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xiaogutou

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[求助] 求助一段英文翻译

To a cooled  suspension of  the hydroxy-9-xanthenone (0.01 mole)  in glacial acetic acid  (30 ml)  was added the  secondarv base  (0.011 mole),  followed  by paraformaldehyde  (0.011 mole). The reaction  mixture was then  heated  under  reflux  for  4  hours  and  left overnight  at room  temperature. After  the  acetic  acid was removed, in  a vacuum, the residue was treated with dilute hydrochloric acid  to dissolve  the Mannich base formed.  The  reaction  mixture  was  filtered  and  the  cooled  filtrate  was  made  alkaline  with  ammonium hydroxide. The product was isolated either in the form of  the solid free base or its hydrochloride . The hydrochloride was formed by saturating the dry ethereal solution of  the base with dry hydrogen chloride gas.

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editorlin

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【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★
爱与雨下(金币+1): !~ 2011-09-15 08:41:01
sltmac(金币+2): 欢迎常来~ 2011-09-16 08:09:32
sltmac(金币+5, 翻译EPI+1): 2011-09-19 10:15:41
sltmac: 感谢应助,欢迎常来~ 2011-09-19 10:15:46
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广结纳米材料同好,乐谈学术论文写作!editorlin@sina.com或hqgcxyxb@sina.com
2楼2011-09-14 22:13:35
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