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wangguomin7322金虫 (小有名气)
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[求助]
求助各位高手翻译一个有机合成的步骤
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| Under the nitrogen air current, at 0 degree C, 25 mg (0.2mmol) of dimethylamino pyridine and 4.3 ml (30.6mmol) of triethylamine were added to 10 ml of anhydrous salt-ized methylene solution of the furfuryl alcohol 2g (20.4mmol), and it agitated as it is for 10 minutes. Subsequently, 3.3 ml (26.5mmol) of chloride pivalate was dropped at this solution, and it agitated by the ** for 30 minutes. |
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8814402
至尊木虫 (职业作家)
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wangguomin7322: 金币+2, 翻译EPI+1 2012-05-04 22:53:45
wangguomin7322: 金币+2, 翻译EPI+1 2012-05-04 22:53:45
| Under the nitrogen air current, at 0 degree C, 25 mg (0.2mmol) of dimethylamino pyridine and 4.3 ml (30.6mmol) of triethylamine were added to 10 ml of anhydrous salt-ized methylene solution of the furfuryl alcohol 2g (20.4mmol), and it agitated as it is for 10 minutes. 氮气流、0摄氏度条件下，向10mL含2g呋喃甲醇的无水盐化甲叉溶液中加入25mg二甲氨基吡啶和4.3mL三乙胺，搅拌10min。Subsequently, 3.3 ml (26.5mmol) of chloride pivalate was dropped at this solution, and it agitated by the ** for 30 minutes.随后，向溶液中滴入3.3mL chloride pivalate（特戊酸氯化物？），搅拌30min。 |
2楼2012-05-03 16:40:28
wangguomin7322
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3楼2012-05-04 22:54:19
8814402
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4楼2012-05-05 08:13:33
wangguomin7322
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5楼2012-05-05 18:46:13
8814402
至尊木虫 (职业作家)
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6楼2012-05-05 23:37:04
