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| 1-Hexanethiol. A mixture of n-hexyl chloride (3.49 g, 0.029 mol) and 15 mL of a 2.2 M H2S (0.033 mol) solution in equal volumes of Et3N and methanol was heated in a sealed glass tube at 75℃ for 6h. Analysis by GLC indicated that the reaction was 80% complete with the products being 99.1% 1-hexanethiol and 0.9% dihexyl sulfide. |
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2楼2011-05-23 12:32:44