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jamon1212

铜虫 (初入文坛)

[求助] 关于川乌含量测定减压蒸干的问题

川乌含量测定是(药典法):用异丙醇-乙酸乙酯(1:1)混合,溶剂在40℃以下减压回收溶剂至干,可是这两种溶剂在40度下减压蒸干基本上没什么变化,但是如果把温度提高不知道是否对有效成分有影响,该如何处理,青做过的大侠指教一下,非常感谢!
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yzkww

金虫 (小有名气)

【答案】应助回帖

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qinhy(金币+1): 多谢参与交流~ 2011-11-14 22:02:57
这两种溶剂在40度下减压蒸干基本上没什么变化。是因为你的减压真空度不够造成的!保持真空度大于95%肯定没问题。
2楼2011-11-14 17:30:01
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