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xingyu6203

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[求助] 15个BB求ZnO的XRD标准曲线啊，灰常感谢

15个BB求ZnO的XRD标准曲线啊，灰常感谢
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1楼 2012-05-17 11:58:29
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duyuhai

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【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
xingyu6203: 金币+15, ★有帮助 2012-07-20 10:07:57
PDF#36-1451: QM=Star(S); d=Diffractometer; I=Diffractometer
Zincite, syn
Zn O        Colorless
Radiation=CuKa1        Lambda=1.5405981        Filter=Graph
Calibration=        2T=31.769-142.910        I/Ic(RIR)=
Ref: McMurdie, H., Morris, M., Evans, E., Paretzkin, B., Wong-Ng, W., Ettlinger, L., Hubbard, C.
Powder Diffraction, v1 p76 (1986)
Hexagonal - Powder Diffraction,  P63mc (186)        Z=2        mp=
CELL: 3.24982 x 3.24982 x 5.20661 <90.0 x 90.0 x 120.0>        P.S=hP4 (S Zn)
Density(c)=5.675        Density(m)=6.43A        Mwt=81.38        Vol=47.62        F(27)=129.6(.0072,29/0)
Ref: 1. Bragg, W.
Philos. Mag., v39 p647 (1920)
Strong Lines: 2.48/X 2.81/6 2.60/4 1.62/3 1.48/3 1.91/2 1.38/2 1.36/1 0.91/1 1.09/1
NOTE:  The sample was obtained from the New Jersey Zinc Co., Bethlehem, Pennsylvania, USA.
References to other early patterns may be found in reference (5).
The structure was determined by Bragg (1) and refined by Abrahams, Bernstein (2).
A high pressure cubic NaCl-type of ZnO is reported by Bates et al.
(3) and a cubic, sphalerite type is reported by Radczewski, Schicht (4).
The approximate temperature of data collection was 26 C.
To replace 00-005-0664 (5).
See ICSD 31052 (PDF 01-075-1526).

2-Theta    d(Å   I(f)  ( h k l)   Theta  1/(2d)   2pi/d  n^2  
31.769  2.8143   57.0  ( 1 0 0)  15.885  0.1777  2.2326     
34.421  2.6033   44.0  ( 0 0 2)  17.211  0.1921  2.4135     
36.252  2.4759  100.0  ( 1 0 1)  18.126  0.2019  2.5377     
47.538  1.9111   23.0  ( 1 0 2)  23.769  0.2616  3.2877     
56.602  1.6247   32.0  ( 1 1 0)  28.301  0.3077  3.8672     
62.862  1.4771   29.0  ( 1 0 3)  31.431  0.3385  4.2537     
66.378  1.4072    4.0  ( 2 0 0)  33.189  0.3553  4.4652     
67.961  1.3782   23.0  ( 1 1 2)  33.981  0.3628  4.5590     
69.098  1.3583   11.0  ( 2 0 1)  34.549  0.3681  4.6259     
72.560  1.3017    2.0  ( 0 0 4)  36.280  0.3841  4.8268     
76.953  1.2380    4.0  ( 2 0 2)  38.476  0.4039  5.0752     
81.368  1.1816    1.0  ( 1 0 4)  40.684  0.4231  5.3174     
89.604  1.0931    7.0  ( 2 0 3)  44.802  0.4574  5.7479     
92.781  1.0638    3.0  ( 2 1 0)  46.390  0.4700  5.9061     
95.301  1.0423    6.0  ( 2 1 1)  47.650  0.4797  6.0284     
98.609  1.0159    4.0  ( 1 1 4)  49.305  0.4922  6.1845     
102.942  0.9846    2.0  ( 2 1 2)  51.471  0.5078  6.3812     
104.130  0.9766    5.0  ( 1 0 5)  52.065  0.5120  6.4335     
107.426  0.9556    1.0  ( 2 0 4)  53.713  0.5232  6.5751     
110.388  0.9381    3.0  ( 3 0 0)  55.194  0.5330  6.6976     
116.274  0.9069    8.0  ( 2 1 3)  58.137  0.5513  6.9279     
121.567  0.8826    4.0  ( 3 0 2)  60.783  0.5665  7.1193     
125.183  0.8677    1.0  ( 0 0 6)  62.591  0.5762  7.2414     
133.925  0.8370    3.0  ( 2 0 5)  66.963  0.5973  7.5065     
136.513  0.8293    1.0  ( 1 0 6)  68.257  0.6029  7.5767     
138.505  0.8237    2.0  ( 2 1 4)  69.253  0.6070  7.6280     
142.910  0.8125    3.0  ( 2 2 0)  71.455  0.6154  7.7334
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2楼2012-05-17 16:22:23
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xingyu6203

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引用回帖:
2楼: Originally posted by duyuhai at 2012-05-17 16:22:23:
PDF#36-1451: QM=Star(S); d=Diffractometer; I=Diffractometer
Zincite, syn
Zn O        Colorless
Radiation=CuKa1        Lambda=1.5405981        Filter=Graph
Calibration=        2T=31.769-142.910        I/Ic(RIR)=
Ref: McMurdie, H ...

用哪2列啊谢谢啊
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幸福就是每天吃饱了撑着睡觉
3楼2012-05-17 16:46:40
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