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[求助]
摘要请人帮忙翻译下，用在线翻译直接翻译的就不用打酱油了。谢谢
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| 以氯代苯乙酮为原料，经Wolff-Kishner-黄鸣龙还原法合成2-氯代乙基苯。通过正交实验考察了原料配比、反应时间等因素与2-氯代乙基苯收率的关系。产物通过红外光谱表征，经比较，初步确定该反应的最佳工艺条件： 在120 ℃下氯代乙基苯与85 %水合肼的投料比为1 ∶7 (物质的量比) 时, 反应2 h ,2-氯代乙基苯的收率达到90.1 % 。 |
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3楼2011-05-17 11:46:20
【答案】应助回帖
★ ★
Mally89(金币+2): 感谢老哥应助！↖(^ω^)↗ 2011-05-17 11:52:22
lianty(金币+20, 翻译EPI+1): 谢谢 2011-05-17 16:45:05
Mally89(金币+2): 感谢老哥应助！↖(^ω^)↗ 2011-05-17 11:52:22
lianty(金币+20, 翻译EPI+1): 谢谢 2011-05-17 16:45:05
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2 - chloro-ethyl benzene was synthesized by chlorinated acetophenone via Wolff-Kishner-Huangminglong reduction. the relationship between raw material ratio and reaction time and 2 - chloro-ethyl benzene yield was Investigated by orthogonal test. products were characterized by FT-IR, and the best optimum conditions was at 120 ℃ and the ratio 85% chloro-ethylbenzene feed and hydrazine was at 1: 7 (molar ratio), the reaction of 2 h and the yield of 2 - chloro-ethyl benzene was 90.1%. of and relationship. Products by IR spectroscopy, by comparison, the initial reaction to determine the |
2楼2011-05-17 11:45:55
