, ★★★★★最佳答案 2012-09-07 16:19:45
|
能给1000金币吗？我解的结果可以达到你的要求。 Correction method= Not given Data completeness= 0.996 Theta(max)= 25.000 R(reflections)= 0.0638( 3367) wR2(reflections)= 0.2028( 3769) S = 1.056 Npar= 269 -------------------------------------------------------------------------------- The following ALERTS were generated. Each ALERT has the format test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. --------------------------------------------------------------------------------Alert level A SYMM001_ALERT_1_A _symmetry_cell_setting is missing The cell setting should be one of the following * triclinic * monoclinic * orthorhombic * tetragonal * rhombohedral * trigonal * hexagonal * cubic The following tests will not be performed. SYMMS_01,SYMMS_02 SYMM003_ALERT_1_A _symmetry_space_group_name_H-M is missing Space-group symbol, including unique axis. The following tests will not be performed. CELLZ_01,CHEMW_03,REFLT_03,SYMMG_01,SYMMG_02 CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 EXPT009_ALERT_1_A No crystal dimensions have been given. The following tests will not be performed. CRYSS_01,CRYSS_02 EXPT108_ALERT_1_A The magnitudes of the crystal dimensions do not match the min, mid and max definitions EXPT010_ALERT_1_A _exptl_crystal_colour (_pd_char_colour for powder) is missing Crystal colour. The following tests will not be performed. CRYSC_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. DIFF005_ALERT_1_A _diffrn_measurement_method is missing Mode of intensity measurement and scan. DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. ABSTY01_ALERT_1_A The absorption correction should be one of the following * none * analytical * integration * numerical * gaussian * empirical * psi-scan * multi-scan * refdelf * sphere * cylinder PLAT043_ALERT_1_A Check Reported Molecular Weight ................ 854.83 PLAT044_ALERT_1_A Calculated and Reported Dx Differ .............. ? PLAT051_ALERT_1_A Mu(calc) and Mu(CIF) Ratio Differs from 1.0 by . 74.27 Perc. PLAT053_ALERT_1_A Minimum Crystal Dimension Missing (or Error) ... ? PLAT054_ALERT_1_A Medium Crystal Dimension Missing (or Error) ... ? PLAT055_ALERT_1_A Maximum Crystal Dimension Missing (or Error) ... ? PLAT122_ALERT_1_A No _symmetry_space_group_name_H-M Given ........ ? PLAT761_ALERT_1_A CIF Contains no X-H Bonds ...................... ? PLAT762_ALERT_1_A CIF Contains no X-Y-H or H-Y-H Angles .......... ? --------------------------------------------------------------------------------Alert level B PLAT052_ALERT_1_B Info on Absorption Correction Method Missing ... ? PLAT093_ALERT_1_B No su's on H-atoms, but refinement reported as . mixed --------------------------------------------------------------------------------Alert level C ABSTY02_ALERT_1_C An _exptl_absorpt_correction_type has been given without a literature citation. This should be contained in the _exptl_absorpt_process_details field. Absorption correction given as Not Given PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT048_ALERT_1_C MoietyFormula Not Given ........................ ? PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... ? PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 2.54 PLAT125_ALERT_4_C No '_symmetry_space_group_name_Hall' Given ..... ? PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0110 Ang -------------------------------------------------------------------------------- |
8楼2012-09-07 14:50:52
9楼2012-09-07 15:19:04
10楼2012-09-07 15:22:46
130