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xizhao2000

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xizhao2000: ½ð±Ò+10, ·­ÒëEPI+1, ¡ïÓаïÖú, лл~ 2012-04-17 16:58:15
xizhao2000: ½ð±Ò+20, ¡ïÓаïÖú 2012-04-17 22:58:19
xizhao2000: ½ð±Ò+20, ¡ïÓаïÖú 2012-04-18 20:20:57
Based on synthetizing ¦Â- zeolite by solid phase method at low cost in the earlier stages of laboratory, we have performed semi-works production according to the optimal synthetic scheme, further have optimizated the existing industrialized synthetic raw material, have realized the transition of industrialized raw material and technology; further have optimizated crystallization accelerator, material ratio and crystallization time by adding the crystallization accelerator; and have determined the stirrer suitable for agitated reactor. We have solved the problems in the course of enlargement experiment, so as to save raw materials and energy consumption, increase production efficiency and product quality, improve the comprehensive cost performance of ¦Â- zeolite, further decreasing the cost of production. We have succeeded to synthetize a number of ¦Â- zeolite products at pilot scale production by the method at the different feeding ratios of silicon and aluminium, and have performed comprehensive analysis of characterization for the adsorption of XRD, XRF, ft-ir, SEM, Py-IR, NH3-TPD and N2. We have synthetized ¦Â- zeolite with different ratios of silicon and aluminium at pilot scale production as active components, have introduced into mode catalyst, have tested its catalytic activity in micro live evaluation device, and have optimized active sample in fixed fluid bed to investigate catalytic cracking performance. Finally, we have obtained a set of solid phase method at low cost for synthetizing ¦Â- zeolite and pilot scale production of performance test, thereby gathering experience for the industrial production.
2Â¥2012-04-17 09:00:56
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

Ƶ»Øíííù

ÖÁ×ðľ³æ (Ö°Òµ×÷¼Ò)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

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xizhao2000: ½ð±Ò+15, ¡ïÓаïÖú, лл°¡~ 2012-04-17 16:58:42
xizhao2000: ½ð±Ò+30, ¡ïÓаïÖú 2012-04-17 22:58:30
xizhao2000: ½ð±Ò+5, ¡ïÓаïÖú 2012-04-18 20:21:04
This paper has a research on the pilot-plant test in a optimized way ,which based on the early laboratory  research  on the solid phase method to obtain the low cost zeolite Beta .We prefer the industry raw material to achieve the commercial process .We add crystallization promoter to further optimization of crystallization promoter mmaterial composition and crystallization time and determine the suitable for agitator type of reactor .In this way ,we can solove the problem encountered in the laboratory and we can reach such a purpose ,saving raw materials and energy consumption ,improving production efficiency and product quality ,improving the comprehensive performance of zeolit Beta .In this way ,we have successfully synthsised a batch of zeolite Beta ,and we have totally analysised the product with XRD ,XRF ,FT-IR ,SEM ,PY-IR ,NH3-TPD ,and N2 absorption .We try to zoom in synthesis of zeolite Beta for active components of different silica alumina ratio, which is introduced into model catalysts, testing their catalytic activity on evaluation of micro-device, and selection activity better samples at fixed fluidized-bed catalytic cracking unit study on the performance .At last we achieved a suit of solid phase methods to synthesis the zeolite Beta ,which contribute to the industry product .
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3Â¥2012-04-17 09:44:48
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
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