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[求助]
求助微谱数据，谢谢！
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急求三个化合物的结构数据，其碳谱数据如下： 1. 30.90,31.00,32.53,32.60,33.39,39.14,50.15,51.60,58.25,64.94,66.14,68.54,70.69,71.29,115.08,118.03,123.69,124.15,128.64,130.60,132.23,134.60,143.91,146.32,151.73,158.03,170.71,221.14 2. 14.31,23.29,27.76,32.60,36.12,130.55 3. 48.56,109.32,112.70,136.22,148.41,159.41 |
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二氯甲烷
金虫 (正式写手)
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2 1 . compound 2 B10C12H24 相似度:83.3% Tetrahedron Letters 2000 41 2499-2501 Is the halogen–metal exchange faster than deprotonation in the reaction of ortho-carboranyl aryl bromide with butyllithium? Mouad Lamrani, Ryo Hamasaki, Yoshinori Yamamoto Structure 13C NMR 碳谱模拟图 2 . Z-9-nonacosene C29H58 相似度:71.4% Phytochemistry 1990 29 1625-1628 Constituents of the latex of Euphorbia antiquorum Mohan B. Gewali,Masao Hattori,Yasuhiro Tezuka,Tohru Kikuchi,Tsuneo Namba Structure 13C NMR 碳谱模拟图 3 . compound 1a C14H34N2Si 相似度:71.4% Zeitschrift für Naturforschung B 2011 66 917-922 CO2 as an Oxygen Source for Polysiloxanes - Preparation, Crystal Structure and Thermal Decomposition of Two Novel Silylcarbamates C. Wiltzsch, K. Kraushaar, A. Schwarzer, and E. Kroke Structure 13C NMR 碳谱模拟图 4 . compound 2d C13H24N2O4F6 相似度:71.4% Heterocycles 2000 53 1317-1328 Solution Parallel Synthesis of Cyclic Guanidines Christelle Marmillon, Jacques Bompart, Michèle Calas, Roger Escale,* and Pierre-Antoine Bonnet Structure 13C NMR 碳谱模拟图 5 . (Z)-2-heptene 相似度:71.4% Organic Magnetic Resonance 1973 5 147-153 Configurations and conformations in acyclic, unsaturated hydrocarbons. A 13C NMR study J. W. de Haan and L. J. M. Van de Ven Structure 13C NMR 碳谱模拟图 6 . cis-hept-2-ene 相似度:71.4% Organic Magnetic Resonance 1976 8 426-431 13C chemical shifts of some model olefins P. A. Couperus, A. D. H. Clague and J. P. C. M. van Dongen Structure 13C NMR 碳谱模拟图 7 . Compound 9 C5H15O6P2N 相似度:66.6% Bioorganic & Medicinal Chemistry Letters 2005 15 4685-4690 Synthesis and biological evaluation of 1-amino-1,1-bisphosphonates derived from fatty acids against Trypanosoma cruzi targeting farnesyl pyrophosphate synthase Sergio H. Szajnman, Esteban L. Ravaschino, Roberto Docampo, Juan B. Rodriguez Structure 13C NMR 碳谱模拟图 8 . Compound 10 C6H17O6P2N 相似度:66.6% Bioorganic & Medicinal Chemistry Letters 2005 15 4685-4690 Synthesis and biological evaluation of 1-amino-1,1-bisphosphonates derived from fatty acids against Trypanosoma cruzi targeting farnesyl pyrophosphate synthase Sergio H. Szajnman, Esteban L. Ravaschino, Roberto Docampo, Juan B. Rodriguez Structure 13C NMR 碳谱模拟图 9 . Hexyn-1-yl silver 相似度:66.6% Magnetic Resonance in Chmesitry 2004 42 831-834 Triphenylphosphane complex formation with hexyn-1-yl silver Ulla Létinois-Halbes, Patrick Pale and Stefan Berger Structure 13C NMR 碳谱模拟图 10 . compound 4a 相似度:66.6% Zeitschrift für Naturforschung B 2011 66 917-922 CO2 as an Oxygen Source for Polysiloxanes - Preparation, Crystal Structure and Thermal Decomposition of Two Novel Silylcarbamates C. Wiltzsch, K. Kraushaar, A. Schwarzer, and E. Kroke Structure 13C NMR 碳谱模拟图 11 . 1,4-dideutero-2,3-di(pentyl)buta-1,3-diene C14H26D2 相似度:66.6% Russian Journal of Organic Chemistry 2005 41 667-672 Cycloaluminizing of Acetylenes and 1,4-Enynes in the Presence of Zr-containing Catalysts U. M. Dzhemilev, A. G. Ibragimov, L. O. Khafizova, L. R. Yakupova and L. M. Khalilov Structure 13C NMR 碳谱模拟图 12 . 15-nonacosanol C29H60O 相似度:66.6% Journal of the Chinese Chemical Society 2009 56 600-605 Palaeophytochemical Components from the Miocene-Fossil Wood of Pinus griffithii Jian-Rong Luo, Qing-Yun Ma, You-Xing Zhao,Tie-Mei Yi, Cheng-Sen Li and Jun Zhou Structure 13C NMR 碳谱模拟图 13 . trans-dec-5-ene 相似度:66.6% Organic Magnetic Resonance 1976 8 426-431 13C chemical shifts of some model olefins P. A. Couperus, A. D. H. Clague and J. P. C. M. van Dongen Structure 13C NMR 碳谱模拟图 14 . 3-methyl-thiane 相似度:66.6% Organic Magnetic Resonance 1976 8 469-476 13C n.m.r. of organosulphur compounds: II—13C chemical shifts and conformational analysis of methyl substituted thiacyclohexanes Giovanna Barbarella, Pasquale Dembech, Anna Garbesi and Antonino Fava Structure 13C NMR 碳谱模拟图 15 . n-Butyl phenyl selenide 相似度:62.5% Canadian Journal of Chemistry 2009 87 678-683 On the reactivity of indium(III) benzenechalcogenolates (chalcogen = sulfur and selenium) towards organyl halides for the synthesis of organyl phenyl chalcogenides Clovis Peppe and Liérson Borges de Castro Structure 13C NMR 碳谱模拟图 16 . (R)-5-butyltetrahydrofuran-2-ol(Major isomer) C8H16O2 相似度:62.5% Organic Letters 2007 Vol. 9, No. 10 1975-1978 Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski Structure 13C NMR 碳谱模拟图 17 . 7,8-bis-bromomethyl-tetra-decane C16H32Br2 相似度:62.5% Tetrahedron Letters 2000 41 8237-8241 Solubilized zirconocene dihydride as a promotor of alkene coupling reactions Peter Wipf, Xiaodong Wang Structure 13C NMR 碳谱模拟图 18 . (E,E)-1,1,3,3-tetramethyl-1,3-bis(1-heptenyl)disiloxane C18H38OSi2 相似度:62.5% Chinese Chemical Letters 2010 21 312-316 Tri(t-butyl)phosphine-assisted selective hydrosilylation of terminal alkynes Wei Wu; Xiao Yun Zhang; Shou Xing Kang; Yan Min Gao Structure 13C NMR 碳谱模拟图 19 . compound 3f C9H16O2 相似度:62.5% Tetrahedron Letters 2004 45 9225-9227 An efficient stereoselective synthesis of (E)- and (Z)-trisubstituted alkenes from unactivated Baylis-Hillman adducts using NaBH4/CuCl2·2H2O Biswanath Das, Joydeep Banerjee, Anjoy Majhi, Gurram Mahender Structure 13C NMR 碳谱模拟图 20 . (Z)-2-octene 相似度:62.5% Organic Magnetic Resonance 1973 5 147-153 Configurations and conformations in acyclic, unsaturated hydrocarbons. A 13C NMR study J. W. de Haan and L. J. M. Van de Ven Structure 13C NMR 碳谱模拟图 21 . 2-methylhept-2-ene 相似度:62.5% Organic Magnetic Resonance 1976 8 426-431 13C chemical shifts of some model olefins P. A. Couperus, A. D. H. Clague and J. P. C. M. van Dongen Structure 13C NMR 碳谱模拟图 22 . 1-Oxaspiro[4.5]decan-2-one 相似度:57.1% Molecules 2004 9 330-348 Masked ω-Lithio Ester Enolates: Synthetic Applications Miguel Yus, Rosario Torregrosa and Isidro M. Pastor Structure 13C NMR 碳谱模拟图 23 . 1-Heptanethiol 相似度:57.1% Molecules 2009 14 4634-4643 3-(2-Aminophenyl)-4-methyl-1, 3-thiazole-2(3H)-thione as an Ecofriendly Sulphur Transfer Agent to Prepare Alkanethiols in High Yield and High Purity Mohammed Amine Mehdid, Ayada Djafri, Christian Roussel and Federico Andreoli Structure 13C NMR 碳谱模拟图 24 . cis-decalin-9-carboxylic acid C11H18O2 相似度:57.1% Helvetica Chimica Acta 1978 61 2831-2842 Photochemische Reaktionen. 99. Mitteilung. Photochemistry of N-Acylimidazoles. IV. Structural Factors Leading to Norrish Type II Elimination and to Cyclobutanol Formation in the Photolysis of Acylimidazoles Shigeo Iwasaki Structure 13C NMR 碳谱模拟图 |
3楼2012-06-28 17:05:24
二氯甲烷
金虫 (正式写手)
- 应助: 105 (高中生)
- 金币: 2190.7
- 散金: 1870
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- 性别: GG
- 专业: 天然药物化学
【答案】应助回帖
感谢参与，应助指数 +1
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1 查询结果：共查到11个化合物(查询结果仅供参考) 1 . Navirine B C30H40N2O3 相似度:53.5% Natural Product Communications 2008 3 1985-1989 Diterpenoid Alkaloids and Phenol Glycosides fromAconitum naviculare (Brühl) Stapf. Stefano Dall’Acqua, Bharat B. Shrestha , Mohan Bikram Gewali, Pramod Kumar Jha ,Maria Carrara and Gabbriella Innocenti Structure 13C NMR 碳谱模拟图 2 . Paniculatine C31H35NO7 相似度:51.7% Chemistry of Natural Compounds 2000 36 419-477 HETISANE-TYPE DITERPENOID ALKALOIDS I. A. Bessonova and Sh. A. Saidkhodzhaeva Structure 13C NMR 碳谱模拟图 3 . paniculatine 相似度:51.7% Journal of Natural Products 1989 Vol 52 430 The Structure of Paniculatine: a Revision A. Katz Structure 13C NMR 碳谱模拟图 4 . Bongkrekic acid 相似度:51.6% Tetrahedron Letters 2004 45 8863-8866 Total synthesis of (+)-bongkrekic acid Mitsuru Shindo, Tomoyuki Sugioka, Yuko Umaba, Kozo Shishido Structure 13C NMR 碳谱模拟图 5 . XML-2 相似度:51.5% The Journal of Antibiotics 1993 46 141-148 ENZYMATIC DIMERIZATION OF PENICILLIN X HITOSI AGEMATU, Tosmo TSUCHIDA, KAICHIRO KOMINATO, NORIO SHIBAMOTO, TAKEO YOSHIOKA, HIROSHI NISHIDA, ROKURO OKAMOTO, TAKASHI SHIN, SAWAO MURAO Structure 13C NMR 碳谱模拟图 6 . Benzyl 12(S)-[[N-(tert-Butyloxy)carbonyl]aminol-4-methoxy-11-o xo-10-aza-2-oxatricyclo[12.2.2.1(3,7)]nonadeca-3,5,7(19),14,16,17-hexaen-9(S)-carboxylate C31H34N2O7 相似度:50% Bioorganic & Medicinal Chemistry 1995 3 1579-1593 Key analogs of the tetrapeptide subunit of RA-VII and deoxybouvardin Dale L. Boger, Jiacheng Zhou, Brian Winter, Paul A. Kitos Structure 13C NMR 碳谱模拟图 7 . 10-N-Demethyl-10-N-(6'-phthalimidohexyl)-galanthamine C30H34N2O5 相似度:50% Bioorganic & Medicinal Chemistry 1998 6 1835-1850 Potent acetylcholinesterase inhibitors: design, synthesis, and structure–Activity relationships of bis-interacting ligands in the galanthamine series Aude Mary, Dolor Zafiarisoa Renko, Catherine Guillou, Claude Thal Structure 13C NMR 碳谱模拟图 8 . (1S,2R,5S)-5-methyl-2-[1-methyl-1-(2-naphthyl)ethyl]cyclohexyl (1S,4R)-5-(6-chloro-3-pyridyl)-2-oxa-3-azabicyclo[2.2.2]oct-5-ene-3-carboxylate C32H35N2O3Cl 相似度:50% The Journal of Organic Chemistry 1998 63 8397-8406 Total Synthesis of (?)-Epibatidine Using an Asymmetric Diels?Alder Reaction with a Chiral N-Acylnitroso Dienophile Sakae Aoyagi, Ryuta Tanaka, Masaichi Naruse, and Chihiro Kibayashi Structure 13C NMR 碳谱模拟图 9 . 5,11,17,23-tetra-(tert-butyl)-25,27-bis[3-(phenoxyacetyl)penicillopropyloxy]-26,28-dihydroxycalix[4]arene C82H100N4O14S2 相似度:50% Bioorganic & Medicinal Chemistry 2011 19 7534-7540 Molecular drug-organiser: Synthesis, characterization and biological evaluation of penicillin V and/or nalidixic acid calixarene-based podands Adel Ben Salem, Guillaume Sautrey, Stéphane Fontanay, Rapha?l E. Duval, Jean-Bernard Regnouf-de-Vains Structure 13C NMR 碳谱模拟图 10 . 2-(4-hydroxymethyl-1,3,4,5-tetrahydroxy-2-piperidinyl)-2-[(O-t-butylcarbonyl)tyrosylamino]acetic acid n-butyl ester p-toluenesulfonate salt 相似度:50% The Journal of Antibiotics 2000 53 1282-1292 Synthesis and Activity of Analogues of SB-219383: Novel Potent Inhibitors of Bacterial Tyrosyl tRNA Synthetase JOHN M. BERGE,NIGEL J. P. BROOM,CATHERINE S. V. HOUGE-FRYDRYCH,RICHARD L. JARVEST,LUCY MENSAH,DAVID J. MCNAIR,PETER J. O'HANLON,ANDREW J. POPE and STEPHEN RITTENHOUSE Structure 13C NMR 碳谱模拟图 11 . 6'-O-cinnamoylmussaenosidic acid C25H30O11 相似度:50% Journal of Natural Products 2011 74 943-948 HCV-NS3/4A Protease Inhibitory Iridoid Glucosides and Dimeric Foliamenthoic Acid Derivatives from Anarrhinum orientale Riham Salah El Dine, Azza R. Abdel Monem, Ali M. El-Halawany, Masao Hattori, and Essam Abdel-Sattar Structure 13C NMR 碳谱模拟图 |
2楼2012-06-28 17:03:52
二氯甲烷
金虫 (正式写手)
- 应助: 105 (高中生)
- 金币: 2190.7
- 散金: 1870
- 红花: 15
- 帖子: 538
- 在线: 120.8小时
- 虫号: 1337209
- 注册: 2011-07-04
- 性别: GG
- 专业: 天然药物化学
【答案】应助回帖
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yubo7758: 金币+1, ★★★★★最佳答案 2012-10-18 15:27:28
yubo7758: 金币+1, ★★★★★最佳答案 2012-10-18 15:27:28
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1 . ellagic acid 3 相似度:71.4% Chemistry & Biodiversity 2004 Vol.1 426 Novel Lipid-Peroxidation- and Cyclooxygenase-Inhibitory Tannins from Picrorhiza kurroa Seeds Yanjun Zhang, David L. DeWitt, Sorimuthu Murugesan, and Muraleedharan G. Nair Structure 13C NMR 碳谱模拟图 2 . ellagic acid 相似度:71.4% China Journal of Chinese Materia Medica 2007 32 496-500 Studies on chemical constituents in fruits of Eucalyptus globulus YANG Xiuwei, GUO Qingmei Structure 13C NMR 碳谱模拟图 3 . ellagic acid C14H6O8 相似度:71.4% China Journal of Chinese Materia Medica 2006 31 1503-1506 Studies on chemical constituents in roots of Euphorbia soongarica SHI Xinhong, DU xiaohong, DU Xiaoli, KONG Lingyi Structure 13C NMR 碳谱模拟图 4 . 鞣花酸 相似度:71.4% China Journal of Chinese Materia Medica 2005 30 1131-1132 思茅蛇菰的化学成分研究 II 戴 忠, 王钢力, 刘 燕, 张 继, 林瑞超 Structure 13C NMR 碳谱模拟图 5 . ellagic acid 相似度:71.4% China Journal of Chinese Materia Medica 2002 27 43-45 Studies on the Chemical Constituents in the Leaves of Cyclocarya paliurus YI Xing, SHI Jiangong, ZHOU Guangxiong, XIE Mingyong Structure 13C NMR 碳谱模拟图 6 . Ellagic acid C14H6O8 相似度:71.4% Natural Product Sciences 2008 14 1-11 Peroxynitrite scavengers from Phellinus linteus Jeong, Da-Mi; Jung, Hyun-Ah; Kang, Hye-Sook; Choi, Jae-Sue Structure 13C NMR 碳谱模拟图 7 . ellagic acid 相似度:71.4% Zeitschrift für Naturforschung B 2005 60b 555-560 Tannins and Flavonoids from the Erodium cicutarium Herb Izabela Fecka and Wojciech Cisowski Structure 13C NMR 碳谱模拟图 8 . ellagic acid C14H6O8 相似度:71.4% Phytochemistry 1990 29 251-256 Ellagic compounds from Diplopanax stachyanthus Duc Do Khac,Sung Tran-Van,Angela Martha Campos,Jean-Yves Lallemand,Marcel Fetizon Structure 13C NMR 碳谱模拟图 9 . ellagic acid C14H6O8 相似度:71.4% Molecules 2010 15 1453-1465 Identification of Major Phenolic Compounds from Nephelium lappaceum L. and Their Antioxidant Activities Nont Thitilertdecha, Aphiwat Teerawutgulrag, Jeremy D. Kilburn and Nuansri Rakariyatham Structure 13C NMR 碳谱模拟图 10 . 鞣花酸 相似度:71.4% Chinese Traditional and Herbal Drugs 2000 31 92-93 青岛老鹳草化学成分的研究 李琳波,马天波,肖月星,崔宝国,王玉丽 Structure 13C NMR 碳谱模拟图 11 . ellagic acid 相似度:71.4% Chinese Pharmaceutical Journal 2011 46 20-23 Polyphenols from Potentilla discolor Bunge ZHANG Wei-wei, ZHANG Peng, CHENG Wei, WANG Bin, WANG Jing-li, ZHANG Qing-ying*, LIANG Hong, ZHAO Yu-ying Structure 13C NMR 碳谱模拟图 12 . ellagic acid 相似度:71.4% Journal of Shenyang Pharmaceutical University 2010 27 530-532 Constituentswith anti-diabetic activity from the involucre of Castanea mollissima Blume. ZHANG Lin, GAO Hui-yuan, Masaki BABA, Yoshihito OKADA, Toru OKUYAMA, WU Li-jun Structure 13C NMR 碳谱模拟图 13 . ellagic acid 相似度:71.4% Bioscience, Biotechnology, and Biochemistry 2001 65 1869-1871 Ellagic Acid Formation from Galloylglucoses by a Crude Enzyme of Cornus capitata Adventitious Roots Norie TANAKA, Koichiro SHIMOMURA, Kanji ISHIMARU Structure 13C NMR 碳谱模拟图 14 . Ellagic acid 相似度:71.4% Acta Pharmaceutica Sinica 2010 45 334-337 One new galloyl glycoside from fresh leaves of Psidium guajava L. SHU Ji-cheng, CHOU Gui-xin* Structure 13C NMR 碳谱模拟图 15 . 4-Bromo-2-methoxybenzenamine 相似度:57.1% Canadian Journal of Chemistry 2009 87 440-447 Synthesis of arylbromides from arenes and Nbromosuccinimide (NBS) in acetonitrile - A convenient method for aromatic bromination Eli Zysman-Colman, Karla Arias, and Jay S. Siegel Structure 13C NMR 碳谱模拟图 16 . ellagic acid 相似度:57.1% Chinese Traditional and Herbal Drugs 2008 39 1612-1616 Chemical constituents of Discocleidion rufescens(Ⅲ) ZHU Hua-xu; TANG Yu-ping; GONG Zhu-nan; MIN Zhi-da Structure 13C NMR 碳谱模拟图 17 . N,N,N',N'-Tetrupropyl-furan-2,5-dicarboxamid C18H30N2O3 相似度:50% Helvetica Chimica Acta 1980 63 191-196 Ionophore vom Typ der 3-Oxapentandiamide Ern? Pretsch, Daniel Ammann, Hans F. Osswald, Mare Güggi, Wilhelm Simon Structure 13C NMR 碳谱模拟图 18 . formylpyrrothine C7H6N2O2S2 相似度:50% Journal of Natural Products 2010 73 1164-1166 Dithiolopyrrolone Antibiotic Formation Induced by Adding Valeric Acid to the Culture Broth of Saccharothrix algeriensis Rabiaa Merrouche, Noureddine Bouras, Yannick Coppel, Florence Mathieu, Marie-Carmen Monje, Nasserdine Sabaou and Ahmed Lebrihi Structure 13C NMR 碳谱模拟图 19 . pyromucic acid 相似度:50% Acta Pharmaceutica Sinica 2002 Vol 37 784-787 STUDIES ON THE CHEMICAL CONSTITUENTS OF SPATHOLOBUS SUBERECTUS DUNN CUI Yan jun; LIU Ping; CHEN Ruo yun Structure 13C NMR 碳谱模拟图 20 . 2-trideuteriomethylpyridine-4,6-d2 相似度:50% Journal of Heterocyclic Chemistry 2009 46 213-216 Synthesis and spectroscopic properties of some di-and trideuterated methylpyridines James W. Pavlik,Tharinee Vongnakorn and Supawan Tantayanon Structure 13C NMR 碳谱模拟图 21 . N1,N4-bis(1H-1,2,4-triazol-3-yl)phenylenediformamidine C12H12N10 相似度:50% Journal of Heterocyclic Chemistry 2009 46 837-842 Utility of p-phenylenediformamidine in the synthesis of bisazoles and phenanthroline Saleh M. Al-Mousawi and Abdel-Zaher A. Elassar Structure 13C NMR 碳谱模拟图 22 . 5-Methyl-2-morpholino-7H-1,3,4-thiadiazolo[3,2-a]pyrimidin- 7-one C10H13N4O2S 相似度:50% Journal of Heterocyclic Chemistry 2005 42 1105-1109 Preparation of 2-amino-5-methyl-7H-1,3,4-thiadiazolo[3,2-]pyrimidin-7-ones Saifidin Safarov,Muhamacho Ahmadovich Kukaniev,Heinz Kolshorn and Herbert Meier Structure 13C NMR 碳谱模拟图 23 . 5-(2-Furfurylidene)barbituric acid C9H6N2O4 相似度:50% Journal of Heterocyclic Chemistry 2001 38 655-657 A simple method for knoevenagel condensation of ,β-conjugated and aromatic aldehydes with barbituric acid Branko S. Jursic Structure 13C NMR 碳谱模拟图 24 . 4-chloro-5-(dimethylamino)-2H-pyridazin-3-one C6H8N3OCl 相似度:50% Journal of Heterocyclic Chemistry 2000 37 1591-1595 Reaction of chloropyridazines with N,N-dimethylformamide Woo Song Lee, Yong-Jin Yoon and Sung-Kyu Kim Structure 13C NMR 碳谱模拟图 25 . 4-chloro-5-(dimethylamino)-2-methyl-2H-pyridazin-3-one C7H10N3OCl 相似度:50% Journal of Heterocyclic Chemistry 2000 37 1591-1595 Reaction of chloropyridazines with N,N-dimethylformamide Woo Song Lee, Yong-Jin Yoon and Sung-Kyu Kim Structure 13C NMR 碳谱模拟图 26 . 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4楼2012-06-28 17:06:55
5楼2012-06-29 08:00:03
