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表1.1 玉米淀粉的化学组成 Table 1.1 Chemical composition of corn starch 图1.1 α-D-葡萄糖 Fig. 1.1 α-D-glucose 图1.2 (a)直连淀粉和(b)支链淀粉的分子结构 Fig. 1.2 Molecular structure of (a) amylose and (b) amylopectin 图1.3 淀粉颗粒的环层结构 Fig. 1.3 Annulate layer structure of starch granule 图1.4 淀粉颗粒的超大分子模型 Fig. 1.4 Supramolecular model of starch granule 表1.2 四种常规聚合方法之比较 Table 1.2 Comparison of four conventional polymerization methods 表1.3 国内淀粉接枝引发体系概况 Table 1.3 Domestic overview of initiating systems for starch grafting 图1.5 电磁波谱 Fig. 1.5 The electromagnetic spectrum 图1.6 微波中的电场和磁场 Fig. 1.6 Electric and magnetic field components in microwaves 图1.7 微波中电场的两种加热机理 Fig. 1.7 Two heating mechanisms of electric component in microwaves 图1.8 微波加热与油浴加热的温度分布对比 Fig. 1.8 Comparison temperature profiles of microwave heating and oil-bath heating 表1.4 传统加热与微波加热的主要区别 Table 1.4 Main differences between conventional heating and microwave heating 图1.9 微波辅助有机合成和微波辅助聚合的发展趋势 Fig. 1.9 Publication trends of microwave-assisted organic synthesis and microwave-assisted polymerization 图1.10 微波合成的优点 Fig. 1.10 Merits of microwave synthesis 图示1.1 传统法、微波引发和微波辅助合成接枝共聚物的示意图 Scheme 1.1 Schematic representation for the synthesis of graft copolymer using conventional, microwave-initiated and microwave-assisted method 表1.5 不同种类的多糖在微波下的改性 Table 1.5 Various polysaccharides and their modification under microwaves 图示1.2 淀粉接枝共聚物的微波辅助合成与焦化废水处理应用 Scheme 1.2 Microwave-assisted synthesis of starch graft copolymer and its application in the treatment of coking wastewater 表2.1 实验药品明细 Table 2.1 Chemical reagents 表2.2 实验仪器清单 Table 2.2 Experimental equipments 表2.3 玉米淀粉的水分含量 Table 2.3 Moisture content of corn starch 图2.1 玉米淀粉的粒径分布 Fig. 2.1 Particle size distribution of corn starch 图2.2 红外测温校正曲线 Fig. 2.2 Calibration curve of the infrared thermometer 图2.3 淀粉的显微照片 Fig. 2.3 Microphotographs of starches 图2.4 不同处理淀粉的SEM照片：(a)原淀粉、(b)水浴30 min和(c)微波10 min Fig. 2.4 SEM images of starches (a) native starch, (b) water-bath for 30 min, and (c) microwave irradiation for 10 min 图2.5 葡萄糖、水浴糊化淀粉、微波糊化淀粉、空白试样的菲林反应 Fig. 2.5 Fehling reactions of glucose, water-bath gelatinized starch, microwave gelatinized starch, and blank 图2.6 不同淀粉的红外光谱图：(a)原淀粉；(b)微波糊化淀粉；(c)水浴糊化淀粉 Fig. 2.6 FTIR spectra of different starches: (a) native starch, (b) microwave gelatinized starch and (c) water-bath gelatinized starch 图2.7 不同微波辐照时间淀粉的红外光谱图：(a)5 min；(b)10 min；(c)15 min Fig. 2.7 FTIR spectra of starches with various irradiation times: (a) 5 min, (b) 10 min and (c)15 min 图2.8 淀粉的Zeta电势分析 Fig. 2.8 Zeta potential analysis of starches. Data correspond to mean ± s.d.; n=30. 图示3.1 接枝反应机理 Scheme 3.1 Mechanism of grafting 图示3.2 对苯二酚淬灭自由基 Scheme 3.2 Free radicals quenching by p-hydroquinone 图3.1 微波反应器装置图 Fig. 3.1 Setup of the microwave reactor 表3.1 实验药品明细 Table 3.1 Chemical reagents 表3.2 实验仪器清单 Table 3.2 Experimental equipments 表3.3 产物的溶解度 Table 3.3 Solubility of the products 图3.2 反滴定法的终点现象（左） Fig. 3.2 Endpoint of the inverse titration (left) 图3.3 80 mL水在不同微波功率下的升温曲线 Fig. 3.3 Temperature curves of 80-mL water heated under various microwave powers 图3.4 微波辐照时间对GE和CD的影响 Fig. 3.4 Effect of time of microwave irradiation on GE and CD 图3.5 微波辐照功率对GE和CD的影响 Fig. 3.5 Effect of power of microwave irradiation on GE and CD 图3.6 过硫酸钾浓度对GE和CD的影响 Fig. 3.6 Effect of concentration of KPS on GE and CD 图3.7 两种单体配比对GE和CD的影响 Fig. 3.7 Effect of AM-to-DADMAC ratio on GE and CD 图3.8 两种单体总量对GE和CD的影响 Fig. 3.8 Effect of monomer-to-starch ratio on GE and CD 表3.4 不同报道产品的特性黏度和分子量比较 Table 3.4 Comparison of intrinsic viscosity and molecular weight of different reported products 图4.1 (a)原淀粉和(b)接枝淀粉的SEM照片 Fig. 4.1 SEM images of (a) native starch and (b) grafted starch 图4.2 淀粉接枝共聚物的能谱分析 Fig. 4.2 EDS analysis of St-g-P(AM-DADMAC) 表4.1 元素分析结果 Table 4.1 Elemental analysis results 图4.3 XRD谱图（a）玉米淀粉；（b）接枝侧链；（c）接枝淀粉 Fig. 4.3 XRD of (a) native starch, (b) grafted side chain and (c) grafted starch 图4.4 (a)原淀粉、(b)糊化淀粉和(c)回生淀粉的XRD谱图[37] Fig. 4.4 XRD[37] of (a) native starch, (b) gelatinized starch, and (c) retrograded starch 图4.5 (a)淀粉、(b)AM、(c)DADMAC和(d)接枝产品的红外光谱图 Fig. 4.5 FTIR spectrum of (a) St, (b) AM, (c) DADMAC and (d) St-g-P(AM-DADMAC) 表5.1 实验药品明细 Table 5.1 Chemical reagents 表5.2 实验仪器清单 Table 5.2 Experimental equipments 图5.1 浊度标准曲线 Fig. 5.1 Standard curve of turbidity (n = 3; error bars, ± s.d.) 图5.2 PFS、PAFC和PAC处理焦化废水效果 Fig. 5.2 Image of coking wastewater treated by PFS, PAFC and PAC 图5.3 三种无机絮凝剂对CODCr的去除效果 Fig. 5.3 Dose of three inorganic flocculants on CODCr removal 图5.4 无机絮凝剂对色度去除效果 Fig. 5.4 Dose of three inorganic flocculants on chroma removal 图5.5 有机絮凝剂处理焦化废水效果对比 Fig. 5.5 Image of coking wastewater treated by three organic flocculants 图5.6 PFS与有机絮凝剂组合对CODCr、色度和浊度的脱除率 Fig. 5.6 PFS combined with organic flocculants on CODCr, chroma and turbidity removal 图5.7 沉降物显微形态对比 Fig. 5.7 Comparison of microscopic morphologies of the flocs 图5.8 CPAM浓度对CODCr、色度和浊度的影响 Fig. 5.8 CPAM concentration on CODCr, chroma and turbidity removal 图5.9 CTAB浓度对CODCr、色度和浊度的影响 Fig. 5.9 Effect of CTAB concentration on CODCr, chroma and turbidity removal 图5.10 产品投加量对CODCr、色度和浊度的影响 Fig. 5.10 Concentration of St-g-P(AM-DADMAC) on CODCr, chroma and turbidity removal 图5.11 絮凝处理前后焦化废水的照片 Fig. 5.11 Photo of coking wastewater before and after flocculation treatment 图5.12 CPAM和产物处理焦化废水絮体形态对比 Fig. 5.12 Comparison of morphologies of flocs from coking wastewater treated by CPAM and the product 图5.13 (a)原水自沉降物、(b)加产物所得沉降物的SEM照片 Fig. 5.13 SEM images of flocs from (a) self-sedimentation and (b) with the addition of the product 表5.3 处理焦化废水效果对比 Table 5.3 Comparison of coking wastewater treatment |
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thorny_rose
金虫 (小有名气)
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sltmac: 金币+1 2012-06-04 09:21:03
sltmac: 金币+25, 翻译EPI+1 2012-06-25 09:34:29
sltmac: 金币+1 2012-06-04 09:21:03
sltmac: 金币+25, 翻译EPI+1 2012-06-25 09:34:29
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1、图1.4中你用"supramolecular"来表达超大分子，因为我也不懂这个专业，只是想问一下，超分子与大分子应该有区别的吧？ 2、图 1.8 译为Temperature profiles comparison of microwave heating and oil-bath heating会不会更好一些？ 3、图1.9中的“发展趋势”为什么不用简单的"development"而选择了"publication"呢？ 4、图示1.1中的using可以用by来代替（仅供参考）； 5、表1.5 不同种类的多糖在微波下的改性可译为“different types of polysaccharide modified under microwave”； 6、图2.7译文中应在various后加上microwave； 7、图3.2按你中文的意思应该是苯二酚中的自由基被淬灭了，可你的译文则成了苯二酚淬灭了自由基； 8、图3.4译文可简单点，直接就是effect of microwave irradiation time on the GE and CD，同理图3.5译文； 9、图4.3和图4.4中“谱图”（spectrogram)没有译出； 10、图5.3译文参考：removal efficiency of CODCr by three kinds of flocculants，同理图5.4; 11、图5.5的中文是否应为“三种”有机絮凝剂……更为准确些； 12、图5.6脱除率为removal rate; 13、图5.10中你将产品投加量译为了concentration of……是否准确？ 14、表5.3译文参考：effects comparison of …… |
2楼2012-06-03 17:26:21
