²é¿´: 1135  |  »Ø¸´: 2
±¾Ìû²úÉú 1 ¸ö ·­ÒëEPI £¬µã»÷ÕâÀï½øÐв鿴

yongbinz

½ð³æ (ÖøÃûдÊÖ)

[ÇóÖú] ¼±ÇóººÒëÓ¢Ò»¶Î»°£¬100½ð±Ò£¬Ð»¾øÈí¼þ·­Ò룡

Èçͼ7Ëùʾ£¬ÒÔDMAͼÖÐTan¦ÄÇúÏßÉϵķ嶥ζȱíʾ¸÷PIµÄ²£Á§»¯×ª±äζȣ¬ÕâЩ±¡Ä¤µÄ²£Á§»¯×ª±äζȳöÏÖÔÚ305£­433¡æµÄ¸ßη¶Î§ÄÚ£¬±íÃ÷ËùÓоۺÏÎï¾ù¾ßÓÐÓÅÒìµÄÈÈÎȶ¨ÐÔ¡£¾ù¾ÛÎïA³öÏÖÁ½¸öÃ÷ÏÔµÄËðºÄ·å£¬¶ÔÓ¦ÓÚÁ½¸ö²£Á§»¯×ª±ä¡£ÓÉWAXDµÄ½áÂÛ£¬ÎÒÃÇÖªµÀ¾ù¾ÛÎïA¾ßÓнϸߵÄÓÐÐò¶È£¬Òò´Ë£¬ÎÒÃÇÍÆ¶Ï£¬ÔÚµÍÎÂÇøµÄ¸ßTan¦ÄËðºÄ·å¶ÔÓ¦ÓÚÎÞ¶¨ÐÍÇøµÄ²£Á§»¯×ª±ä£¨304¡æ£©£¬¶øÔÚ¸ßÎÂÇøµÄµÍTan¦ÄËðºÄ·åÔò¶ÔÓ¦ÓÚÆä½á¾§»òÓÐÐòÇøµÄ·Ö×ÓÁ´ËɳÚת±ä£¨410¡æ£©¡£¾ù¾ÛÎïEÖ»ÔÚ433¡æ´¦³öÏÖÒ»¸ö²£Á§»¯×ª±ä£¬ÕâÓëÒÔǰµÄÑо¿½á¹ûÏà·û[4]¡£ËùÓй²¾ÛÎïµÄDMAÇúÏßͼÖоùÖ»³öÏÖÒ»¸öÃ÷ÏÔµÄTanËðºÄ·å£¬ËµÃ÷ËüÃǾùÐγÉÁËÎ޹湲¾ÛÎ¼´BDA/OAÓëBDA/IAÁ´¶ÎÑØ×Ź²¾ÛÎï·Ö×ÓÁ´½øÐÐÁËÎÞ¹æÅÅÁС£¶ÔÓ¦ÓÚ¾ù¾ÛÎïAµÄ½á¾§»òÓÐÐòÇøÄÚ·Ö×ÓÁ´Ô˶¯µÄ²£Á§»¯×ª±ä£¨Ô¼Îª410¡æ£©µÄTan¦ÄËðºÄ·åÔÚ¹²¾ÛÎïÖÐÏûʧÁË£¬Õâ¿ÉÄܹéÒòÓÚ¹²¾ÛÎïµÄÓÐÐò¶È̫С£¬Òò¶øÆäÔÚÓÐÐòÇøÄÚµÄÎÞ¶¨ÐÍ·Ö×ÓÁ´µÄ²£Á§»¯×ª±ä²»Ã÷ÏÔ¡£¹²¾ÛÎïB¡¢C¡¢DµÄ²£Á§»¯×ª±äζȷֱðΪ339¡¢372¡¢387¡æ£¬±íÃ÷²£Á§»¯×ª±äζÈËæ×Ź²¾ÛÎïÖÐBOAº¬Á¿µÄ¼õÉÙ¶øÔö¼Ó¡£ÓɺìÍâ½áÂÛ£¬õ£°·½á¹¹µÄÒýÈëʹ¾Ûõ£Ñǰ·ÌåϵÄÚÇâ¼üÏ໥×÷ÓÃÔöÇ¿£¬Òò´Ë£¬²£Á§»¯×ª±äζȵÄÔö¼Ó¹éÒòÓÚ¹²¾ÛÎï·Ö×ÓÁ´¼äÏ໥×÷ÓõÄÔöÇ¿¡£

» ²ÂÄãϲ»¶

ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

lewmihu

½ð³æ (СÓÐÃûÆø)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï ¡ï
sltmac(½ð±Ò+50): 2011-12-28 10:40:59
sltmac(½ð±Ò+50, ·­ÒëEPI+1): »¶Ó­³£À´±¾°æ½»Á÷ 2011-12-28 10:41:13
sltmac(½ð±Ò-40): 2011-12-31 09:02:10
sltmac(½ð±Ò-10): ·­ÒëÒ»°ë 2011-12-31 09:02:30
as DMA in Fig7 show, the peak temperature of the Tan¦Ä curve represent the vitrification transformation temperature of each PI which ranges in high temperature of 305~433¡æ indicate that all the polymer provided with a excellent hermostability. There are two obvious loss peak in Homopolymer A correspond to two vitrification transformation. We know that there are a high extent ordering in Homopolymer A from WAXD¡¯s conclusion .since we conclude that the high Tan¦Ä loss peak in low temperature area correspond to vitrification transformation of undefined area. Moreover , the low Tan¦Ä loss peak in high temperature area correspond to relaxation transformation of crystallization and ordered area. There are only one vitrification transformation in Homopolymer E which is consist with the result of the  former research. There are only one obvious tan loss peak appeard in all DMA curve indicate that all the Homopolymer have formed ruleless Homopolymer.

ûʱ¼äÁË ÏÈ·­Õâô¶à°É
×ß×Ô¼ºµÄ·ÈñðÈË´ò³µÈ¥°É
2Â¥2011-12-11 12:35:58
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû

lewmihu

½ð³æ (СÓÐÃûÆø)

¡¾´ð°¸¡¿Ó¦Öú»ØÌû

¡ï ¡ï
°®ÓëÓêÏÂ(½ð±Ò+2): 2011-12-12 08:35:42
as DMA in Fig7 show, the peak temperature of the Tan¦Ä curve represent the vitrification transformation temperature of each PI which ranges in high temperature of 305~433¡æ indicate that all the polymer provided with a excellent hermostability. There are two obvious loss peak in Homopolymer A correspond to two vitrification transformation. We know that there are a high extent ordering in Homopolymer A from WAXD¡¯s conclusion .since we conclude that the high Tan¦Ä loss peak in low temperature area correspond to vitrification transformation of undefined area. Moreover , the low Tan¦Ä loss peak in high temperature area correspond to relaxation transformation of crystallization and ordered area. There are only one vitrification transformation in Homopolymer E which is consist with the result of the  former research. There are only one obvious tan loss peak appeard in all DMA curve indicate that all the Homopolymer have formed ruleless Homopolymer.

ûʱ¼äÁË ÏÈ·­Õâô¶à°É
×ß×Ô¼ºµÄ·ÈñðÈË´ò³µÈ¥°É
3Â¥2011-12-11 12:36:33
ÒÑÔÄ   »Ø¸´´ËÂ¥   ¹Ø×¢TA ¸øTA·¢ÏûÏ¢ ËÍTAºì»¨ TAµÄ»ØÌû
Ïà¹Ø°æ¿éÌø×ª ÎÒÒª¶©ÔÄÂ¥Ö÷ yongbinz µÄÖ÷Ìâ¸üÐÂ
×î¾ßÈËÆøÈÈÌûÍÆ¼ö [²é¿´È«²¿] ×÷Õß »Ø/¿´ ×îºó·¢±í
[¿¼ÑÐ] Ò»Ö¾Ô¸ÎäÀí²ÄÁϹ¤³Ì348Çóµ÷¼Á +5 £þ^£þ©bº¹ 2026-03-19 7/350 2026-03-22 19:44 by ¹«èªåÐÒ£
[¿¼ÑÐ] 306Çóµ÷¼Á +6 chuanzhu´¨Öò 2026-03-18 6/300 2026-03-22 19:39 by ¹«èªåÐÒ£
[¿¼ÑÐ] ÉúÎïѧ071000 329·ÖÇóµ÷¼Á +5 ÎÒ°®ÉúÎïÉúÎﰮΠ2026-03-17 5/250 2026-03-22 16:42 by tcx007
[¿¼ÑÐ] Ò»Ö¾Ô¸ Î÷±±´óѧ £¬070300»¯Ñ§Ñ§Ë¶£¬×Ü·Ö287£¬Ë«·ÇÒ»±¾£¬Çóµ÷¼Á¡£ +3 ³¿»èÏßÓëÐǺ£ 2026-03-20 3/150 2026-03-22 16:00 by ColorlessPI
[¿¼ÑÐ] Çóµ÷¼ÁԺУÐÅÏ¢ +6 CX 330 2026-03-21 6/300 2026-03-22 15:25 by ÎÞи¿É»÷111
[¿¼ÑÐ] »¯Ñ§µ÷¼Á +5 yzysaa 2026-03-21 5/250 2026-03-21 22:12 by peike
[¿¼ÑÐ] ²ÄÁÏÓ뻯¹¤£¨0856£©304ÇóBÇøµ÷¼Á +3 Çñgl 2026-03-20 7/350 2026-03-21 19:05 by 15709483992
[¿¼ÑÐ] 299Çóµ÷¼Á +5 shxchem 2026-03-20 7/350 2026-03-21 17:09 by ColorlessPI
[¿¼ÑÐ] 316Çóµ÷¼Á +6 ÁºÜçö© 2026-03-19 6/300 2026-03-21 06:32 by Ecowxq666£¡
[¿¼ÑÐ] 346Çóµ÷¼Á[0856] +4 WayneLim327 2026-03-16 7/350 2026-03-21 04:02 by JourneyLucky
[¿¼ÑÐ] »ª¶«Ê¦·¶´óѧ-071000ÉúÎïѧ-293·Ö-Çóµ÷¼Á +3 Ñо¿ÉúºÎÑþÃ÷ 2026-03-18 3/150 2026-03-21 01:30 by JourneyLucky
[¿¼ÑÐ] Ò»Ö¾Ô¸Î÷ÄϽ»´ó£¬Çóµ÷¼Á +5 ²Ä»¯ÖðÃÎÈË 2026-03-18 5/250 2026-03-21 00:26 by JourneyLucky
[¿¼ÑÐ] ÄϾ©´óѧ»¯Ñ§376Çóµ÷¼Á +3 hisfailed 2026-03-19 6/300 2026-03-20 23:43 by hisfailed
[¿¼ÑÐ] 261ÇóBÇøµ÷¼Á£¬¿ÆÑо­Àú·á¸» +3 Å£Ä̺Üæ 2026-03-20 4/200 2026-03-20 19:34 by JourneyLucky
[¿¼ÑÐ] 298-Ò»Ö¾Ô¸Öйúũҵ´óѧ-Çóµ÷¼Á +9 ÊÖ»úÓû§ 2026-03-17 9/450 2026-03-20 14:24 by ÎÞи¿É»÷111
[¿¼ÑÐ] 085410È˹¤ÖÇÄÜר˶317Çóµ÷¼Á£¨0854¶¼¿ÉÒÔ£© +4 xbxudjdn 2026-03-18 4/200 2026-03-20 09:07 by ²»168
[¿¼ÑÐ] Ò»Ö¾Ô¸Öйúº£Ñó´óѧ£¬ÉúÎïѧ£¬301·Ö£¬Çóµ÷¼Á +5 1ËïÎò¿Õ 2026-03-17 6/300 2026-03-19 23:46 by zcl123
[¿¼ÑÐ] 085600²ÄÁÏÓ뻯¹¤Çóµ÷¼Á +6 Ð÷ÐÒÓë×Ó 2026-03-17 6/300 2026-03-19 13:27 by houyaoxu
[¿¼ÑÐ] ±¾¿ÆÖ£ÖÝ´óѧÎïÀíѧԺ£¬Ò»Ö¾Ô¸»ª¿Æ070200ѧ˶£¬346Çóµ÷¼Á +4 ÎÒ²»ÊÇÒ»¸ù´Ð 2026-03-18 4/200 2026-03-19 09:11 by ¸¡ÔÆ166
[¿¼ÑÐ] 301Çóµ÷¼Á +4 A_JiXing 2026-03-16 4/200 2026-03-17 17:32 by ruiyingmiao
ÐÅÏ¢Ìáʾ
ÇëÌî´¦ÀíÒâ¼û