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[求助]
求翻译一小段简单的实验操作
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A typical microwave irradiation experiment used 200 mg (1.67 mmol) of A1, 1.0 g of Ni–Al alloy, and 2 mL of H2 O in a pressure resistant glass ampoule equipped with a rubber septum and an aluminum cap. The loaded ampoule (10 mL capacity) was introduced into the cavity of the microwave apparatus and irradiated with microwaves for 60 min at 120 C. The ampoule was cooled in an ice/water bath and the organic ma- terials were extracted with ether. The ether fraction was analyzed by GC and GC-MS to identify and quantify the products. |
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2楼2012-08-29 22:09:04