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2£¬ ´ò¿ªÊý¾Ý£ºfile ---> open pattern file --->2INSTRM=0:Free F.(Ti. Step.Tf) ---> OK --->kcnQH.dat
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Point selection ---> Automatic peak search ---> ÔÚµ¯³ö¶Ô»°¿òÖÐ Peak threshold ĬÈÏÖµÊÇ0.02£¬¿ÉÒԸijÉ0.05¡£Ñ¡ÔñSearch CuKa1/CuKa2 (¶ÔÓ¦X ÉäÏßÊý¾Ý) »òÕß Search single peaks (¶ÔÓ¦ÖÐ×ÓÑÜÉäÊý¾Ý)¡£×îÏÂÃæÒ»ÐÐÑ¡ÉÏDisplay Bragg peaks position ---> OK ---> µ¯³ö¶Ô»°¿ò£¨Automatic peaks search results 26?(maybe) peaks have been found£©---> È·¶¨
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µãÊó±ê×ó¼üÔÚÑÜÉäͼÉÏÍÏÀ£¬¿ÉÒÔ·Å´ó¾Ö²¿---> Points selection ---> Remove peaks/Background points ---> ×ó¼üµã»÷Ҫɾ³ýµÄ·å---> ÔÚ»ÃæÉϵãÓÒ¼ü»Ö¸´Í¼ÐÎÔ´óС¡££¨ÕâÒ»¹ý³Ì¿ÉÄÜÒª¶à´ÎÖظ´ÒÔ±ãɾ³ýËùÓв»ÏëÓÃÀ´Ö¸±ê»¯µÄ·å¡££©
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Points selection --->Save as (×¢Òâ²»ÊÇSave peaks) ---> Save points for Dicvol 04 ---> ÔÚµ¯³ö¶Ô»°¿òÖÐÌîдÌõ¼þ
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---> OK --->OK --->µ¯³ö¶Ô»°¿ò Edit Dicvol04 input file? ---> ¿ÉÒÔÑ¡¡°ÊÇ¡±Ò²¿ÉÒÔÑ¡¡°·ñ¡±£¬Ñ¡Ôñ¡°ÊÇ¡±¿ÉÒԲ鿴»ò±à¼Ò»ÏÂ×Ô¼ºËùÑ¡ÔñµÄ·åλ»òÎó²îµÈÌõ¼þ£¬±£´æһϣ¬È»ºó¹Ø±Õ¸Ã´°¿Ú¡£Ö®ºóºÍÑ¡Ôñ¡°·ñ¡±Ò»Ñù--->ÈôÑ¡¡°·ñ¡±£¬---> µã°´Å¥ Dicvol---> µ¯³ö¶Ô»°¿ò Select Dicvol input file---> ÕÒµ½ºó׺Ϊ.dic04 µÄÎļþ£¬´ò¿ª--->Dicvol ÔËÐУ¬Íê±Ïºóµ¯³ö¶Ô»°¿ò£¬Ñ¡ÔñX-Ray diffractometer ϵÚÒ»Ïî conventional powder diffractometer £¨Èç¹ûÊÇÖÐ×ÓÑÜÉäÊý¾Ý£¬Ñ¡Ôñmy neutron powder diffraction--->OK--->U,V,WÖµ±£³ÖĬÈÏ--->OK£©---> OK---> Kenvao --->Ö¸±ê»¯½áÊø¡£
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