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[求助]
跪求能用微谱数据库的虫子们，帮忙查一下碳谱数据，本人送6个金币！！！
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跪求：能用微谱数据库的虫子们，帮忙查下列三萜类化合物的C谱数据的目核及文献，文献越近越好，本人送6个金币！多谢虫侠！ 化合物1的C谱： 216.98,141.63,123.93,76.50,51.31,50.83,47.68,47.61,46.61,45.40,41.95,39.35,38.44,38.04,36.31,34.04,31.97,31.93,30.47,27.22,25.33,25.26,25.02,23.90,20.59,20.52,16.87,15.15,13.91 化合物2的C谱： 217.08,141.68,124.00,71.79,50.89,47.72,47.66,46.62,45.26,44.99,42.09,39.59,36.77,34.60,34.09,33.54,32.00,31.82,28.77,27.27,25.49,25.28,24.98,23.79,20.54,20.48,16.95,16.35,12.83 化合物3的C谱： 216.64,213.16,141.71,123.47,53.45,50.75,47.61,47.48,46.52,45.08,44.62,41.91,40.21,39.34,37.31,36.51,33.98,31.90,31.52,27.09,25.20,24.99,23.97,21.88,20.49,16.75,13.32,11.57 |
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2楼2012-04-02 13:22:51
3楼2012-04-02 14:52:00
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化合物1 的C谱： 13.91,15.15,16.87,20.52,20.59,23.9,25.02,25.26,25.33,27.22,30.47,31.93,31.97,34.04,36.31,38.04,38.44,39.35,41.95,45.4,46.61,47.61,47.68,50.83,51.31,76.5,123.93,141.63,216.98 化合物2的碳谱： 12.83,16.35,16.95,20.48,20.54,23.79,24.98,25.28,25.49,27.27,28.77,31.82,32,33.54,34.09,34.6,36.77,39.59,42.09,44.99,45.26,46.62,47.66,47.72,50.89,71.79,124,141.68,217.08 化合物3的碳谱： 11.57,13.32,16.75,20.49,21.88,23.97,24.99,25.2,27.09,31.52,31.9,33.98,36.51,37.31,39.34,40.21,41.91,44.62,45.08,46.52,47.48,47.61,50.75,53.45,123.47,141.71,213.16,216.64  |
4楼2012-04-02 15:20:24
【答案】应助回帖
感谢参与，应助指数 +1
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结果太多，不能都复制，你先看一下吧 1 . 22β-hydroxy-12-oleanen-3-one C30H48O2 相似度:76.6% Journal of Natural Products 2008 71(11) 1829-1832 Triterpenoids and Aromatics from Derris laxiflora Hsi-Lin Chiu, Jyh-Horng Wu, Yu-Tang Tung, Tzong-Huei Lee, Shin-Chang Chien, and Yueh-Hsiung Kuo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . Abrisapogenol F 相似度:76.6% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 29-hydroxy-12-oleanene-3,22-dione C30H46O3 相似度:73.3% Journal of Natural Products 2008 71(11) 1829-1832 Triterpenoids and Aromatics from Derris laxiflora Hsi-Lin Chiu, Jyh-Horng Wu, Yu-Tang Tung, Tzong-Huei Lee, Shin-Chang Chien, and Yueh-Hsiung Kuo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . abrisapogenol F C30H48O2 相似度:73.3% Chemical & Pharmaceutical Bulletin 1989 37 846-848 NEW TRITERPENOID SAPOGENOLS FROM ABRUS CANTONIENSIS (I) Takashi TAKESHITA,Shuichi HAMADA and Toshihiro NOHARA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . Machaeric acid C30H46O4 相似度:73.3% Chemistry of Natural Compounds 2007 43 214-215 CHEMICAL RESEARCH OF Caragana microphylla Seeds Yan Huo, Cheng Guo, Shan Lu,Qiao-Yan Zhang, and Lu-Ping Qin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . Soyasapogenol E 相似度:73.3% Phytochemistry 1998 49 709-717 Bioactive polar triterpenoids from Melilotus messanensis Francisco A. Macías, Ana M. Simonet, Juan Carlos G. Galindo, Pedro C. Pacheco, Jose A. Sánchez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . camelliagenone C30H48O4 相似度:73.3% Chemical & Pharmaceutical Bulletin 2011 59(6) 778-782 New Triterpenes from Barringtonia asiatica Consolacion Yasaña RAGASA, Dinah Lorenzana ESPINELI, and Chien-Chang SHEN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . regelin D C31H48O4 相似度:70.9% Acta Pharmaceutica Sinica 1989 Vol 24 75-79 STUDIES ON NEW TRITERPENOIDS OF TRIPTERYGIUM REGELII GM Pang; CJ Zhao; H Hori and S Inayama Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 3-Oxo-12-en-28-(2'-nitro-vinyl)-olean C31H47NO3 相似度:70.9% Journal of Asian Natural Products Research 2012 14 355-363 Synthesis and biological evaluation of oleanolic acid derivatives as antitumor agents Lei Chen,Jian-Bo Wu,Fan Lei,Shan Qian,Li Hai and Yong Wu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . olean-18-en-3-one 相似度:70% Chemical & Pharmaceutical Bulletin 2002 50(9) 1273-1275 Fern Constituents: Triterpenoids from Adiantum capillus-veneris Takahisa NAKANE,Yoshiko MAEDA, Hideharu EBIHARA,Yoko ARAI,Kazuo MASUDA,Akihito TAKANO, Hiroyuki AGETA,Kenji SHIOJIMA,Shao-Qing CAI,and Osama Bashir ABDEL-HALIM Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . sumaresinolic acid 相似度:70% Journal of Natural Products 2006 69(5) 807-810 Triterpenoids from the Resin of Styrax tonkinensis and Their Antiproliferative and Differentiation Effects in Human Leukemia HL-60 Cells Feng Wang, Huiming Hua, Yuehu Pei, Duo Chen, and Yongkui Jing Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . 19α-hydroxyoleanonic acid C30H46O4 相似度:70% Journal of Natural Products 2006 69 1092-1094 Triterpenes from Natural and Transformed Roots of Plocama pendula Braulio M. Fraga, Carmen E. Daz, and Nayra Quintana Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 22β-Hydroxyoleanonic Acid 相似度:70% Chemistry of Natural Compounds 2006 42 442-444 OPTIMIZATION OF LANTADENES ISOLATION AND PREPARATION OF 22b-HYDROXYOLEANONIC ACID Manu Sharma and P. D. Sharma Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . β-amyrone 相似度:70% Acta Botanica Sinica 2001 43 426-430 The Chemical Constituents of Amoora yunnanensis LUO Xiao-Dong, WU Shao-Hua, MA Yun-Bao, WU Da-Gang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 3-oxo-19α-hydroxyurs-12-en-28-oic acid 相似度:70% China Journal of Chinese Materia Medica 2005 30 1833-1836 Triterpenes from root of Rhaponticum uniflorum ZHANG Yonghong, ZHANG Jiangang, XIE Jieming, CHEN Gelin, CHENG Dongliang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . cycloartenol 相似度:70% China Journal of Chinese Materia Medica 2003 28 1040-1042 Studies on Chemical Constituents in of Ervatamia hainanensis TAN Xingqi, CHEN Haisheng, XU Congli, LIU Runhui, XUAN Weidong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . soyasapogenol E 相似度:70% Journal of Natural Products 1988 Vol 51 335 Melilotigenin, a New Sapogenin from Melilotus officinalis Sam Sik Kang, Won Sick Woo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 3-oxo-19α-hydorxyurs-12-en-28-oic acid C30H46O4 相似度:70% Phytochemistry 1992 31 1317-1320 Pomolic acid derivatives from the rootof Sanguisorba officinalis Cheng, D. and Cao, X. Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 21-oxo-3,4-seco-olean-4(23)-12-dien-3-oic acid C30H46O3 相似度:70% Phytochemistry 1991 30 1221-1223 Seco ring-A triterpene acids from the resin of Dacryodes normandii Ian C. Parsons, Alexander I. Gray, Peter G. Waterman, Catherine Lavaud, Georges Massiot Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . β-amyrenone C30H48O 相似度:70% Chinese Journal of Natural Medicines 2010 8 270-273 Chemical Constituents from the Roots of Dysoxylum densiflorum LI Chang-Song; YU Hong-Wei; LI Guo-You; ZHANG Guo-Lin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . β-amyrone 相似度:70% Chinese Journal of Natural Medicines 2010 8 244-246 A New Benzoic Acid Derivative from Eclipta prostrata SUN Zhi-Hua; ZHANG Chao-Feng; ZHANG Mian Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . Cycloartenol C26H34O11 相似度:70% Chemistry of Natural Compounds 2010 46 459-461 Chemical investigation of Ervatamia yunnanensis Jing-Ling Du, Yong-Sheng Jin, Li-Ming Qiao, Li Jin and Hai-Sheng Chen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . 3β,4α,14α,20R,24R-4,14-二甲基麦角 相似度:70% Journal of China Pharmaceutical University 1997 28 271-274 Sterols from Sedum sarmentosum He Aimin; Hao Hongyan; Wang Mingshi; Zhang Decheng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 2α-Hydroxyurs-12-en-28-oic acid C30H48O3 相似度:68.9% Journal of Natural Products 2009 72 1414-1418 Synthesis of 3-Deoxypentacyclic Triterpene Derivatives as Inhibitors of Glycogen Phosphorylase Pu Zhang,Jia Hao,Jun Liu,Qian Lu, Huaming Sheng, Luyong Zhang, and Hongbin Sun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . 3α,22β-dihydroxyolean-12-ene C30H50O2 相似度:68.9% Natural Product Research 2002 16 415-418 Alysinol - A New Triterpene from Alysicarpus Monolifer Naheed Riaz; Itrat Anis; Pir Muhammad Khan; Raza Shah; Abdul Malik Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . compound 3 相似度:68.9% Phytochemistry 1994 37 1517-1575 13C NMR Spectra of pentacyclic triterpenoids—a compilation and some salient features Shashi B. Mahato, Asish P. Kundu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . (5R,8R,9R,10S,14S,17R,18R)-28-norolean-12-en-3,11,16-trione C29H42O3 相似度:68.9% Phytochemistry 2011 72 1804-1813 Triterpenes and neolignans from the roots of Nannoglottis carpesioides Cai-Bin Xue, Duo-Wu Chai, Xiao-Jie Jin, Yu-Rong Bi, Xiao-Jun Yao, Wang-Suo Wu, Ying Zhu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . Conicasterol H C29H48O3 相似度:68.9% Steroids 2012 77 484-495 4-Methylenesterols from Theonella swinhoei sponge are natural pregnane-X-receptor agonists and farnesoid-X-receptor antagonists that modulate innate immunity Simona De Marino ,Raffaella Ummarino,Maria Valeria D’Auria,Maria Giovanna Chini ,Giuseppe Bifulco,Claudio D’Amore ,Barbara Renga, Andrea Mencarelli,Sylvain Petek ,Stefano Fiorucci,Angela Zampella Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . mzikonone C28H38O5 相似度:68.9% Phytochemistry 1988 27 2353-2355 A new limonoid from Turraea robusta Mohamed S. Rajab,Michael D. Bentley,Ahmed Hassanali,Andrew Chapya Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . 21β,28-dihydroxy-3-oxo-olean-12,20(30)-diene C29H44O3 相似度:68.9% Tetrahedron 2001 57 8413-8424 Immunosuppressive terpenoids from extracts of Tripterygium wilfordii Hongquan Duan, Yoshihisa Takaishi, Hiroshi Momota, Yasukazu Ohmoto, Takao Taki, Motoo Tori, Shigeru Takaoka, Yongfeng Jia, Duan Li Structure 13C NMR 碳谱模拟图 |
5楼2012-04-02 15:38:01
6楼2012-04-02 15:54:17
【答案】应助回帖
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化合物2的搜索结果： 查询结果：共查到6984个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . 19β-28-Epoxy-18α-oieanan-3-one 相似度:73.3% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . camelliagenone C30H48O4 相似度:73.3% Chemical & Pharmaceutical Bulletin 2011 59(6) 778-782 New Triterpenes from Barringtonia asiatica Consolacion Yasaña RAGASA, Dinah Lorenzana ESPINELI, and Chien-Chang SHEN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 环阿尔廷-23Z-烯-3β,25-二醇（cycloart-23Z-ene-3β,25-diol) C30H50O2 相似度:72.4% Chinese Traditional and Herbal Drugs 2011 42(4) 664-667 Chemical constituents of Dracocephalum heterophyllum and antibacterial activity REN Ai-mei Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . olean-18-en-3-one 相似度:70% Chemical & Pharmaceutical Bulletin 2002 50(9) 1273-1275 Fern Constituents: Triterpenoids from Adiantum capillus-veneris Takahisa NAKANE,Yoshiko MAEDA, Hideharu EBIHARA,Yoko ARAI,Kazuo MASUDA,Akihito TAKANO, Hiroyuki AGETA,Kenji SHIOJIMA,Shao-Qing CAI,and Osama Bashir ABDEL-HALIM Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 3α,21β-dihydroxy-olean-12-ene 相似度:70% Phytochemistry 2008 69 1057-1064 21β-Hydroxy-oleanane-type triterpenes from Hippocratea excelsa David Cáceres-Castillo, Gonzalo J. Mena-Rejón,Roberto Cedillo-Rivera, Leovigildo Quijano Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . α-boswellic acid 相似度:70% Phytochemistry 2003 537-541 A lupane triterpene from frankincense (Boswellia sp., Burseraceae) Gérald Culioli, Carole Mathe, Paul Archier, Cathy Vieillescazes Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . β-boswellic acid 相似度:70% Phytochemistry 2003 537-541 A lupane triterpene from frankincense (Boswellia sp., Burseraceae) Gérald Culioli, Carole Mathe, Paul Archier, Cathy Vieillescazes Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . sumaresinolic acid 相似度:70% Journal of Natural Products 2006 69(5) 807-810 Triterpenoids from the Resin of Styrax tonkinensis and Their Antiproliferative and Differentiation Effects in Human Leukemia HL-60 Cells Feng Wang, Huiming Hua, Yuehu Pei, Duo Chen, and Yongkui Jing Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . siaresinolic acid 相似度:70% Journal of Natural Products 2006 69(5) 807-810 Triterpenoids from the Resin of Styrax tonkinensis and Their Antiproliferative and Differentiation Effects in Human Leukemia HL-60 Cells Feng Wang, Huiming Hua, Yuehu Pei, Duo Chen, and Yongkui Jing Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 19α-hydroxyoleanonic acid C30H46O4 相似度:70% Journal of Natural Products 2006 69 1092-1094 Triterpenes from Natural and Transformed Roots of Plocama pendula Braulio M. Fraga, Carmen E. Daz, and Nayra Quintana Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . subprogenin A 相似度:70% Chemical & Pharmaceutical Bulletin 1991 39 1908-1910 FOUR NEW AND TWELVE KNOWN SAPOGENOLS FROM SOPHORAE SUBPROSTRATE RADIX Takashi TAKESHITA,Kei YOKOYAMA,Ding YI,Junei KINJO and Toshihiro NOHARA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . Abrisapogenol F 相似度:70% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . pinicolic acid B, 3,16-dioxolanosta-8,24-dien-21-oic acid 相似度:70% Phytochemistry 1999 52 1621-1627 Steroids from the fungus Fomitopsis pinicola Joachim Rosecke, Wilfried A. Konig Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . Soyasapogenol E 相似度:70% Phytochemistry 1998 49 709-717 Bioactive polar triterpenoids from Melilotus messanensis Francisco A. Macías, Ana M. Simonet, Juan Carlos G. Galindo, Pedro C. Pacheco, Jose A. Sánchez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . soyasapogenol E 相似度:70% Journal of Natural Products 1988 Vol 51 335 Melilotigenin, a New Sapogenin from Melilotus officinalis Sam Sik Kang, Won Sick Woo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . soyasapogenol E 相似度:70% Journal of Natural Products 1991 Vol 54 830 Constituents of Leguminous Plants, XIII. New Triterpenoid Saponins from Wistaria brachybotrys Takao Konoshima, Mutsuo Kozuka, Mitsumasa Haruna, Kazuo Ito Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . subprogenin A 相似度:70% Phytochemistry 1994 37 1517-1575 13C NMR Spectra of pentacyclic triterpenoids—a compilation and some salient features Shashi B. Mahato, Asish P. Kundu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . Soyasapogenol E 相似度:70% Korean Journal of Pharmacognosy 2008 39(3) 186-193 Phytochemical Studies on Astragalus Root (3);Triterpenoids and Sterols Jung, Hye-Sil; Lee, Eun-Ju; Lee, Je-Hyun; Kim, Ju-Sun; Kang, Sam-Sik Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . bayogenin 相似度:70% Planta Medica 1995 61 246-249 New Triterpenoid Saponins, Asterbatanoside D and E, from Aster batangensis hao, Yu; Zhou, Bing-Nan; Ma, Kan; Wu, Hou-Ming Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . 2,3-seco-19β,28-Epoxy-28-oxo-18α-olean-2,3-dioic Acid C30H46O6 相似度:70% Chemistry of Natural Compounds 2010 46 393-396 Effective synthesis of 2,3-seco-2,3-dicarboxyplatanic acid O. B. Kazakova, E. F. Khusnutdinova, O. S. Kukovinets, T. I. Zvereva and G. A. Tolstikov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 常春藤皂苷元 C30H48O4 相似度:70% Journal of China Pharmaceutical University 2003 34 222-224 Chemical Constituents from the Root of Polygala fallax Hemsl. ZHU Dan-Ni; LI Li; ZHU Yao-Jun; YAN Yong-Qing Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . α-Boswellic acid C30H48O3 相似度:70% Natural Product Communications 2008 3 21-26 Boswellic Acids with Acetylcholinesterase InhibitoryProperties from Frankincense Masahiro Ota and Peter J. Houghton Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . 3-oxo-22α-hydroxy-olean-12-en-28-oic acid C30H46O4 相似度:70% Natural Product Communications 2012 7 13-14 Constituents of Kenyan Gardenia volkensii Esther W. Kinuthia, Moses K. Langat*, Elizabeth M. Mwangi and Peter K Cheplogoi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 3α-hydroxyolean-12-dien-23,28-dioic acid 相似度:68.9% Acta Pharmaceutica Sinica 2004 Vol 39 354-358 Structures of four new triterpenoid saponins from the leaves of Oplopanax elatus Nakai WANG Guang-shu; YANG Xiao-hong; XU Jing-da Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . compound 3 相似度:68.9% Phytochemistry 1994 37 1517-1575 13C NMR Spectra of pentacyclic triterpenoids—a compilation and some salient features Shashi B. Mahato, Asish P. Kundu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . 17,24-epoxy-20α,25-dihydroxy-21-norbaccharan-3-one C29H48O4 相似度:68.9% Journal of Natural Products 2010 73 1873-1878 Isolation and Characterization of Minor Analogues of Silvestrol and Other Constituents from a Large-Scale Re-collection of Aglaia foveolata Li Pan, Leonardus B. S. Kardono, Soedarsono Riswan, Heebyung Chai, Esperanza J. Carcache de Blanco, Caroline M. Pannell, Djaja Doel Soejarto, Thomas G. McCloud, David J. Newman, and A. Douglas Kinghorn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . 3-oxoberenjenol 相似度:67.7% Journal of Natural Products 2007 70 835-838 Constituents of Oxandra cf. xylopioides with Anti-inflammatory Activity Benjamin Rojano, Edwin Pérez,Bruno Figadère,Marie Thérèse Martin, María C. Recio,Rosa Giner,José L. Ríos, Guillermo Schinella,and Jairo Sáez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . 3-oxoolean-12-en-30-oic acid methyl ester C31H47O3 相似度:67.7% Chemistry of Natural Compounds 2009 45 519-521 BECKMANN REARRANGEMENT OF 11-DEOXO-GLYCYRRHETICACID 3-KETOXIME L. R. Mikhailova, M. V. Khudobko,L. A. Baltina, Jr., and L. A. Baltina Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . 3-oxcolean-12-en-28-oic acid 相似度:67.7% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . compound 1b 相似度:67.7% Natural Product Research 1994 5 233-240 Two new Triterpenoid Saponins, Asterbatanoside F and G, from Aster batangensis Yu Shao; Bing-Nan Zhou; Long-Ze Lin; Geoffrey A. Cordell Structure 13C NMR 碳谱模拟图 |
7楼2012-04-02 15:57:58
【答案】应助回帖
★ ★
xiaoxiao270: 金币+2, 3Q 2012-04-02 17:23:28
xiaoxiao270: 金币+2, 3Q 2012-04-02 17:23:28
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化合物3的结果： Chemistry & Biodiversity 2008 Vol. 5 751 New Pentacyclic Triterpenes from Gypsophila oldhamiana and Their Biological Evaluation as Glycogen Phosphorylase Inhibitors Jian-Guang Luo, Jun Liu, and Ling-Yi Kong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 3-Keto,16α-hydroxy,24-noroleanolic acid 相似度:75.8% Bioorganic & Medicinal Chemistry 2008 16 2912-2920 New triterpenoid saponins with strong α-glucosidase inhibitory activity from the roots of Gypsophila oldhamiana Jian-Guang Luo, Li Ma, Ling-Yi Kong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . compound 5 C27H40O4 相似度:71.4% Phytochemistry 1990 29 919-922 Dammarane triterpenes of Salvia hierosolymitana Samuel Pedreros,Benjamin Rodríguez,María C. De La Torre,Maurizio Bruno,Giuseppe Savona,Aurea Perales,Maria R. Torres Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . Methyl(20R)-20-(4-methyl-3-pentenyl)-3-oxo-pregnan-1-en-21-oate C28H42O3 相似度:71.4% Steroids 2010 75 1153-1163 Synthesis and antitumor evaluation of methyl spongoate analogs Cheng-Shi Jiang, Cai-Guo Huang, Bo Feng, Jia Li, Jing-Xu Gong, Tibor Kurtán, Yue-Wei Guo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . Soyasapogenol E 相似度:70% Phytochemistry 1998 49 709-717 Bioactive polar triterpenoids from Melilotus messanensis Francisco A. Macías, Ana M. Simonet, Juan Carlos G. Galindo, Pedro C. Pacheco, Jose A. Sánchez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . camelliagenone C30H48O4 相似度:70% Chemical & Pharmaceutical Bulletin 2011 59(6) 778-782 New Triterpenes from Barringtonia asiatica Consolacion Yasaña RAGASA, Dinah Lorenzana ESPINELI, and Chien-Chang SHEN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 3-oxoolean-12-en-30-oic acid methyl ester C31H47O3 相似度:67.7% Chemistry of Natural Compounds 2009 45 519-521 BECKMANN REARRANGEMENT OF 11-DEOXO-GLYCYRRHETICACID 3-KETOXIME L. R. Mikhailova, M. V. Khudobko,L. A. Baltina, Jr., and L. A. Baltina Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 3-Oxo-16β-hydroxy-olean-12-en-28-al C30H46O3 相似度:66.6% Chemical & Pharmaceutical Bulletin 2007 55(4) 577-579 A Novel Benzofuran Derivative, a New Olean-Type Triterpene and Other Constituents from Ligularia odontomanes Dong Qing FEI, Gang WU, Chun Mei LIU, and Kun GAO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 22β-hydroxy-12-oleanen-3-one C30H48O2 相似度:66.6% Journal of Natural Products 2008 71(11) 1829-1832 Triterpenoids and Aromatics from Derris laxiflora Hsi-Lin Chiu, Jyh-Horng Wu, Yu-Tang Tung, Tzong-Huei Lee, Shin-Chang Chien, and Yueh-Hsiung Kuo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 29-hydroxy-12-oleanene-3,22-dione C30H46O3 相似度:66.6% Journal of Natural Products 2008 71(11) 1829-1832 Triterpenoids and Aromatics from Derris laxiflora Hsi-Lin Chiu, Jyh-Horng Wu, Yu-Tang Tung, Tzong-Huei Lee, Shin-Chang Chien, and Yueh-Hsiung Kuo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . 23-Hydroxylongispinogenin 相似度:66.6% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . Abrisapogenol F 相似度:66.6% Chemistry of Natural Compounds 1992 28 1-23 13C NMR SPECTROSCOPY OF OLEANANE DERIVATIVES A. I. Kalinovskii Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . soyasapogenol E 相似度:66.6% Journal of Natural Products 1988 Vol 51 335 Melilotigenin, a New Sapogenin from Melilotus officinalis Sam Sik Kang, Won Sick Woo Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . gypsogenic acid 相似度:66.6% Archives of Pharmacal Research 1985 8 133-137 Phytochemical study on Melandrium firmum Won Sick Woo, Jae Sue Choi and Hye Soon Chang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 3-oxo-22α-hydroxy-olean-12-en-28-oic acid C30H46O4 相似度:66.6% Natural Product Communications 2012 7 13-14 Constituents of Kenyan Gardenia volkensii Esther W. Kinuthia, Moses K. Langat*, Elizabeth M. Mwangi and Peter K Cheplogoi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . acinospesigenin-A C32H50O6 相似度:65.6% Journal of Natural Products 2003 66 1121-1123 Acinospesigenin-A, -B, and -C: Three New Triterpenoids from Phytolacca acinosa Summon Koul, T. K. Razdan,and C. S. Andotra Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 19a-hydroxy-3-oxo-24-norolean-12-en-28-oic acid C29H44O4 相似度:65.5% Helvetica Chimica Acta 2006 Vol. 89 1971 Three New 24-Noroleanane Triterpenoids from Quercus aliena var. acuteserrata Hua-Dong Chen, Sheng-Ping Yang, Shang-Gao Liao, Chuan-Rui Zhang, and Jian-Min Yue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 2a,19a-dihydroxy-3-oxo-24-norolean-12-en-28-oic acid C29H44O5 相似度:65.5% Helvetica Chimica Acta 2006 Vol. 89 1971 Three New 24-Noroleanane Triterpenoids from Quercus aliena var. acuteserrata Hua-Dong Chen, Sheng-Ping Yang, Shang-Gao Liao, Chuan-Rui Zhang, and Jian-Min Yue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 24-nor-2α,3β-dihydroxyolean-4(23),12-ene (4) C29H46O2 相似度:65.5% Planta Medica 2006 72 643-649 New Polyhydroxylated Triterpenes and Anti-Inflammatory Activity of Salvia hierosolymitana A. De Felice,A. Bader,A. Leone,S. Sosa,R. Della Loggia,A. Tubaro,N. De Tommasi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . 17β-hydroxy-3,16-dioxo-28-norolean-12-ene C29H44O3 相似度:65.5% Planta Medica 2003 69 258-264 New Dihydrobenzofurans and Triterpenoids from Roots of Microglossa pyrifolia homas J.Schmidt,Meike R.Hildebrand,Günter Willuhn Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . 3-keto,16α-hydroxyl,24-noroleanolic acid 相似度:65.5% Phytochemistry 1998 48 529-536 Triterpenoid saponins and sapogenins from Vaccaria segetalis Zhonghua Jia, Kazuo Koike, Momoe Kudo, Hongyu Li, Tamotsu Nikaido Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . aglycone of dianchinenoside A 相似度:65.5% Journal of Natural Products 1993 Vol 56 1065 Dianchinenosides A and B, Two New Saponins from Dianthus chinensis Hong-yu Li, Kazuo Koike, Taichi Ohmoto, Keiji Ikeda Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . (5R,8R,9R,10S,14S,17R,18R)-28-norolean-12-en-3,11,16-trione C29H42O3 相似度:65.5% Phytochemistry 2011 72 1804-1813 Triterpenes and neolignans from the roots of Nannoglottis carpesioides Cai-Bin Xue, Duo-Wu Chai, Xiao-Jie Jin, Yu-Rong Bi, Xiao-Jun Yao, Wang-Suo Wu, Ying Zhu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 3-N-1-[N(3-[4-Aminobutyl])-1,3-diaminopropane]-7,22-dihydroxy-23,24-bisnor-5α-cholane trihydrochloride C29H55N3O2 相似度:65.5% Bioorganic & Medicinal Chemistry 2000 8 2059-2065 Synthesis and antimicrobial activity of squalamine analogue Hong-Seok Kim, Bo-Seung Choi, Kyung-Chan Kwon, Sang-Ok Lee, Hyun Jung Kwak, Cheol Hae Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . (22E,24S)-3α,5-cyclo-stigmast-22-en-6-one 相似度:65.5% Steroids 2012 77 91-99 Brassinosteroids and analogs as neuroprotectors: Synthesis and structure–activity relationships Jihane Ismaili, Martin Boisvert, Fanny Longpré, Julie Carange, Céline Le Gall, Maria-Grazia Martinoli, Benoit Daoust Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . β-sitosterol-3-O-stearate 相似度:65.5% Natural Product Research and Development 1996 8(1) 5-9 THE CONSTITUENTS FROM THE RHIZOMA OF ALTSMA ORIENTALIS (SAM) JUZEP. Cai Lining; Wang Hongshu; Cao Hongxing; Zhang Ruyi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . 21β,28-dihydroxy-3-oxo-olean-12,20(30)-diene C29H44O3 相似度:65.5% Tetrahedron 2001 57 8413-8424 Immunosuppressive terpenoids from extracts of Tripterygium wilfordii Hongquan Duan, Yoshihisa Takaishi, Hiroshi Momota, Yasukazu Ohmoto, Takao Taki, Motoo Tori, Shigeru Takaoka, Yongfeng Jia, Duan Li Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . 3-oxohederagenin 相似度:64.5% Journal of Natural Products 1999 62 445-448 Triterpenoid Saponins of Acanthopanax nipponicus Leaves Masazumi Miyakoshi, Katsuya Shirasuna, Yasuaki Hirai, Kazushi Shingu, Susumu Isoda, Junzo Shoji, Yoshiteru Ida, and Torao Shimizu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . pisonolic acid C31H48O5 相似度:64.5% Journal of Natural Products 2011 74 976-982 Antitubercular Chromones and Flavonoids from Pisonia aculeata Ming-Chun Wu, Chien-Fang Peng, Ih-Sheng Chen, and Ian-Lih Tsai Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . remangilone B C28H38O3 相似度:64.2% Journal of Natural Products 1999 62 471-476 Remangilones A-C, New Cytotoxic Triterpenes from Physena madagascariensis Yonghong Deng, Tian-Yi Jiang, Shijie Sheng, Manoelson Tianasoa-Ramamonjy, and John K. Snyder Structure 13C NMR 碳谱模拟图 |
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