24小时热门版块排行榜

返回列表

当前只显示满足指定条件的回帖，点击这里查看本话题的所有回帖

guo-qian

铜虫 (小有名气)

应助: 0 (幼儿园)
金币: 60.8
散金: 20
帖子: 77
在线: 23.8小时
虫号: 1152775
注册: 2010-11-22
性别: MM
专业: 化石能源储存与输送

[求助] 投稿 Acta E，编辑给的修改意见，请各位大侠给解释下，在线等结果~

4) Values for wR2 for the submitted FCF file and those calculated by checkCIF are different. This is usually caused by the FCF and CIF being from different rounds of refinement. Please ensure that these files come from the same refinement round.

6) Abstract: There is pi-pi stacking of inversion related pyridine rings, and of at least one of the phenyl groups (C9-C14). These interactions should be described, including the interplanar spacing or centroid-centroid distances (with SU values).

7) Related literature: Please expand this section by giving some indication of what the cited references are for. Also, for the cited reference the proper citation would be "Speier & Fulop (1989)". Please see the Notes for Authors for more detail.

8) Computing details: _computing_data_collection should be the name of a program, not the name of a machine.

9) Refinement: The description of hydrogen atom treatment is incomplete. The methyl H atoms were placed at a distance of 0.96Å with Uiso = 1.5Ueq(C).

CIF formatting details:

_symmetry_space_group_name_H-M 'P -1'
_symmetry_space_group_name_Hall '-P 1'

_diffrn_standards_interval_count .
_diffrn_standards_interval_time .
_diffrn_standards_decay_% ?

_reflns_threshold_expression >2\s(I)

'calc w=1/[\s^2^(Fo^2^)+(0.0637P)^2^] where P=(Fo^2^+2Fc^2^)/3'

以上是本人不懂的东西，恳请各位大侠帮忙，十万火急，在线等消息，谢谢