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fengqianxv

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[交流] actE 编辑回信请教 已有1人参与

1. The O atoms of both nitro groups exhibit high thermal motion. Might a disorder model be more appropriate?  Please discuss this.
O原子没有无序现象,这个怎么回应?

3. Your software references list all Bruker software, but your Figures at least look like they were produced with PLATON. Correct this.
图确实是PLATON画的,但是以前发的文章都是用Bruker software参考的?

6.  In Related Literature, describe how the 'related structures' cited in Vicente et al (2005) actually relate to the structure in this manuscript.
是让描述两者结构如何相关吗?
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linhua0402313

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1. The O atoms of both nitro groups exhibit high thermal motion. Might a disorder model be more appropriate?  Please discuss this.
硝基的O原子温度因子高,是不是有可能存在无序现象,请解释?
你可以尝试无序处理,即让氧原子部分占据自由精修,看占有率的大小,如果接近100%,说明没有无序现象的存在,温度因子高只能从其他方面解释,比如配位环境等做解释,如果占有率不是接近100%,则告诉占据率,并重新精修数据。

3. Your software references list all Bruker software, but your Figures at least look like they were produced with PLATON. Correct this.
你文中的图看起来PLATON画的,但是引用的文献确实用Bruker software,请确认或更正?

6.  In Related Literature, describe how the 'related structures' cited in Vicente et al (2005) actually relate to the structure in this manuscript.
是让描述两者结构如何相关吗?  是的
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2楼2012-05-07 15:02:12
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fengqianxv

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3楼2012-05-07 15:09:11
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